JPS60126821A - Sample heating device, normal pressure cvd device and vacuum cvd device - Google Patents

Sample heating device, normal pressure cvd device and vacuum cvd device

Info

Publication number
JPS60126821A
JPS60126821A JP23528783A JP23528783A JPS60126821A JP S60126821 A JPS60126821 A JP S60126821A JP 23528783 A JP23528783 A JP 23528783A JP 23528783 A JP23528783 A JP 23528783A JP S60126821 A JPS60126821 A JP S60126821A
Authority
JP
Japan
Prior art keywords
sample
optical fiber
heating device
infrared light
sample heating
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP23528783A
Other languages
Japanese (ja)
Other versions
JPH069187B2 (en
Inventor
Yoichi Onishi
陽一 大西
Junichi Nozaki
野崎 順一
Hirozo Shima
島 博三
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Panasonic Holdings Corp
Original Assignee
Matsushita Electric Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Matsushita Electric Industrial Co Ltd filed Critical Matsushita Electric Industrial Co Ltd
Priority to JP23528783A priority Critical patent/JPH069187B2/en
Publication of JPS60126821A publication Critical patent/JPS60126821A/en
Publication of JPH069187B2 publication Critical patent/JPH069187B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104Forming layers
    • H01L21/02365Forming inorganic semiconducting materials on a substrate
    • H01L21/02612Formation types
    • H01L21/02617Deposition types
    • H01L21/0262Reduction or decomposition of gaseous compounds, e.g. CVD
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104Forming layers
    • H01L21/02365Forming inorganic semiconducting materials on a substrate
    • H01L21/02518Deposited layers
    • H01L21/02521Materials
    • H01L21/02524Group 14 semiconducting materials
    • H01L21/02532Silicon, silicon germanium, germanium

Abstract

PURPOSE:To unify distribution of the surface temperature of a sample by a method wherein window holes of the plural number of pieces are provided to a sample base to load a sample to be heated, the tips of optical fibers are inserted therein respectively, and infrared light sources enabled to control arbitrary the supply quantity are provided at the rear ends thereof. CONSTITUTION:A sample base 11 is provided with a loading base 13 to load a sample 12 to be heated and consisting of a transparent quartz plate. Window holes 14 of the plural number of pieces are provided thereto, and the tips of optical fibers 15 are inserted respectively into the window holes 14 thereof. Infrared light sources 16 are provided at the rear ends of the optical fibers 15. When infrared lights supplied through the optical fibers 15 from the light sources 16 of the plural number of pieces are controlled, heating of the sample 12 can be controlled partially or wholly. When an exhaust vent 19 to be connected to a vacuum pump 20 is provided to a closed vessel 17, a vacuum CVD device is constructed.

Description

【発明の詳細な説明】 〔発明の目的〕本発明は半導体基板にシリコン薄膜を蒸
着する場合等に使用する試料加熱装置並びに該試料加熱
装置を備えた常圧OVD装置および減圧OVD装置に関
するものである。なお、OVDはChemical v
apowr Depositionの頭文字である。O
VD装置は密閉容器内において試料を加熱し、形成され
る薄M管組成元素を含む化合物ガスを供給し、試料の表
面から発生する熱エネルギーによって前記化合物ガスを
分解して試料の表面に薄膜を形成させる装置であって、
常圧で行なう場合と、減圧、又は真空で行なう場合とが
ある。CVD装置によって形成さハる薄膜の良否U膜質
および膜厚分布の均一性によっで定するので良質の薄膜
をうるためには供給されるガスの分布、試料の温度およ
び加熱の分布等を十分に監視制御する必要がある。
DETAILED DESCRIPTION OF THE INVENTION [Object of the Invention] The present invention relates to a sample heating device used for depositing a silicon thin film onto a semiconductor substrate, and an atmospheric pressure OVD device and a reduced pressure OVD device equipped with the sample heating device. be. In addition, OVD is Chemical v
It is an acronym for ``apowr Deposition''. O
The VD device heats a sample in a sealed container, supplies a compound gas containing the constituent elements of the thin M tube to be formed, and decomposes the compound gas using thermal energy generated from the surface of the sample to form a thin film on the surface of the sample. An apparatus for forming
There are cases where it is carried out at normal pressure and cases where it is carried out at reduced pressure or vacuum. The quality of the thin film formed by the CVD device is determined by the film quality and the uniformity of the film thickness distribution, so in order to obtain a good quality thin film, the distribution of the gas supplied, the temperature of the sample, the distribution of heating, etc. must be carefully controlled. need to be monitored and controlled.

従来の試料加熱装置およびCVD装置を第1図、第2図
および第6図について説明する。第1図(試料加熱装&
)において、1は加熱される試料、2はヒータ6を内蔵
する試料台、4はヒータ6の電源である。第2図は第1
図の試料加熱装置を備えた常圧CVD装置で、5は密閉
容器、6Vi密閉容器5に薄膜を形成する組成元素を含
む化合物ガスを供給する供給口である。第3図は第1図
の試料加熱装置を備えた減圧CVD装置で、第2図の密
閉容器5にX窒ポンプ7に連結される排気口8を設けた
構造を有する。
A conventional sample heating apparatus and CVD apparatus will be explained with reference to FIGS. 1, 2, and 6. Figure 1 (sample heating device &
), 1 is a sample to be heated, 2 is a sample stage with a built-in heater 6, and 4 is a power source for the heater 6. Figure 2 is the first
In the atmospheric pressure CVD apparatus equipped with the sample heating device shown in the figure, reference numeral 5 denotes a closed container and a supply port for supplying a compound gas containing constituent elements to form a thin film into the 6Vi closed container 5. FIG. 3 shows a reduced pressure CVD apparatus equipped with the sample heating device shown in FIG. 1, and has a structure in which the closed container 5 shown in FIG. 2 is provided with an exhaust port 8 connected to the X-nitrogen pump 7.

ところで上記第1図の試料加熱装置は、試料1の表面温
度の制御が困難である。特に、表面温度を均一に昇温さ
せ、あるいは表面温度に温度勾配を形成するよう温度制
御することが困難である。これは装置の構造を基く必然
的な欠点でろって、試料1の表面温度の制御が製品の品
質に大きく影響する第2図の常圧CVD装置および第6
図の減圧CVD装置においては看過するととのできない
重要な問題である。本発明は上記のような欠点のない試
料加熱装置並びにと名を備えた常圧CVD装置および減
圧CVD装置を提供することを目的とするものである。
However, in the sample heating apparatus shown in FIG. 1, it is difficult to control the surface temperature of the sample 1. In particular, it is difficult to control the temperature so that the surface temperature is raised uniformly or a temperature gradient is formed in the surface temperature. This is an inevitable drawback based on the structure of the apparatus, and the atmospheric pressure CVD apparatus shown in Fig. 2 and the
This is an important problem that cannot be overlooked in the reduced pressure CVD apparatus shown in the figure. The object of the present invention is to provide a sample heating apparatus, an atmospheric pressure CVD apparatus, and a reduced pressure CVD apparatus having the above-mentioned names.

〔発明の構成〕本発明の試料加熱装置は加熱される試料
を載置する試料台に複数個の窓孔を設け、該窓孔に光フ
ァイバーの先端をそれぞれ挿入し、該光ファイバーの後
端には供給量を任意を制御することのできる赤外光の光
源を設けたことを特徴とするものであシ、本発明の常圧
CVD装置は、試料の表面に形成される薄膜元素を含む
化合物ガスを供給する供給口を備えた密閉容器内に前記
試料加熱装置を設けたものであり、本発明の減圧CVD
装置は前記化合物ガスの供給口と、真空ポンプに連結さ
れる排気口とを備えた密閉容器内に前記試料加熱装置を
設けた構成を有する。
[Structure of the Invention] The sample heating device of the present invention has a plurality of window holes in the sample stage on which the sample to be heated is placed, the tips of optical fibers are inserted into each of the window holes, and the rear end of the optical fiber is provided with a plurality of window holes. The atmospheric pressure CVD apparatus of the present invention is characterized by being equipped with an infrared light source whose supply amount can be arbitrarily controlled. The sample heating device is provided in a closed container equipped with a supply port for supplying the low pressure CVD of the present invention.
The apparatus has a configuration in which the sample heating device is provided in a closed container equipped with a supply port for the compound gas and an exhaust port connected to a vacuum pump.

〔実施例〕第4図は本発明の試料加熱装置の実施例であ
る。11は加熱される試料(例・シリコン板)12を載
置する透明な石英プレートより寿る載置板16を俯えた
試料台で、複数個の窓孔14を崩し、略窓孔14にはそ
れそハ光ファイバー15の先端が挿入されている。16
は光ファイバー15の後端に設けた赤外光の光源である
。上記の構成において複数個の光源16から元ファイバ
ー15を通して供給される赤外光を制御すると試料12
の加熱を部分的々いしは全体的に制御することが可能で
ある。
[Embodiment] FIG. 4 shows an embodiment of the sample heating device of the present invention. Reference numeral 11 denotes a sample stand that looks down on a mounting plate 16 that is longer than a transparent quartz plate on which a heated sample (e.g. silicon plate) 12 is placed. The tip of the optical fiber 15 is inserted therein. 16
is an infrared light source provided at the rear end of the optical fiber 15. In the above configuration, when the infrared light supplied from the plurality of light sources 16 through the original fiber 15 is controlled, the sample 12
It is possible to control the heating locally or completely.

第5図は第4図に試料加熱装置を密閉容器17の内部に
設けた本発明の常圧CVD装置の実施例で、18は形成
される薄膜の組成元素を含む化合物ガスの供給口でるる
。化合物ガスがモノシラン(SZH4)、アンモニア(
lJHj )、窒素(N2)の混合ガスの場合は試料1
2(シリコン板)の表面に窒化シリコン膜(sL、n4
)が形成される。第6図は第5図の密閉容器17に真空
ポンプ20と連結さねる排気口19を設けた本発明の減
圧CVD装置の実施例で、真空ポンプ20を駆動するこ
とによって密閉容器17の内部を真空に近い圧力に減圧
することができる。
FIG. 5 shows an embodiment of the atmospheric pressure CVD apparatus of the present invention in which the sample heating device shown in FIG. 4 is provided inside a closed container 17, and 18 is a supply port for a compound gas containing the constituent elements of the thin film to be formed. . The compound gas is monosilane (SZH4), ammonia (
lJHj ), sample 1 in the case of a mixed gas of nitrogen (N2)
2 (silicon plate) with a silicon nitride film (sL, n4
) is formed. FIG. 6 shows an embodiment of the reduced pressure CVD apparatus of the present invention in which the airtight container 17 shown in FIG. 5 is provided with an exhaust port 19 connected to a vacuum pump 20. The pressure can be reduced to near vacuum.

5発明の効果〕本発明の試料加熱装置の第1の%長は試
料を加熱する熱源(赤外光)を部分的に制御することが
可能であるため、試料の表面温度の分布のバラツキを±
1℃以内に押えることができる点にある。その結果、第
1図の従来の装置においては不可能とされていた表面温
度の均一昇温ないしは表面温度に所定の温度勾配を形成
する温度制御が可能となる。第2の崎長は赤外綜の輻射
熱による加熱であるため、立上9の早いことである。第
1図の従来の装置は試料の表面温度が所定の300℃に
達するのに約6時間を必要とするが、本発明の装置によ
ると10分以内で可能である。本発明の試料加熱装置は
上記のようなすぐtまた特性を有するのでこれを使用す
る第4図の常圧CVD装置および第5図の減圧CvD装
置によって形成される薄膜は膜質がすぐれ、膜厚分布の
バラツキを±14係以内に押えることができ、ピンホー
ルのない良質の薄膜をうろことができる。しかも立上シ
が早いので薄膜形成の時間が短縮れ、良質の薄膜を不す
る基板の生産性を向上するすぐれた効果をイコする。
5 Effects of the Invention] The first percent length of the sample heating device of the present invention is that the heat source (infrared light) for heating the sample can be partially controlled, so variations in the surface temperature distribution of the sample can be reduced. ±
The point is that it can be kept within 1°C. As a result, it becomes possible to uniformly raise the surface temperature or to control the temperature to form a predetermined temperature gradient in the surface temperature, which was impossible in the conventional apparatus shown in FIG. The second heating is due to heating by the radiant heat of the infrared heel, so the start-up 9 is early. The conventional apparatus shown in FIG. 1 requires approximately 6 hours for the surface temperature of the sample to reach the predetermined 300° C., but the apparatus of the present invention can achieve this within 10 minutes. Since the sample heating device of the present invention has the above-mentioned characteristics, the thin films formed by the normal pressure CVD device shown in FIG. 4 and the low pressure CVD device shown in FIG. The variation in distribution can be suppressed to within ±14 factors, and a high-quality thin film without pinholes can be obtained. Moreover, since the start-up is quick, the time for forming a thin film is shortened, which has an excellent effect of improving the productivity of substrates that do not require high-quality thin films.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図:従来の試料加熱装置を示す図 第21ン1:従来の常圧OVD装置を示す図第3し1:
従来の減圧OVD装置を示す図第4回層本発明の試料加
熱装置を示す図第5回層本発明の常圧OVD装餉゛を示
す図第6図:本発明の減圧OVDを示す図 11・・・試料台、12・・・試料、13・・・載置板
、14・・・窓孔、15・・・光ファイバー、16・・
・光源、17・・・密閉容器、18・・・供給口、19
・・・排気口、20・・・真空ポンプ 第4図 第5図
Fig. 1: Diagram showing a conventional sample heating device Fig. 21-1: Fig. 3 showing a conventional atmospheric pressure OVD device Fig. 3-1:
A diagram showing a conventional low pressure OVD apparatus 4th layer A diagram showing a sample heating device of the present invention 5th layer A diagram showing an atmospheric pressure OVD apparatus of the present invention FIG. 6: A diagram showing a low pressure OVD apparatus of the present invention ...sample stand, 12...sample, 13...mounting plate, 14...window hole, 15...optical fiber, 16...
・Light source, 17... Airtight container, 18... Supply port, 19
...Exhaust port, 20...Vacuum pump Fig. 4 Fig. 5

Claims (1)

【特許請求の範囲】 (1)加熱される試料を載置する試料台に複数個の窓孔
を設け、該窓孔に光ファイバーの先端をそね七ね挿入し
、該光ファイバーの後端には供給量を任意に制御するこ
とのできる赤外光の光跡を設けたことを特徴とする試料
加熱装置 (2)加熱さねる試料を載置する試料台に複数個の窓孔
を設け、庭窓孔に光ファイバーの先端をそれぞれ挿入し
、該光ファイバーの後端には供給量を任意に制御するこ
とのできる赤外光の光源を設けた試料加熱装置を、前記
試料の表面に形成される薄膜の組成元素を含む化合物ガ
スを供給する供給口を備えた密閉容器の内部に設けたこ
とを特徴とする常圧OVD装置 (6)加熱される試料を載置する試料台に複数個の窓孔
を設け、該窓孔に光ファイバーの先端をそれぞれ挿入し
、該光ファイバーの後端には供給量を任意に制御するこ
とのできる赤外光の光源を設けた試料加熱装置を、前記
試料の表面に形成される薄膜の組成元素を含む化合物ガ
スを供給する供給口と、真4空ポンプに連結される排気
口とを備えた密閉容器の内部に設けたことを特徴とする
減圧OVD装置
[Claims] (1) A plurality of window holes are provided in the sample stage on which the sample to be heated is placed, and the tip of an optical fiber is inserted seven times into the window hole, and the rear end of the optical fiber is inserted into the window hole. A sample heating device characterized by being provided with an infrared light trail that allows the supply amount to be arbitrarily controlled. The tip of an optical fiber is inserted into each window hole, and a sample heating device, which is equipped with an infrared light source whose supply amount can be arbitrarily controlled, is installed at the rear end of the optical fiber. An atmospheric pressure OVD apparatus characterized in that it is provided inside a closed container equipped with a supply port for supplying a compound gas containing a compositional element (6) A plurality of window holes in a sample stage on which a sample to be heated is placed. The tip of an optical fiber is inserted into each of the window holes, and a sample heating device, which is equipped with an infrared light source whose supply amount can be arbitrarily controlled, is attached to the surface of the sample at the rear end of the optical fiber. A reduced-pressure OVD device, characterized in that it is provided inside a closed container, which is equipped with a supply port for supplying a compound gas containing the constituent elements of the thin film to be formed, and an exhaust port connected to a vacuum pump.
JP23528783A 1983-12-14 1983-12-14 Sample heating device, atmospheric pressure CVD device and reduced pressure CVD device Expired - Lifetime JPH069187B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP23528783A JPH069187B2 (en) 1983-12-14 1983-12-14 Sample heating device, atmospheric pressure CVD device and reduced pressure CVD device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP23528783A JPH069187B2 (en) 1983-12-14 1983-12-14 Sample heating device, atmospheric pressure CVD device and reduced pressure CVD device

Publications (2)

Publication Number Publication Date
JPS60126821A true JPS60126821A (en) 1985-07-06
JPH069187B2 JPH069187B2 (en) 1994-02-02

Family

ID=16983870

Family Applications (1)

Application Number Title Priority Date Filing Date
JP23528783A Expired - Lifetime JPH069187B2 (en) 1983-12-14 1983-12-14 Sample heating device, atmospheric pressure CVD device and reduced pressure CVD device

Country Status (1)

Country Link
JP (1) JPH069187B2 (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1995028002A1 (en) * 1994-04-08 1995-10-19 Hitachi, Ltd. Method and device for processing semiconductor wafer
CN106463402A (en) * 2014-06-09 2017-02-22 应用材料公司 Substrate temperature control apparatus including optical fiber heating, substrate temperature control systems, electronic device processing systems, and methods
JP2017108155A (en) * 2009-08-12 2017-06-15 ジョージア ステート ユニバーシティ リサーチ ファウンデーション,インコーポレイテッド High pressure chemical vapor deposition apparatuses and methods, and compositions produced therewith
CN109560035A (en) * 2013-09-06 2019-04-02 应用材料公司 Support component and semiconductor processing system
CN110211902A (en) * 2019-06-19 2019-09-06 北京北方华创微电子装备有限公司 Bogey and processing chamber

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9986598B2 (en) * 2014-07-02 2018-05-29 Applied Materials, Inc. Temperature control apparatus including groove-routed optical fiber heating, substrate temperature control systems, electronic device processing systems, and processing methods

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1995028002A1 (en) * 1994-04-08 1995-10-19 Hitachi, Ltd. Method and device for processing semiconductor wafer
JP2017108155A (en) * 2009-08-12 2017-06-15 ジョージア ステート ユニバーシティ リサーチ ファウンデーション,インコーポレイテッド High pressure chemical vapor deposition apparatuses and methods, and compositions produced therewith
CN109560035A (en) * 2013-09-06 2019-04-02 应用材料公司 Support component and semiconductor processing system
CN106463402A (en) * 2014-06-09 2017-02-22 应用材料公司 Substrate temperature control apparatus including optical fiber heating, substrate temperature control systems, electronic device processing systems, and methods
JP2017527980A (en) * 2014-06-09 2017-09-21 アプライド マテリアルズ インコーポレイテッドApplied Materials,Incorporated Substrate temperature control apparatus including optical fiber heating, substrate temperature control system, electronic device processing system and method
CN110211902A (en) * 2019-06-19 2019-09-06 北京北方华创微电子装备有限公司 Bogey and processing chamber
CN110211902B (en) * 2019-06-19 2021-08-13 北京北方华创微电子装备有限公司 Bearing device and process chamber

Also Published As

Publication number Publication date
JPH069187B2 (en) 1994-02-02

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