JPS5933231A - Apparatus for extracting chlorophyll - Google Patents

Abstract

PURPOSE:To provide the titled apparatus capable of extracting chlorophyll safely, in high purity, by using a raw material compounding tank to compound the raw material containing chlorophyll with an alcohol solvent, a circulation pipe and pump for circulating said raw material, and an ultrasonic extraction tank inserted in the middle of said pipe. CONSTITUTION:The circulation pump 2 is connected to the raw material compounding tank 1 for the compounding of a raw material containing chlorophyll (e.g. extrement of silkworm) with an alcohol solvent. The ultrasonic extraction tank is attached to the pump 2, and the extraction tank is connected with the raw material compounding tank 1 through the circulation pipe 5. The ultrasonic extraction tank 4 is composed of a central large-diameter pipe 4A, the upper and lower tapered pipes 4B, and the liquid inlet 4C and the liquid outlet 4D connected to the contracted openings of the tapered pipes. Ultrasonic vibrators 8 each having ultrasonic radiation faces at both ends are placed in the large- diameter pipe 4A parallel to the axis of the tube directing the ultrasonic radiation faces toward the tapered pipes. The taper of the tapered pipe is selected to focus the ultrasonic radiation at the liquid inlet 4C and the liquid outlet 4D by the total reflection of the radiation with the tapered face.

Description

DETAILED DESCRIPTION OF THE INVENTION The present invention relates to an apparatus for extracting chlorophyll from silkworms, seaweed, etc. at room temperature using superconvex waves.
Ru.

Natural chlorophyll is one of the beneficial medical products for human tissue cells, promoting the growth of germ cells, activating the revival of fJI cells, and treating disorders in various organs of the human body: C, two vs. U7
Increases resistance and applies l+ to human tissue! Lie the power” (
It has strong bactericidal, detoxifying, and energizing effects, and is especially effective against diabetes, hypertension, anemia, gastric ulcers, intestinal ulcers, etc.
It is known that there is.

The conventional method for extracting chlorophyll is to immerse the leaves and stems of plants in organic solvents such as ammonium, hydrochloric acid, etc. that are harmful to the human body, and then extract the chlorophyll using the general extraction method. Dispose of own machine 〆111 on 1&! However, there are problems in that it is difficult to completely remove the self-harmful organic solvent, and it is also difficult to obtain highly pure chlorophyll.

The present invention is aimed at solving these problems, and does not use harmful solvents.

Extract chlorophyll by ultrasound without using 1.:1'lA? 3 activities: 1 (6 things in common).

Hereinafter, the 4' light will be explained based on an example without being shown in the drawings.

Figure 1 shows the steps of the leaf element extraction method according to the present invention.
゛Culm diagram, Fig. 2 G, 1 C which does not show the embodiment device of the present invention
2) Mix raw materials such as silkworm food and ethyl alcohol.
7 and 11 people can sit in the raw material mixing tank + 11! Connect the i-ring pump (2) 1, and attach the ultrasonic extraction tank (4) to the circulation pump (2). A cooling device (6) is connected to the ultrasonic extraction tank (4) with a circulation valve (5), and a cooling device (0) is connected to the ultrasonic extraction tank (4).
is the connecting slot with the raw material blending tank (1). As shown in Figures 3 and 4, the ultrasonic extraction tank
A), the upper and lower tapered pipe parts (4B), and each tapered pipe part (
4B) is connected to the small i, \l' l at the end of the pipe (4C) and the liquid outlet pipe part (41'), and the large diameter pipe part (4A) has one part of both pipes. The ultrasonic wave 1 radiator (8), whose output width is the ultra-convex wave, is directed along the axial direction of the tube, and the output direction of the ultrasonic wave is directed toward the tapered surface of the tapered tube section (4B) indicated by -l-. Arrange multiple pieces using all metal fittings 9). The oscillation output from the ultrasonic oscillator (3) is applied to each ultrasonic transducer (8). By configuring the ultrasonic extraction tank (4) like this-4, the ultrasonic extraction tank (4) is The ultrasonic wave (11) output from both sides of the 'S'' wave vibration (1a) is transmitted to the tapered tube part (
41 () is totally reflected at the Theno ζ plane 1+, and is focused at the input pipe part (4C) and the output part (41)), so in this, (10 ) In the direction of the arrow indicated by C; when the oligoliquid is passed through the inlet, the introduction of the gamma 1 wave extraction tank (4)
When passing through the raw material 1, the chlorophyll in the raw material 1 is exposed to the powerful ultrasonic waves 1
↓i attack wave and sky N, 11 phenomena (ki~l, hif 11stion)
mechanical destruction, decomposition, dispersion,
Due to the micronization action, the 4JI woven bonding chains and cell membranes of the silkworms are destroyed, the chlorophyll is separated from the cellulose and protein, and the chlorophyll is extracted into the refrigerant in 11 minutes. Things happen.

Chlorophyll extractor configured like this:? 7, purity of 1 (°
In order to extract the dark chlorophyll within a short time, we use 2 as a solvent.
with a purity of 94% or higher (without using I-L)
.

Put the selected silkworms or seaweeds and ethyl alcohol into the raw material mixing tank (1) from raw material input 11 (7+), and pump it with the pump (2) connected to raw material mixing 41!!1 (!). Send the sound wave to the sonic extraction tank (4).
The ultrasonic wave emitted from the ultrasonic vibration f(1) which forms a surface at both ends/it beam is the ultrasonic wave installed on the two blade surfaces of the transducer. The ultrasonic wave is reflected by the tapered surface of the tapered pipe part (413) of the extraction tank (4) and enters the L part of the extraction tank f, 11 and the tapered pipe part (4B) of the part 1.
It is focused at the part where the 2nd part (=I (: ) III liquid pipe part (41)) connects.

At this time, a cooling tank (6) was installed to prevent the ultrasonic shock and cavitation phenomenon from converting into thermal energy. ', C was kept at room temperature.

In addition, the cooling tank (6) was connected to the raw material mixing tank (11) to simultaneously circulate the solution and raw materials.
When the leaf f31 element separated from the buccal tissue of the σ algae is passed through the device into the iII+7 ring, Il:! $1 and raw materials 14
It is extracted into the solvent by 1 stroke and 141 stroke with the impeller of a pump, etc.

After the predetermined circulation of the cycle has been completed and most of the chlorophyll has been extracted from the raw material, the solution from which the chlorophyll has been extracted is filtered to separate the lees, which are dried and used as feed feed 1. The solution is separated from the alcohol in a vacuum concentrator to obtain pure A-leaf 1.
4. The meme is f4I, and the word is C).

As mentioned above, mix the unexploded IM RoJ and the confectionery element 1 [1'l of white sugar raw material and the alcohol solvent C; Circulate profits bihli
Ring Pa ``zo) Q and circulation bonfu look, the same 1 shield ring pa ``pu 1 = J tun:, l;
I felt angry. ! A! Green extraction equipment: ゛, and the ultrasonic extraction tank has a central human diameter section, +1 "I-" taper tube section, and each taper tube section has a small f, \:l':I The human wave pipe section and the liquid output pipe section connected to the large diameter pipe section are ωh, and the ultra i'nu vibration 1', which is a plane (both ends of which are ultrasonic transducers), is applied to the large diameter pipe section in the axial direction of the tube. along the same line, and so that the direction in which the ultrasonic waves are emitted is oriented toward the tapered surface of the tapered tube section described in 1.k.

The structure is as follows. Therefore, it produces the effect as described in f.

■ Each time 1°ζ of focused ultrasonic waves is used, one cell of J, Rihara O'1 is destroyed and chlorophyll can be extracted at room temperature.

■By circulating the raw materials, pure +rli eastern green pigment can be extracted.

■ N Yong Qi Q,! : Ethylalnylene has a history of 64 times and 11 days of harm to the human body.

[Brief explanation of drawings]

FIG. 1 shows the present invention: 1. ? ",! A1. The extraction frame of J element is used in Bo 41', culm diagram, Fig. 2 (51 The structure of the embodiment of the present invention is not shown; An example of an ultrasonic extraction tank is shown below,
Figure 4 is a diagram of 2j bar J Otsu 1υi on the I l line of Figure 3. +11: i Small blending tank (2): 1 ring pump) 2 ultra high wave generator +41: Ultrasonic extraction tank (5): Circulating vizo (6): Cooling device Figure 1 Figure 2 Figure 2 3 diagrams

Claims (1)

[Scope of Claims] 1. A second blending tank in which the raw material for turning chlorophyll into gold and an alcohol solvent are mixed, and the raw material in the raw material blending tank is circulated through the mouth. The IJ vibe, the circulation pump, and the ultrasonic extraction tank installed in the middle of the same circulation path and f-zo are α11 and IS leaf 1. , I unextracted device. 2. Ultrasonic extraction tank (J) equipped with a central large-diameter pipe section, upper and lower Taber pipe sections, and a human wave pipe section and an ejecting pipe section connected to the small-diameter "1" of each Taber pipe section. Both ends of the large-diameter tube part are arranged so that the ultrasonic wave IM', which is the ultrasonic output end mi, is along the axial direction of the movable metal tube, and the output direction of the ultrasonic wave is directed toward the tapered surface of the tipper i section. of the Taber tube section so that the ultrasonic waves output from both ends of the ultrasonic transducer are totally reflected on the tapered surface of the Taber tube section and focused in the human wave tube section and the liquid output tube section. The chlorophyll extraction device according to claim 1, characterized in that the slope of the tapered surface is set.