JPS5920233A - １，２−ジクロルエタンの製法 - Google Patents
１，２−ジクロルエタンの製法Info
- Publication number
- JPS5920233A JPS5920233A JP58115309A JP11530983A JPS5920233A JP S5920233 A JPS5920233 A JP S5920233A JP 58115309 A JP58115309 A JP 58115309A JP 11530983 A JP11530983 A JP 11530983A JP S5920233 A JPS5920233 A JP S5920233A
- Authority
- JP
- Japan
- Prior art keywords
- ethylene
- gas
- waste gas
- acetaldehyde
- dichloroethane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 title claims description 20
- 238000004519 manufacturing process Methods 0.000 title description 8
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 claims description 58
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 48
- 239000005977 Ethylene Substances 0.000 claims description 48
- 239000002912 waste gas Substances 0.000 claims description 40
- 239000007789 gas Substances 0.000 claims description 34
- 238000000034 method Methods 0.000 claims description 29
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 26
- 229910052760 oxygen Inorganic materials 0.000 claims description 26
- 239000001301 oxygen Substances 0.000 claims description 26
- 238000006243 chemical reaction Methods 0.000 claims description 24
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 20
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- 229910052757 nitrogen Inorganic materials 0.000 claims description 11
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 10
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 10
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 10
- 239000003054 catalyst Substances 0.000 claims description 8
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 8
- 230000003197 catalytic effect Effects 0.000 claims description 7
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims description 6
- 238000003860 storage Methods 0.000 claims description 6
- 229910052786 argon Inorganic materials 0.000 claims description 5
- 238000007872 degassing Methods 0.000 claims description 5
- 238000012432 intermediate storage Methods 0.000 claims description 5
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims description 2
- 239000012495 reaction gas Substances 0.000 claims description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 1
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 229910002092 carbon dioxide Inorganic materials 0.000 description 7
- 239000001569 carbon dioxide Substances 0.000 description 6
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 6
- 238000007792 addition Methods 0.000 description 4
- 239000011261 inert gas Substances 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000006227 byproduct Substances 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- SCYULBFZEHDVBN-UHFFFAOYSA-N 1,1-Dichloroethane Chemical compound CC(Cl)Cl SCYULBFZEHDVBN-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 2
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 description 2
- 239000003570 air Substances 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 239000002841 Lewis acid Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- HRYZWHHZPQKTII-UHFFFAOYSA-N chloroethane Chemical compound CCCl HRYZWHHZPQKTII-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 150000001879 copper Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- MKDSZDXMLSNRDV-UHFFFAOYSA-N ethene;gold Chemical compound [Au].C=C MKDSZDXMLSNRDV-UHFFFAOYSA-N 0.000 description 1
- 229960003750 ethyl chloride Drugs 0.000 description 1
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- -1 ethylene, ethylene Chemical group 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 150000007517 lewis acids Chemical class 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/15—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination
- C07C17/152—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons
- C07C17/156—Preparation of halogenated hydrocarbons by replacement by halogens with oxygen as auxiliary reagent, e.g. oxychlorination of hydrocarbons of unsaturated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19823226042 DE3226042A1 (de) | 1982-07-12 | 1982-07-12 | Verfahren zur herstellung von 1,2-dichlorethan |
| DE32260423 | 1982-07-12 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS5920233A true JPS5920233A (ja) | 1984-02-01 |
Family
ID=6168261
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58115309A Pending JPS5920233A (ja) | 1982-07-12 | 1983-06-28 | １，２−ジクロルエタンの製法 |
Country Status (6)
| Country | Link |
|---|---|
| JP (1) | JPS5920233A (enrdf_load_stackoverflow) |
| AU (1) | AU555622B2 (enrdf_load_stackoverflow) |
| CA (1) | CA1201729A (enrdf_load_stackoverflow) |
| DE (1) | DE3226042A1 (enrdf_load_stackoverflow) |
| IT (1) | IT1172398B (enrdf_load_stackoverflow) |
| MX (1) | MX161306A (enrdf_load_stackoverflow) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4946357A (en) * | 1989-10-30 | 1990-08-07 | James Harrison | Diverter chute assembly for molding machine |
| JP2009275014A (ja) * | 2008-05-16 | 2009-11-26 | Tosoh Corp | １，２−ジクロロエタンの製造方法 |
| JP2011513270A (ja) * | 2008-02-28 | 2011-04-28 | ソルベイ（ソシエテ アノニム） | 少なくとも１つのエチレン誘導体化合物の製造方法 |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2096095A1 (en) * | 2008-02-28 | 2009-09-02 | SOLVAY (Société Anonyme) | Process for the manufacture of at least one ethylene derivative compound |
| EP2130814A1 (en) * | 2008-06-03 | 2009-12-09 | SOLVAY (Société Anonyme) | Process for the manufacture of at least one ethylene derivative compound |
| EA201290428A1 (ru) * | 2009-12-03 | 2013-01-30 | Солвей Са | Способ получения по меньшей мере одного производного соединения этилена |
| EA024187B1 (ru) * | 2009-12-03 | 2016-08-31 | Солвей Са | Способ получения по меньшей мере одного производного этилена |
| DE102011108211A1 (de) | 2011-07-21 | 2013-01-24 | Thyssenkrupp Uhde Gmbh | Verfahren zum Konzentrieren wässriger Lauge und dafür geeignete Vorrichtung |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0053335A1 (de) * | 1980-11-28 | 1982-06-09 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von 1,2-Dichlorethan |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2603477C3 (de) * | 1976-01-30 | 1983-02-03 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Entfernung von Verunreinigungen aus durch Oxychlorierung gewonnenem 1,2-Dichloräthan |
| DE2733502C3 (de) * | 1977-07-25 | 1980-09-25 | Wacker-Chemie Gmbh, 8000 Muenchen | Verfahren zur Herstellung von 1,2-Dichloräthan aus Äthylen enthaltenden Restgasen, die aus einer Oxychlorierung stammen |
| US4151212A (en) * | 1978-07-07 | 1979-04-24 | Ppg Industries, Inc. | Purification of ethylene dichloride |
-
1982
- 1982-07-12 DE DE19823226042 patent/DE3226042A1/de active Granted
-
1983
- 1983-06-03 CA CA000429652A patent/CA1201729A/en not_active Expired
- 1983-06-20 IT IT48537/83A patent/IT1172398B/it active
- 1983-06-28 JP JP58115309A patent/JPS5920233A/ja active Pending
- 1983-07-11 AU AU16729/83A patent/AU555622B2/en not_active Ceased
- 1983-07-11 MX MX197990A patent/MX161306A/es unknown
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0053335A1 (de) * | 1980-11-28 | 1982-06-09 | Hoechst Aktiengesellschaft | Verfahren zur Herstellung von 1,2-Dichlorethan |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4946357A (en) * | 1989-10-30 | 1990-08-07 | James Harrison | Diverter chute assembly for molding machine |
| JP2011513270A (ja) * | 2008-02-28 | 2011-04-28 | ソルベイ（ソシエテ アノニム） | 少なくとも１つのエチレン誘導体化合物の製造方法 |
| JP2009275014A (ja) * | 2008-05-16 | 2009-11-26 | Tosoh Corp | １，２−ジクロロエタンの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| AU1672983A (en) | 1984-01-19 |
| IT8348537A0 (it) | 1983-06-20 |
| DE3226042C2 (enrdf_load_stackoverflow) | 1990-11-22 |
| CA1201729A (en) | 1986-03-11 |
| DE3226042A1 (de) | 1984-01-12 |
| AU555622B2 (en) | 1986-10-02 |
| MX161306A (es) | 1990-09-05 |
| IT1172398B (it) | 1987-06-18 |
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