JPS5884103A - 過酸化水素の製造方法 - Google Patents
過酸化水素の製造方法Info
- Publication number
- JPS5884103A JPS5884103A JP57185892A JP18589282A JPS5884103A JP S5884103 A JPS5884103 A JP S5884103A JP 57185892 A JP57185892 A JP 57185892A JP 18589282 A JP18589282 A JP 18589282A JP S5884103 A JPS5884103 A JP S5884103A
- Authority
- JP
- Japan
- Prior art keywords
- gas
- working
- anthraquinone
- hydrogen peroxide
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 7
- 239000007789 gas Substances 0.000 claims abstract description 47
- 238000000034 method Methods 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 150000004056 anthraquinones Chemical class 0.000 claims abstract description 14
- 239000000203 mixture Substances 0.000 claims abstract description 13
- 239000007788 liquid Substances 0.000 claims description 27
- RZVHIXYEVGDQDX-UHFFFAOYSA-N 9,10-anthraquinone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3C(=O)C2=C1 RZVHIXYEVGDQDX-UHFFFAOYSA-N 0.000 claims description 3
- 238000005984 hydrogenation reaction Methods 0.000 abstract description 13
- 239000012224 working solution Substances 0.000 abstract description 8
- 230000003647 oxidation Effects 0.000 abstract description 5
- 238000007254 oxidation reaction Methods 0.000 abstract description 5
- 239000008246 gaseous mixture Substances 0.000 abstract 1
- 239000012530 fluid Substances 0.000 description 20
- 238000001035 drying Methods 0.000 description 15
- 239000002904 solvent Substances 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 4
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 229910001882 dioxygen Inorganic materials 0.000 description 3
- PCFMUWBCZZUMRX-UHFFFAOYSA-N 9,10-Dihydroxyanthracene Chemical class C1=CC=C2C(O)=C(C=CC=C3)C3=C(O)C2=C1 PCFMUWBCZZUMRX-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000011049 pearl Substances 0.000 description 2
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- YEVQZPWSVWZAOB-UHFFFAOYSA-N 2-(bromomethyl)-1-iodo-4-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC=C(I)C(CBr)=C1 YEVQZPWSVWZAOB-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 102100021102 Hyaluronidase PH-20 Human genes 0.000 description 1
- 101150055528 SPAM1 gene Proteins 0.000 description 1
- 241000583234 Suisha Species 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- -1 aliphatic secondary alcohols Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000003795 desorption Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229910052573 porcelain Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
- C01B21/093—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms containing also one or more sulfur atoms
- C01B21/096—Amidosulfonic acid; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Luminescent Compositions (AREA)
- Ultra Sonic Daignosis Equipment (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE8106244-0 | 1981-10-22 | ||
| SE8106244A SE425079B (sv) | 1981-10-22 | 1981-10-22 | Forfarande for framstellning av veteperoxid genom antrakinonprocessen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5884103A true JPS5884103A (ja) | 1983-05-20 |
| JPS6251203B2 JPS6251203B2 (enExample) | 1987-10-29 |
Family
ID=20344855
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57185892A Granted JPS5884103A (ja) | 1981-10-22 | 1982-10-22 | 過酸化水素の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4503028A (enExample) |
| EP (1) | EP0078780B1 (enExample) |
| JP (1) | JPS5884103A (enExample) |
| AT (1) | ATE18534T1 (enExample) |
| CA (1) | CA1203670A (enExample) |
| DE (1) | DE3269859D1 (enExample) |
| FI (1) | FI67352C (enExample) |
| NO (1) | NO158614C (enExample) |
| SE (1) | SE425079B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2024505326A (ja) * | 2021-11-08 | 2024-02-06 | 南京延長反応技術研究院有限公司 | アントラキノン法による過酸化水素製造の酸化反応系におけるマイクロバブル強化の評価方法 |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6342196B2 (en) | 1998-06-29 | 2002-01-29 | University Of Pittsburgh | Synthesis of hydrogen peroxide |
| FR2788052B1 (fr) * | 1998-12-31 | 2001-04-06 | Krebs Speichim | Prparation de peroxyde d'hydrogene par un procede cyclique a l'anthraquinone ameliore |
| WO2000066489A1 (en) * | 1999-04-29 | 2000-11-09 | University Of Pittsburgh | Synthesis of hydrogen peroxide |
| DE10207407A1 (de) * | 2002-02-21 | 2003-09-04 | Degussa | Verfahren zur Herstellung von Wasserstoffperoxid |
| EP1350761A1 (de) | 2002-03-28 | 2003-10-08 | Degussa AG | Verfahren zur Herstellung von Wasserstoffperoxid |
| US7722847B2 (en) * | 2002-09-30 | 2010-05-25 | Evonik Degussa Gmbh | Aqueous hydrogen peroxide solutions and method of making same |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US763387A (en) * | 1903-02-09 | 1904-06-28 | Eldred P Dickinson | Method of drying materials. |
| DE411801C (de) * | 1922-01-04 | 1925-04-04 | Adolf Schneider Dr Ing | Verfahren und Vorrichtung zum Eindampfen von Fluessigkeiten |
| US1833717A (en) * | 1927-01-13 | 1931-11-24 | Heat Treating Company | Purification and concentration of liquids |
| FR675258A (fr) * | 1928-05-18 | 1930-02-07 | Industrikemiska Ab | Procédé et dispositif d'évaporation |
| US1854385A (en) * | 1928-10-27 | 1932-04-19 | Schaack Bros Chemical Works In | Process of drying organic liquids |
| US1996852A (en) * | 1932-02-06 | 1935-04-09 | Bergell Clemens | Process and apparatus for distilling or expelling volatile constituents from liquids |
| US2867507A (en) * | 1958-05-08 | 1959-01-06 | Du Pont | Hydrogenation of alkylanthraquinones |
| US3111460A (en) * | 1960-10-31 | 1963-11-19 | Phillips Petroleum Co | Method of and apparatus for controlling a fluid separation process |
| US3326778A (en) * | 1962-12-27 | 1967-06-20 | Arthur E Mock | Direct contact flash distillation with air and steam |
| US3330625A (en) * | 1963-10-22 | 1967-07-11 | Pittsburgh Plate Glass Co | Hydrogen peroxide manufacture |
| US3345272A (en) * | 1965-05-14 | 1967-10-03 | Richard A Collins | Multiple effect purification of contaminated fluids by direct gaseous flow contact |
| US3409515A (en) * | 1966-03-30 | 1968-11-05 | Artisan Ind | Method of stripping volatile constituents from a mixture |
| DE2042522C3 (de) * | 1970-08-27 | 1979-01-25 | Deutsche Gold- U. Silber-Scheideanstalt, Vormals Roessler, 6000 Frankfurt | Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen |
-
1981
- 1981-10-22 SE SE8106244A patent/SE425079B/sv not_active IP Right Cessation
-
1982
- 1982-09-29 US US06/428,435 patent/US4503028A/en not_active Expired - Lifetime
- 1982-10-12 AT AT82850197T patent/ATE18534T1/de not_active IP Right Cessation
- 1982-10-12 CA CA000413240A patent/CA1203670A/en not_active Expired
- 1982-10-12 DE DE8282850197T patent/DE3269859D1/de not_active Expired
- 1982-10-12 EP EP82850197A patent/EP0078780B1/en not_active Expired
- 1982-10-18 FI FI823549A patent/FI67352C/fi not_active IP Right Cessation
- 1982-10-21 NO NO823505A patent/NO158614C/no not_active IP Right Cessation
- 1982-10-22 JP JP57185892A patent/JPS5884103A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2024505326A (ja) * | 2021-11-08 | 2024-02-06 | 南京延長反応技術研究院有限公司 | アントラキノン法による過酸化水素製造の酸化反応系におけるマイクロバブル強化の評価方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3269859D1 (en) | 1986-04-17 |
| JPS6251203B2 (enExample) | 1987-10-29 |
| FI823549L (fi) | 1983-04-23 |
| FI823549A0 (fi) | 1982-10-18 |
| CA1203670A (en) | 1986-04-29 |
| US4503028A (en) | 1985-03-05 |
| ATE18534T1 (de) | 1986-03-15 |
| SE425079B (sv) | 1982-08-30 |
| NO158614C (no) | 1988-10-12 |
| NO158614B (no) | 1988-07-04 |
| EP0078780A1 (en) | 1983-05-11 |
| FI67352B (fi) | 1984-11-30 |
| NO823505L (no) | 1983-04-25 |
| EP0078780B1 (en) | 1986-03-12 |
| FI67352C (fi) | 1985-03-11 |
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