JPS58215488A - 酸素および有機硫黄化合物を含むガスの水素化脱硫方法 - Google Patents
酸素および有機硫黄化合物を含むガスの水素化脱硫方法Info
- Publication number
- JPS58215488A JPS58215488A JP58093340A JP9334083A JPS58215488A JP S58215488 A JPS58215488 A JP S58215488A JP 58093340 A JP58093340 A JP 58093340A JP 9334083 A JP9334083 A JP 9334083A JP S58215488 A JPS58215488 A JP S58215488A
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- gas
- hydrogen
- organic sulfur
- alumina
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007789 gas Substances 0.000 title claims description 28
- 150000002898 organic sulfur compounds Chemical class 0.000 title claims description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims description 11
- 229910052760 oxygen Inorganic materials 0.000 title claims description 11
- 239000001301 oxygen Substances 0.000 title claims description 11
- 238000006477 desulfuration reaction Methods 0.000 title description 3
- 230000023556 desulfurization Effects 0.000 title description 3
- 239000003054 catalyst Substances 0.000 claims description 45
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 30
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 17
- 238000000034 method Methods 0.000 claims description 17
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 16
- 239000001257 hydrogen Substances 0.000 claims description 16
- 229910052739 hydrogen Inorganic materials 0.000 claims description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 14
- 229910052763 palladium Inorganic materials 0.000 claims description 14
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 13
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 12
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 11
- 239000011733 molybdenum Substances 0.000 claims description 11
- 229910052750 molybdenum Inorganic materials 0.000 claims description 11
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 8
- 229910052759 nickel Inorganic materials 0.000 claims description 8
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 7
- 239000000377 silicon dioxide Substances 0.000 claims description 7
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims description 6
- 229910017052 cobalt Inorganic materials 0.000 claims description 5
- 239000010941 cobalt Substances 0.000 claims description 5
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 5
- 229910052717 sulfur Inorganic materials 0.000 claims description 5
- 239000011593 sulfur Substances 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 6
- 150000002430 hydrocarbons Chemical group 0.000 description 4
- 239000003345 natural gas Substances 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 150000003464 sulfur compounds Chemical class 0.000 description 3
- RAOIDOHSFRTOEL-UHFFFAOYSA-N tetrahydrothiophene Chemical compound C1CCSC1 RAOIDOHSFRTOEL-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- CETBSQOFQKLHHZ-UHFFFAOYSA-N Diethyl disulfide Chemical compound CCSSCC CETBSQOFQKLHHZ-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- WQAQPCDUOCURKW-UHFFFAOYSA-N butanethiol Chemical compound CCCCS WQAQPCDUOCURKW-UHFFFAOYSA-N 0.000 description 2
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- WQOXQRCZOLPYPM-UHFFFAOYSA-N dimethyl disulfide Chemical compound CSSC WQOXQRCZOLPYPM-UHFFFAOYSA-N 0.000 description 2
- ALVPFGSHPUPROW-UHFFFAOYSA-N dipropyl disulfide Chemical compound CCCSSCCC ALVPFGSHPUPROW-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 238000005470 impregnation Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000002941 palladium compounds Chemical class 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- SUVIGLJNEAMWEG-UHFFFAOYSA-N propane-1-thiol Chemical compound CCCS SUVIGLJNEAMWEG-UHFFFAOYSA-N 0.000 description 2
- 230000000717 retained effect Effects 0.000 description 2
- 150000003568 thioethers Chemical class 0.000 description 2
- LDVVMCZRFWMZSG-OLQVQODUSA-N (3ar,7as)-2-(trichloromethylsulfanyl)-3a,4,7,7a-tetrahydroisoindole-1,3-dione Chemical compound C1C=CC[C@H]2C(=O)N(SC(Cl)(Cl)Cl)C(=O)[C@H]21 LDVVMCZRFWMZSG-OLQVQODUSA-N 0.000 description 1
- 238000004438 BET method Methods 0.000 description 1
- -1 C08SC82 Chemical class 0.000 description 1
- 239000005745 Captan Substances 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- HTIRHQRTDBPHNZ-UHFFFAOYSA-N Dibutyl sulfide Chemical compound CCCCSCCCC HTIRHQRTDBPHNZ-UHFFFAOYSA-N 0.000 description 1
- BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 description 1
- QMMFVYPAHWMCMS-UHFFFAOYSA-N Dimethyl sulfide Chemical compound CSC QMMFVYPAHWMCMS-UHFFFAOYSA-N 0.000 description 1
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 1
- 229910003294 NiMo Inorganic materials 0.000 description 1
- 101100369567 Nicotiana tabacum THT10 gene Proteins 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 150000004645 aluminates Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000010426 asphalt Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 229940117949 captan Drugs 0.000 description 1
- 238000004517 catalytic hydrocracking Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- WHDPTDWLEKQKKX-UHFFFAOYSA-N cobalt molybdenum Chemical compound [Co].[Co].[Mo] WHDPTDWLEKQKKX-UHFFFAOYSA-N 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- LJSQFQKUNVCTIA-UHFFFAOYSA-N diethyl sulfide Chemical compound CCSCC LJSQFQKUNVCTIA-UHFFFAOYSA-N 0.000 description 1
- 150000002019 disulfides Chemical class 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- DDTIGTPWGISMKL-UHFFFAOYSA-N molybdenum nickel Chemical compound [Ni].[Mo] DDTIGTPWGISMKL-UHFFFAOYSA-N 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- GPNDARIEYHPYAY-UHFFFAOYSA-N palladium(ii) nitrate Chemical compound [Pd+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O GPNDARIEYHPYAY-UHFFFAOYSA-N 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000000629 steam reforming Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C7/00—Purification; Separation; Use of additives
- C07C7/148—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound
- C07C7/163—Purification; Separation; Use of additives by treatment giving rise to a chemical modification of at least one compound by hydrogenation
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Catalysts (AREA)
- Exhaust Gas Treatment By Means Of Catalyst (AREA)
- Industrial Gases (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR8209210 | 1982-05-25 | ||
| FR8209210A FR2527473A1 (fr) | 1982-05-25 | 1982-05-25 | Procede pour l'hydrodesulfuration d'un gaz contenant de l'oxygene et des composes organiques du soufre |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS58215488A true JPS58215488A (ja) | 1983-12-14 |
Family
ID=9274380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58093340A Pending JPS58215488A (ja) | 1982-05-25 | 1983-05-25 | 酸素および有機硫黄化合物を含むガスの水素化脱硫方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US4505880A (enExample) |
| EP (1) | EP0095395B1 (enExample) |
| JP (1) | JPS58215488A (enExample) |
| CA (1) | CA1192023A (enExample) |
| DE (1) | DE3361056D1 (enExample) |
| FR (1) | FR2527473A1 (enExample) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5502606A (en) * | 1992-07-17 | 1996-03-26 | Mitsubishi Denki Kabushiki Kaisha | Rotary magnetic head device having plural magnetic heads which are independently movable |
| JP2010180197A (ja) * | 2008-08-27 | 2010-08-19 | Kobelco Eco-Solutions Co Ltd | 消化ガスの脱酸素方法及び装置 |
| JP2013538880A (ja) * | 2010-07-15 | 2013-10-17 | クアドロジェン・パワー・システムズ・インコーポレイテッド | 水、シロキサン、硫黄、酸素、塩化物、揮発性有機化合物を除去するための統合型バイオガス浄化システム |
| JP2019529306A (ja) * | 2016-09-01 | 2019-10-17 | ティッセンクルップ インダストリアル ソリューションズ アクツィエンゲゼルシャフトＴｈｙｓｓｅｎＫｒｕｐｐ Ｉｎｄｕｓｔｒｉａｌ Ｓｏｌｕｔｉｏｎｓ ＡＧ | 水素富化ガスから有機硫黄化合物を除去するための方法および装置 |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6140807A (ja) * | 1984-08-03 | 1986-02-27 | Hitachi Ltd | アルゴンガスの精製方法および装置 |
| US4892717A (en) * | 1985-07-31 | 1990-01-09 | Union Oil Company Of California | Gas treating process |
| DE3534709C1 (en) * | 1985-09-28 | 1987-04-02 | Ruetgerswerke Ag | Process for obtaining heterocycle-free aromatic compounds |
| KR960010082B1 (ko) * | 1988-09-26 | 1996-07-25 | 니혼 파이오닉스 가부시끼가이샤 | 기체성 수소화물의 정제방법 |
| US5849256A (en) * | 1996-04-26 | 1998-12-15 | Engelhard Corporation | Method for oxidizing carbon monoxide in a gas stream containing oxidizable sulphur compounds |
| AU2005305204B2 (en) * | 2004-11-09 | 2010-04-22 | Fluor Technologies Corporation | Configurations and methods for SOx removal in oxygen-containing gases |
| RU2402515C1 (ru) * | 2009-04-01 | 2010-10-27 | Открытое акционерное общество "Нижнекамскнефтехим" | Способ очистки низших алканов |
| CN102433181B (zh) * | 2010-09-29 | 2014-03-12 | 中国石油化工股份有限公司 | 煤矿区煤层气催化脱氧的方法 |
| WO2018173143A1 (ja) * | 2017-03-22 | 2018-09-27 | 日揮株式会社 | 天然ガスの処理装置 |
| CN111744355B (zh) * | 2020-05-19 | 2022-02-01 | 福建省气柜设备安装有限公司 | 一种工业混合气体的脱硫方法及脱硫装置 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB340016A (en) * | 1929-09-16 | 1930-12-16 | Ig Farbenindustrie Ag | A process for the catalytic desulphurization of gases |
| US3420618A (en) * | 1965-07-06 | 1969-01-07 | Catalysts & Chem Inc | Gas purification by hydrogenation |
| US4175928A (en) * | 1975-12-05 | 1979-11-27 | Conoco Methanation Company | Hydrodesulfurization purification process for coal gasification |
| DE2731611B2 (de) * | 1977-07-13 | 1979-11-22 | Loi Industrieofenanlagen Gmbh, 4300 Essen | Verfahren zum Erzeugen weitgehend schwefelfreier Brenngase bei der Gewinnung von Schutzgasen aus schwefelhaltigen Rohgasen |
| US4181503A (en) * | 1978-10-30 | 1980-01-01 | United Technologies Corporation | Process for alternately steam reforming sulfur containing hydrocarbons that vary in oxygen content |
| US4260840A (en) * | 1980-01-11 | 1981-04-07 | Exxon Research & Engineering Co. | Butene-1 containing feed purification process(CS-165) |
| FR2521448A1 (fr) * | 1982-02-15 | 1983-08-19 | Inst Francais Du Petrole | Procede pour l'hydrodesulfuration de gaz naturel contenant des composes organiques du soufre et de l'oxygene |
-
1982
- 1982-05-25 FR FR8209210A patent/FR2527473A1/fr active Granted
-
1983
- 1983-02-15 US US06/466,689 patent/US4505880A/en not_active Expired - Fee Related
- 1983-04-28 EP EP83400856A patent/EP0095395B1/fr not_active Expired
- 1983-04-28 DE DE8383400856T patent/DE3361056D1/de not_active Expired
- 1983-05-25 CA CA000428824A patent/CA1192023A/fr not_active Expired
- 1983-05-25 JP JP58093340A patent/JPS58215488A/ja active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5502606A (en) * | 1992-07-17 | 1996-03-26 | Mitsubishi Denki Kabushiki Kaisha | Rotary magnetic head device having plural magnetic heads which are independently movable |
| US5684652A (en) * | 1992-07-17 | 1997-11-04 | Mitsubishi Denki Kabushiki Kaisha | Rotary magnetic head device using plural magnets and coils to position plural magnetic heads |
| JP2010180197A (ja) * | 2008-08-27 | 2010-08-19 | Kobelco Eco-Solutions Co Ltd | 消化ガスの脱酸素方法及び装置 |
| JP2013538880A (ja) * | 2010-07-15 | 2013-10-17 | クアドロジェン・パワー・システムズ・インコーポレイテッド | 水、シロキサン、硫黄、酸素、塩化物、揮発性有機化合物を除去するための統合型バイオガス浄化システム |
| US10780391B2 (en) | 2010-07-15 | 2020-09-22 | Quadrogen Power Systems, Inc. | Integrated biogas cleaning system to remove water, siloxanes, sulfur, oxygen, chlorides and volatile organic compounds |
| JP2019529306A (ja) * | 2016-09-01 | 2019-10-17 | ティッセンクルップ インダストリアル ソリューションズ アクツィエンゲゼルシャフトＴｈｙｓｓｅｎＫｒｕｐｐ Ｉｎｄｕｓｔｒｉａｌ Ｓｏｌｕｔｉｏｎｓ ＡＧ | 水素富化ガスから有機硫黄化合物を除去するための方法および装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0095395A1 (fr) | 1983-11-30 |
| EP0095395B1 (fr) | 1985-10-23 |
| FR2527473B1 (enExample) | 1984-12-14 |
| US4505880A (en) | 1985-03-19 |
| CA1192023A (fr) | 1985-08-20 |
| DE3361056D1 (en) | 1985-11-28 |
| FR2527473A1 (fr) | 1983-12-02 |
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