JPS58197724A - Gas introducing tube for vapor growth apparatus - Google Patents

Gas introducing tube for vapor growth apparatus

Info

Publication number
JPS58197724A
JPS58197724A JP7943482A JP7943482A JPS58197724A JP S58197724 A JPS58197724 A JP S58197724A JP 7943482 A JP7943482 A JP 7943482A JP 7943482 A JP7943482 A JP 7943482A JP S58197724 A JPS58197724 A JP S58197724A
Authority
JP
Japan
Prior art keywords
gas
tube
introducing tube
gas introducing
holes
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP7943482A
Other languages
Japanese (ja)
Inventor
Michio Ichikawa
市川 道生
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toshiba Corp
Original Assignee
Toshiba Corp
Tokyo Shibaura Electric Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toshiba Corp, Tokyo Shibaura Electric Co Ltd filed Critical Toshiba Corp
Priority to JP7943482A priority Critical patent/JPS58197724A/en
Publication of JPS58197724A publication Critical patent/JPS58197724A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber
    • C23C16/45563Gas nozzles
    • C23C16/45578Elongated nozzles, tubes with holes
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/455Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for introducing gases into reaction chamber or for modifying gas flows in reaction chamber

Abstract

PURPOSE:To uniformly supply reaction gas onto wafers by erecting a gas introducing tube within the bell jar forming a vapor growth apparatus, this tube is surrounded by a heating susceptor mounting semiconductor wafers, said gas introducing tube is extruded and hole diameter is gradually reduced while the holes becomes closer to the closed end of gas introducing tube on the occasion of boring many gas injection holes. CONSTITUTION:A gas introducing tube 7 of which upper end is closed is erected at the center of bell jar 5 having a gas exhaust port 4 at the side surface of bottom part. At the interim of introducing tube 7, a susceptor 9 having a heater at the lower end thereof surrounding such tube is provided horizontally and a plurality of semiconductor wafers 8 are placed thereon. Next, the gas introducing tube 7 is further extended upward and this tube is provided with many gas injection holes 2 of which diameter is gradually reduced as the holes is located closer to the upper end of tube 3. Accordingly, uniform thickness of thin film obtained by vapor growth can be obtained without relation to placing position of wafers 8.

Description

【発明の詳細な説明】 〔発明の技術分野〕 本発明は気相成長製麹用ガス導入管に関する。[Detailed description of the invention] [Technical field of invention] The present invention relates to a gas introduction pipe for vapor phase growth koji production.

〔発明の技術的背景〕[Technical background of the invention]

従来の気相成長装置用ガス導入管は1例えは第11!3
に示す如く、一端を開口し、かっ他端な閉塞した管体l
の周面に、はぼ同じ大きさの開口径を有するガス噴出孔
2を多数個穿設したものである・而して、この気相成長
′Ikal用ガス導入管Jt’、112因檻:示す如く
、底INユガス排気口4を有するペルジャー1の路中央
部Cユ、ナセプタ支持用のヒーター−を貫挿して立設さ
れたガス導入管F C接続して使用されている・すなわ
ち、多銀個の半導体クエハ1が載置された葉セプタ廖を
、気相成長装置用ガス導入管1を貫挿してヒーターI上
−二設赦し、ガス導入管rから供給された反応ガスを、
ガス噴出孔lから放出することにより、半導体ウニ八8
上感二所定の#m膜【気相成畏区;より形成している。
The conventional gas inlet pipe for vapor phase growth equipment is 1 example 11!3
As shown in the figure, a tube l with one end open and the other end closed.
A large number of gas ejection holes 2 having opening diameters of approximately the same size are bored on the circumferential surface of the gas-phase growth 'Ikal gas inlet pipe Jt', 112 reasons: As shown, the gas inlet pipe FC installed vertically through the central part of the pelger 1 having the bottom IN gas exhaust port 4 is inserted through the heater for supporting the naceptor. A gas inlet pipe 1 for a vapor phase growth apparatus is inserted into the leaf septa chamber on which a silver semiconductor wafer 1 is placed, and a reactant gas supplied from the gas inlet pipe R is inserted into the spacer.
Semiconductor sea urchin 88 is released by releasing gas from the gas outlet l.
It is formed from a predetermined #m film [vapor phase formation area].

〔背景技術の問題点〕[Problems with background technology]

前述の気相成長製麹用ガス尋人管1は、その周−鑑;開
口径が一定の大きさのガス噴出孔1を多数個穿設したも
のであるため、気相成長用ガス導入管から遣くへ位置す
るウニへ上へのガス供給It(供給速度)は小さい・ハ
のため、す七ブタ9上の半導体クエへ1の表[i]6;
、均一な噴出量で反応ガスを噴出することができない・
その結果、半導体ウニ八1上6:形成された薄1lil
l&の績犀値のばらつきを−ベると、第3図6;示す如
く、気相成長用ガス導入管1の近傍≦:配装された半導
体ウニ八1上では、予定した一厚値より大きい値で±l
O悌以上のばらつきがある・そして、気相成長用ガス導
入管1から遠く離れて配置された半導体ウェハ8上では
、予定した膜厚値より小さい値で±10悌以上のばらつ
きがある・このよう6ユ従来の気相成長装置用ガス導入
管から噴出されたガス濃度≦−はむらが生じるため、半
導体ウェハ5の表thN≦;所望の#膜を均一な膜厚で
形成できず、製造歩留を著しく低下させる欠点があった
The gas introduction tube 1 for vapor-phase growth koji production described above has a large number of gas injection holes 1 with a constant opening diameter, so it is a gas introduction tube for vapor-phase growth. Since the upward gas supply It (supply speed) to the sea urchin located in Karakura is small.
, the reaction gas cannot be ejected with a uniform ejection amount.
As a result, the semiconductor sea urchin 81 upper 6: formed thin 1 lil
Looking at the variations in the thickness values of 1&, as shown in Figure 3, 6, in the vicinity of the gas introduction pipe 1 for vapor phase growth ≦: on the arranged semiconductor tube 1, the thickness is smaller than the planned one thickness value. ±l for large values
There is a variation of more than 0° on the semiconductor wafer 8 placed far away from the gas introduction tube 1 for vapor phase growth, and there is a variation of more than ±10° at a value smaller than the planned film thickness value. As a result, the concentration of the gas ejected from the gas introduction pipe for a conventional vapor phase growth apparatus is uneven, so that the desired # film cannot be formed on the surface of the semiconductor wafer 5 with a uniform thickness, and the manufacturing process is delayed. There was a drawback that the yield was significantly reduced.

〔発明の目的〕[Purpose of the invention]

本発明は、ガス噴出孔からの距1llI≦二関係なく。 In the present invention, the distance from the gas nozzle is 1llI≦2 regardless of the distance.

全ての位11t−配置された半導体ウェハの表面≦二。All positions 11t - surface of the semiconductor wafer arranged ≦2.

均一な膜厚の薄−を容易5−形成することができる気相
成長i!i直用ガスガス貨な提供することなその目的と
するものである。
Vapor phase growth i! can easily form a thin film with uniform thickness! Its purpose is to provide gas for direct use.

〔発明の概要〕[Summary of the invention]

本発明は、一端を開口し、他端を閉基した管体の周面に
、閉塞端側(−接近TるCユ従って開口径を次第(二小
さくしたガス噴出孔な多数個穿設することζ−より、閉
lI#1ifNIII11ユ近いガス噴出孔から噴出さ
れるガスの噴出圧力を太き(して。
In the present invention, a large number of gas ejection holes are bored on the circumferential surface of a tube with one end open and the other end closed, with the opening diameter gradually decreasing (2) on the closed end side (-approach T, C). In other words, the ejection pressure of the gas ejected from the gas ejection hole close to the closed lI#1ifNIII11 is increased.

全ての位l(=配置された半導体ウェハの表面Cユ。All places l (= surface C of the placed semiconductor wafer.

均一な膜厚の薄膜を容易≦ユ形成できるよう≦二した気
相成長装置用ガス導入管である。
This is a gas inlet tube for a vapor phase growth apparatus that can easily form a thin film with a uniform thickness.

〔発明の実施例〕[Embodiments of the invention]

以下1本発明の一実施例について図面を参照して説明す
る。弗4内は1本発明の一実施例の正th1因である。
An embodiment of the present invention will be described below with reference to the drawings.弗4 is the positive th1 factor in one embodiment of the present invention.

この気相成長装置用ガス導入管20は、一端を開口し、
他端を閉塞した管体力F14WILi[+20ai’−
、開口一部側から閉塞端部側に向って次@−二開口径が
小さくなるガス噴出孔2)を多数個穿設したものである
・ ここで、開基端部側V〕ガガス出孔271の径を小さく
したのは、噴出する反応ガスの圧力を大きくして、開口
端部側のガス噴出孔21bから噴出された反応ガスとが
同時に同−平tTn t= fiするよう6二−「るこ
と6二よヲ」、同一平面の任意の位1i1−供給される
反応ガスm度yt一定≦ユするためである・径を小さく
したことく−よるガス噴出孔27mからの噴出ガス量の
減少は、ガス噴出孔JjagJl!9増加すること≦ユ
より補償されている・つまり、ガス噴出孔11mは、閉
塞端部IIIJ≦;接近する6:従ってその径が小さく
設定されていると共6二、穿設個数は径Q縮小率区二応
じて増加されているーガス噴出孔21m、21bの径の
縮小串、開口端部側から閉側端部側(−かけての穿設個
数の疎、密状態は、気相成長¥iii用ガス導入管20
内C;供給される反応ガスの供給量、及びこのガス導入
管IOを使用する気相成長装置の半導体ウェハ収納容量
等を考慮して設定するのが4ましい・従って、ガス噴出
孔j J’a l j I’b穿−設個数の疎布状態は
、第5因に示す如く、閉基端部側区;集中的区二径の小
さいガス噴出孔21’ak穿設し、これらと所定の開部
を設けて開口端部側の周Wt&+2/at二、径の大き
いガス噴出孔jj’bを所だ個数疎 状態で穿設しても
良い。
This gas introduction pipe 20 for a vapor phase growth apparatus has one end open,
Tube force with the other end closed F14WILi[+20ai'-
, a large number of gas ejection holes 2) are drilled in which the diameter of the opening becomes smaller from the opening side toward the closed end side. The reason why the diameter of is made small is to increase the pressure of the ejected reaction gas so that the reaction gas ejected from the gas ejection hole 21b on the open end side is at the same time as tTn t=fi. This is because the amount of gas ejected from the gas ejection hole 27m due to the smaller diameter is maintained at any arbitrary location on the same plane. The decrease is due to the gas vent JjagJl! 9 increases ≦Y. In other words, the gas ejection holes 11m approach the closed end IIIJ≦; 6: Therefore, if the diameter is set small, the number of holes drilled is The diameter of the gas ejection holes 21m and 21b is increased according to the reduction rate, and the number of holes from the open end side to the closed end side (-) is sparse and dense due to vapor phase growth. Gas introduction pipe 20 for ¥iii
C: It is preferable to set this by taking into consideration the amount of reactant gas to be supplied and the semiconductor wafer storage capacity of the vapor phase growth apparatus that uses this gas introduction pipe IO. Therefore, the gas injection hole j J As shown in the fifth factor, the number of holes 21'ak drilled in the closed proximal end side section; A predetermined opening may be provided, and a certain number of gas ejection holes jj'b with a large diameter may be bored in a sparse manner at the circumference Wt&+2/at2 on the opening end side.

向して、このように構成された気相成長′IIkIr用
ガス導入管z ov、sz図区二示すものと同様の気相
成装置のペルジャー内鑑;設直し、ヒーター上のサセプ
タ9に載置された半導体ウェハ8区ユ、気相成長処理番
−よる#il膜形成を行った0半導体ウニ八8の載置さ
れた位置とその表[kIt二形酸形成た1IllI!l
Iの基準値−一対するばらつき1に調べたところ第6図
中特性線(11で示す結果を得た。
For this purpose, the gas inlet pipe for vapor phase growth 'IIkIr constructed in this way was rebuilt and mounted on the susceptor 9 above the heater. Semiconductor wafers placed in 8 sections, vapor phase growth process number - 0 semiconductor wafers 8 where #il films were formed and their table [kIt dimorphic acid formed 1IllI! l
When examining the standard value of I-paired variation 1, the results shown by the characteristic line (11) in FIG. 6 were obtained.

同図から明らかなように、半纏体ウェハ8の設置位置に
関係なく、全ての位1ltcDものに対してほぼ基準値
≦ユ等しい膜厚の#dが形成されていることが確認され
た・また、第5図し示す小径のガス噴出孔it’sの配
置と大径のガス噴出孔11’bの配!IY東中的にして
、各々を所定間隔で離間した気相成長装置用ガス導入管
20′礁1ついても同様の実験を行ったところ、第6図
中特性線(厘)≦二て示す結果を得た・この特性線(鳳
)からも明らかなよう一一、全ての配置位kt二おける
半導体ウェハ1の表面&−1予定した基準膜厚値区二対
して±511/J変動率の範囲で所定の薄膜が形成され
ていることが判った・ このよう4二この気相成長装置用ガス導入管ZUI;よ
れば、その近傍≦二装置された全ての半導体ウニ八1上
≦二、−足菫の反応ガスを供給せしめてその濃度を所定
値に容易1二設定できるので、半導体ウニ八8の設置位
1it=左右されず≦ユ。
As is clear from the figure, it was confirmed that regardless of the installation position of the semi-integrated wafer 8, #d was formed with a film thickness that was approximately equal to the reference value≦Y for all 1ltcD wafers. , the arrangement of the small-diameter gas ejection holes it's and the arrangement of the large-diameter gas ejection holes 11'b shown in FIG. A similar experiment was carried out with one gas inlet pipe 20' for a vapor growth apparatus separated at a predetermined interval at IY East and Chuo, and the results shown in the characteristic line (厘)≦2 in Figure 6 were obtained. As is clear from this characteristic line (Otori), there is a variation rate of ±511/J for the surface of the semiconductor wafer 1 at all placement positions kt2 with respect to the predetermined standard film thickness value range 2. It was found that a predetermined thin film was formed within the range of 42.According to the gas inlet pipe ZUI for this vapor phase growth apparatus, it was found that the vicinity of all the semiconductors 81 that were installed in the apparatus was ≦2, - Since the reaction gas of the foot violet can be supplied and its concentration can be easily set to a predetermined value, the installation position of the semiconductor sea urchin 8 is independent of 1it=≦Y.

所定の膜厚の薄膜を均一6;形成できる。その結果、製
造歩留を著しく同上させることができる・〔発明の効果
〕 以上説明した如く1本発明6;係る気相成擾装置用ガス
導入管によれば、全ての位Ik1−配置された半導体ク
エへの表面(−1均一な膜厚を有する薄膜を容易区二形
成して、製造歩留を高めることができるものである。
A thin film of a predetermined thickness can be uniformly formed. As a result, the manufacturing yield can be significantly increased. [Effects of the Invention] As explained above, according to the present invention 6; It is possible to easily form a thin film having a uniform thickness on the surface of a semiconductor substrate, thereby increasing the manufacturing yield.

【図面の簡単な説明】[Brief explanation of drawings]

141図は、従来の気相成長*l[用ガス導入管の正面
図、82図は、同ガス纏入管を使用した気相成長*I[
の断IiI図、塾3図は、膜厚変動率と半導体クエへの
設麹位麹の関係な示す特性図。 第4図は1本発明の一実施例の正th+因、−5因は1
本楯明の他の実施例の上白図、與6図は。 膜厚変動率と半動体ウニへの設置位!ill: co関
係を示す特性図である◎ I O−1tl−・気相61km’ll用Nx尋入管。 出願人を一人弁理土鈴江武 彦
Figure 141 is a front view of a gas introduction tube for conventional vapor phase growth*I[, and Figure 82 is a front view of a gas introduction tube for conventional vapor phase growth*I[.
The cross-section diagram IiI and the figure 3 are characteristic diagrams showing the relationship between the film thickness variation rate and the position of koji for semiconductor processing. Figure 4 shows the positive th+ factor and -5 factor of an embodiment of the present invention.
The top white diagram and the bottom 6 diagram of other examples of this shield are shown. Film thickness variation rate and installation position on semi-moving body sea urchin! ill: This is a characteristic diagram showing the co relationship. Takehiko Suzue, patent attorney for the applicant

Claims (1)

【特許請求の範囲】 一端を開口し他端を閉塞した管体の周を面(:。 開口端部側から閉塞端部側に同って法部(−開口径が小
さくなるガス噴出孔を多数個穿設してなることな特徴と
する気相成長装置用ガス導入管。
[Claims] The periphery of a tube with one end open and the other end closed is a surface (:. A gas ejection hole with a small opening diameter is formed from the open end side to the closed end side. A gas introduction pipe for a vapor phase growth apparatus that has a unique feature of having multiple holes.
JP7943482A 1982-05-12 1982-05-12 Gas introducing tube for vapor growth apparatus Pending JPS58197724A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP7943482A JPS58197724A (en) 1982-05-12 1982-05-12 Gas introducing tube for vapor growth apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7943482A JPS58197724A (en) 1982-05-12 1982-05-12 Gas introducing tube for vapor growth apparatus

Publications (1)

Publication Number Publication Date
JPS58197724A true JPS58197724A (en) 1983-11-17

Family

ID=13689767

Family Applications (1)

Application Number Title Priority Date Filing Date
JP7943482A Pending JPS58197724A (en) 1982-05-12 1982-05-12 Gas introducing tube for vapor growth apparatus

Country Status (1)

Country Link
JP (1) JPS58197724A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5620523A (en) * 1994-04-11 1997-04-15 Canon Sales Co., Inc. Apparatus for forming film
EP1226286A1 (en) * 1999-06-24 2002-07-31 Gadgil, Prasad Narhar Apparatus for atomic layer chemical vapor deposition
US6881295B2 (en) 2000-03-28 2005-04-19 Nec Electronics Corporation Air-tight vessel equipped with gas feeder uniformly supplying gaseous component around plural wafers
US20130068161A1 (en) * 2011-09-15 2013-03-21 Applied Materials, Inc. Gas delivery and distribution for uniform process in linear-type large-area plasma reactor
WO2015155078A1 (en) * 2014-04-09 2015-10-15 Bühler Alzenau Gmbh Gas distribution apparatus in a vacuum chamber, comprising a gas conducting device
CN109237941A (en) * 2018-10-30 2019-01-18 湖南金炉科技股份有限公司 bell-type furnace

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5620523A (en) * 1994-04-11 1997-04-15 Canon Sales Co., Inc. Apparatus for forming film
EP1226286A1 (en) * 1999-06-24 2002-07-31 Gadgil, Prasad Narhar Apparatus for atomic layer chemical vapor deposition
EP1226286A4 (en) * 1999-06-24 2007-08-15 Prasad Narhar Gadgil Apparatus for atomic layer chemical vapor deposition
US6881295B2 (en) 2000-03-28 2005-04-19 Nec Electronics Corporation Air-tight vessel equipped with gas feeder uniformly supplying gaseous component around plural wafers
US20130068161A1 (en) * 2011-09-15 2013-03-21 Applied Materials, Inc. Gas delivery and distribution for uniform process in linear-type large-area plasma reactor
CN103797155A (en) * 2011-09-15 2014-05-14 应用材料公司 Gas delivery and distribution for uniform process in linear-type large-area plasma reactor
TWI550123B (en) * 2011-09-15 2016-09-21 應用材料股份有限公司 Gas delivery and distribution system for uniform process in linear-type large-area plasma reactor and a processing chamber therefor
WO2015155078A1 (en) * 2014-04-09 2015-10-15 Bühler Alzenau Gmbh Gas distribution apparatus in a vacuum chamber, comprising a gas conducting device
CN109237941A (en) * 2018-10-30 2019-01-18 湖南金炉科技股份有限公司 bell-type furnace

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