JPS58181710A - アルカリモノフルオロホスフエ−トの製造方法 - Google Patents
アルカリモノフルオロホスフエ−トの製造方法Info
- Publication number
- JPS58181710A JPS58181710A JP6043382A JP6043382A JPS58181710A JP S58181710 A JPS58181710 A JP S58181710A JP 6043382 A JP6043382 A JP 6043382A JP 6043382 A JP6043382 A JP 6043382A JP S58181710 A JPS58181710 A JP S58181710A
- Authority
- JP
- Japan
- Prior art keywords
- phosphate
- alkali
- alkali metal
- hydrogen fluoride
- anhydrous hydrogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003513 alkali Substances 0.000 title claims abstract description 11
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 5
- 229940074371 monofluorophosphate Drugs 0.000 title claims abstract description 4
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims abstract description 17
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 15
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 13
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 12
- 239000010452 phosphate Substances 0.000 claims abstract description 12
- 150000001340 alkali metals Chemical class 0.000 claims abstract description 6
- 150000001339 alkali metal compounds Chemical class 0.000 claims description 10
- 229910001463 metal phosphate Inorganic materials 0.000 claims description 2
- 235000011180 diphosphates Nutrition 0.000 abstract description 5
- 125000005341 metaphosphate group Chemical group 0.000 abstract description 5
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 4
- 239000000843 powder Substances 0.000 abstract description 4
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 3
- 239000011574 phosphorus Substances 0.000 abstract description 3
- 229910052700 potassium Inorganic materials 0.000 abstract description 3
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract description 2
- 239000008187 granular material Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract description 2
- 229910052708 sodium Inorganic materials 0.000 abstract description 2
- 239000011734 sodium Substances 0.000 abstract description 2
- 229910000765 intermetallic Inorganic materials 0.000 abstract 3
- XPPKVPWEQAFLFU-UHFFFAOYSA-J diphosphate(4-) Chemical compound [O-]P([O-])(=O)OP([O-])([O-])=O XPPKVPWEQAFLFU-UHFFFAOYSA-J 0.000 abstract 2
- 235000019832 sodium triphosphate Nutrition 0.000 abstract 1
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 12
- 235000021317 phosphate Nutrition 0.000 description 10
- 239000007789 gas Substances 0.000 description 9
- 229910000318 alkali metal phosphate Inorganic materials 0.000 description 8
- -1 alkali metal salt Chemical class 0.000 description 8
- 238000000034 method Methods 0.000 description 8
- 239000000203 mixture Substances 0.000 description 6
- 239000002994 raw material Substances 0.000 description 5
- 238000003682 fluorination reaction Methods 0.000 description 4
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 3
- 229910052731 fluorine Inorganic materials 0.000 description 3
- 239000011737 fluorine Substances 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 2
- DGTVXEHQMSJRPE-UHFFFAOYSA-M difluorophosphinate Chemical compound [O-]P(F)(F)=O DGTVXEHQMSJRPE-UHFFFAOYSA-M 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- DLYUQMMRRRQYAE-UHFFFAOYSA-N tetraphosphorus decaoxide Chemical compound O1P(O2)(=O)OP3(=O)OP1(=O)OP2(=O)O3 DLYUQMMRRRQYAE-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 239000004254 Ammonium phosphate Substances 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical compound OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- 101100283604 Caenorhabditis elegans pigk-1 gene Proteins 0.000 description 1
- 239000005696 Diammonium phosphate Substances 0.000 description 1
- 229910017736 MH2PO4 Inorganic materials 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 1
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical class [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 description 1
- 235000019289 ammonium phosphates Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 229910000388 diammonium phosphate Inorganic materials 0.000 description 1
- 235000019838 diammonium phosphate Nutrition 0.000 description 1
- MHJAJDCZWVHCPF-UHFFFAOYSA-L dimagnesium phosphate Chemical compound [Mg+2].OP([O-])([O-])=O MHJAJDCZWVHCPF-UHFFFAOYSA-L 0.000 description 1
- DWYMPOCYEZONEA-UHFFFAOYSA-N fluorophosphoric acid Chemical compound OP(O)(F)=O DWYMPOCYEZONEA-UHFFFAOYSA-N 0.000 description 1
- ZSZNUIGFWQXJMQ-UHFFFAOYSA-K gold(3+);phosphate Chemical compound [Au+3].[O-]P([O-])([O-])=O ZSZNUIGFWQXJMQ-UHFFFAOYSA-K 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6043382A JPS58181710A (ja) | 1982-04-13 | 1982-04-13 | アルカリモノフルオロホスフエ−トの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6043382A JPS58181710A (ja) | 1982-04-13 | 1982-04-13 | アルカリモノフルオロホスフエ−トの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58181710A true JPS58181710A (ja) | 1983-10-24 |
| JPS6222925B2 JPS6222925B2 (enrdf_load_stackoverflow) | 1987-05-20 |
Family
ID=13142111
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP6043382A Granted JPS58181710A (ja) | 1982-04-13 | 1982-04-13 | アルカリモノフルオロホスフエ−トの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS58181710A (enrdf_load_stackoverflow) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5393506A (en) * | 1990-12-24 | 1995-02-28 | Kali-Chemie Aktiengesellschaft | Method for the manufacturing of alkali monofluorophosphate |
| WO2006043538A1 (ja) * | 2004-10-19 | 2006-04-27 | Mitsubishi Chemical Corporation | ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池 |
| JP2006143572A (ja) * | 2004-10-19 | 2006-06-08 | Mitsubishi Chemicals Corp | ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池 |
| WO2006137177A1 (ja) * | 2005-06-20 | 2006-12-28 | Mitsubishi Chemical Corporation | ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池 |
| JP2010260761A (ja) * | 2009-05-01 | 2010-11-18 | Kyushu Univ | 非水電解質二次電池用正極の製造方法及びそれを用いた非水電解質二次電池 |
| JP2021160974A (ja) * | 2020-03-31 | 2021-10-11 | 三井化学株式会社 | フッ化無機化合物粒子の製造方法 |
| JP2021160978A (ja) * | 2020-03-31 | 2021-10-11 | 三井化学株式会社 | アルカリモノフルオロホスフェート組成物の製造方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5673610A (en) * | 1979-11-22 | 1981-06-18 | Central Glass Co Ltd | Manufacture of alkali monofluorophosphate |
-
1982
- 1982-04-13 JP JP6043382A patent/JPS58181710A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5673610A (en) * | 1979-11-22 | 1981-06-18 | Central Glass Co Ltd | Manufacture of alkali monofluorophosphate |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5393506A (en) * | 1990-12-24 | 1995-02-28 | Kali-Chemie Aktiengesellschaft | Method for the manufacturing of alkali monofluorophosphate |
| WO2006043538A1 (ja) * | 2004-10-19 | 2006-04-27 | Mitsubishi Chemical Corporation | ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池 |
| JP2006143572A (ja) * | 2004-10-19 | 2006-06-08 | Mitsubishi Chemicals Corp | ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池 |
| CN101080361B (zh) | 2004-10-19 | 2011-03-30 | 三菱化学株式会社 | 二氟磷酸盐的制造方法、用于二次电池的非水电解液及非水电解液二次电池 |
| US8076033B2 (en) | 2004-10-19 | 2011-12-13 | Mitsubishi Chemical Corporation | Method for producing difluorophosphate, nonaqueous electrolyte solution for secondary battery and nonaqueous electrolyte secondary battery |
| US8137848B2 (en) | 2004-10-19 | 2012-03-20 | Mitsubishi Chemical Corporation | Method for producing difluorophosphate, nonaqueous electrolyte solution for secondary batteries, and nonaqueous electrolyte secondary battery |
| WO2006137177A1 (ja) * | 2005-06-20 | 2006-12-28 | Mitsubishi Chemical Corporation | ジフルオロリン酸塩の製造方法、二次電池用非水系電解液及び非水系電解液二次電池 |
| US8980214B2 (en) | 2005-06-20 | 2015-03-17 | Mitsubishi Chemical Corporation | Method for producing difluorophosphate, non-aqueous electrolyte for secondary cell and non-aqueous electrolyte secondary cell |
| US9593016B2 (en) | 2005-06-20 | 2017-03-14 | Mitsubishi Chemical Corporation | Method for producing difluorophosphate, non-aqueous electrolyte for secondary cell and non-aqueous electrolyte secondary cell |
| JP2010260761A (ja) * | 2009-05-01 | 2010-11-18 | Kyushu Univ | 非水電解質二次電池用正極の製造方法及びそれを用いた非水電解質二次電池 |
| JP2021160974A (ja) * | 2020-03-31 | 2021-10-11 | 三井化学株式会社 | フッ化無機化合物粒子の製造方法 |
| JP2021160978A (ja) * | 2020-03-31 | 2021-10-11 | 三井化学株式会社 | アルカリモノフルオロホスフェート組成物の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6222925B2 (enrdf_load_stackoverflow) | 1987-05-20 |
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