JPS58151332A - 塩化鉄水溶液より鉄を含む水酸化物を製造する方法 - Google Patents
塩化鉄水溶液より鉄を含む水酸化物を製造する方法Info
- Publication number
- JPS58151332A JPS58151332A JP2905882A JP2905882A JPS58151332A JP S58151332 A JPS58151332 A JP S58151332A JP 2905882 A JP2905882 A JP 2905882A JP 2905882 A JP2905882 A JP 2905882A JP S58151332 A JPS58151332 A JP S58151332A
- Authority
- JP
- Japan
- Prior art keywords
- phase
- solvent
- iron
- aqueous solution
- separated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims abstract description 49
- 229910052742 iron Inorganic materials 0.000 title claims abstract description 33
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 title claims abstract description 19
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 title claims description 4
- 239000002904 solvent Substances 0.000 claims abstract description 46
- 238000000638 solvent extraction Methods 0.000 claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000000605 extraction Methods 0.000 claims abstract description 22
- -1 iron ions Chemical class 0.000 claims abstract description 17
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims abstract description 10
- 235000014413 iron hydroxide Nutrition 0.000 claims abstract description 10
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 claims abstract description 10
- 150000002500 ions Chemical class 0.000 claims abstract description 8
- 239000012071 phase Substances 0.000 claims description 37
- 239000007864 aqueous solution Substances 0.000 claims description 30
- 238000000034 method Methods 0.000 claims description 23
- 230000003647 oxidation Effects 0.000 claims description 13
- 238000007254 oxidation reaction Methods 0.000 claims description 13
- 238000004821 distillation Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 239000000243 solution Substances 0.000 claims description 8
- 239000008346 aqueous phase Substances 0.000 claims description 5
- 238000006386 neutralization reaction Methods 0.000 claims description 4
- 239000012141 concentrate Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 238000003287 bathing Methods 0.000 claims 2
- 238000000975 co-precipitation Methods 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 4
- 230000003472 neutralizing effect Effects 0.000 abstract description 2
- 230000001590 oxidative effect Effects 0.000 abstract description 2
- 239000012535 impurity Substances 0.000 description 9
- 239000007791 liquid phase Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- 238000011282 treatment Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000005554 pickling Methods 0.000 description 4
- 238000007664 blowing Methods 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 238000009834 vaporization Methods 0.000 description 2
- 230000008016 vaporization Effects 0.000 description 2
- 229910000859 α-Fe Inorganic materials 0.000 description 2
- SYBYTAAJFKOIEJ-UHFFFAOYSA-N 3-Methylbutan-2-one Chemical compound CC(C)C(C)=O SYBYTAAJFKOIEJ-UHFFFAOYSA-N 0.000 description 1
- 229910002588 FeOOH Inorganic materials 0.000 description 1
- 229910017163 MnFe2O4 Inorganic materials 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000001479 atomic absorption spectroscopy Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 238000011221 initial treatment Methods 0.000 description 1
- 150000002505 iron Chemical class 0.000 description 1
- 150000002506 iron compounds Chemical class 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- ZGHFDIIVVIFNPS-UHFFFAOYSA-N methyl alpha-methylvinyl ketone Natural products CC(=C)C(C)=O ZGHFDIIVVIFNPS-UHFFFAOYSA-N 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000008685 targeting Effects 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Landscapes
- Compounds Of Iron (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2905882A JPS58151332A (ja) | 1982-02-26 | 1982-02-26 | 塩化鉄水溶液より鉄を含む水酸化物を製造する方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2905882A JPS58151332A (ja) | 1982-02-26 | 1982-02-26 | 塩化鉄水溶液より鉄を含む水酸化物を製造する方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58151332A true JPS58151332A (ja) | 1983-09-08 |
| JPS6140601B2 JPS6140601B2 (enrdf_load_stackoverflow) | 1986-09-10 |
Family
ID=12265760
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2905882A Granted JPS58151332A (ja) | 1982-02-26 | 1982-02-26 | 塩化鉄水溶液より鉄を含む水酸化物を製造する方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS58151332A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007230850A (ja) * | 2006-03-03 | 2007-09-13 | Tanaka Chemical Corp | 高純度水酸化鉄の製造方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5286999A (en) * | 1976-01-16 | 1977-07-20 | Nishimurawatanabe Chiyuushiyut | Recovery process for sulfur and metal or metal oxide from ferrous sulfate |
| JPS52115796A (en) * | 1976-03-25 | 1977-09-28 | Solex Res Corp Japan | Recovery process for waste acid containing iron |
-
1982
- 1982-02-26 JP JP2905882A patent/JPS58151332A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5286999A (en) * | 1976-01-16 | 1977-07-20 | Nishimurawatanabe Chiyuushiyut | Recovery process for sulfur and metal or metal oxide from ferrous sulfate |
| JPS52115796A (en) * | 1976-03-25 | 1977-09-28 | Solex Res Corp Japan | Recovery process for waste acid containing iron |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2007230850A (ja) * | 2006-03-03 | 2007-09-13 | Tanaka Chemical Corp | 高純度水酸化鉄の製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6140601B2 (enrdf_load_stackoverflow) | 1986-09-10 |
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