JPS58144377A - ５−メルカプトテトラゾリル−１−酢酸の製造法 - Google Patents
５−メルカプトテトラゾリル−１−酢酸の製造法Info
- Publication number
- JPS58144377A JPS58144377A JP2562382A JP2562382A JPS58144377A JP S58144377 A JPS58144377 A JP S58144377A JP 2562382 A JP2562382 A JP 2562382A JP 2562382 A JP2562382 A JP 2562382A JP S58144377 A JPS58144377 A JP S58144377A
- Authority
- JP
- Japan
- Prior art keywords
- low polarity
- organic solvent
- acid
- mercaptotetrazolyl
- acetic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Substances CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 title claims description 11
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000003960 organic solvent Substances 0.000 claims abstract description 13
- 150000002148 esters Chemical class 0.000 claims abstract description 12
- -1 alkali metal azide Chemical class 0.000 claims abstract description 8
- 239000002253 acid Substances 0.000 claims abstract description 7
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 5
- 150000002576 ketones Chemical class 0.000 claims abstract description 4
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims abstract description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 3
- 239000011707 mineral Substances 0.000 claims abstract description 3
- 239000008096 xylene Substances 0.000 claims abstract description 3
- 238000010438 heat treatment Methods 0.000 claims abstract 3
- 150000008282 halocarbons Chemical class 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims abstract 2
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 2
- PDQXSLJFPJSYBF-UHFFFAOYSA-N 2-(dithiocarboxyamino)acetic acid Chemical compound OC(=O)CNC(S)=S PDQXSLJFPJSYBF-UHFFFAOYSA-N 0.000 claims 1
- 239000012670 alkaline solution Substances 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 4
- 239000007858 starting material Substances 0.000 abstract description 2
- 150000001875 compounds Chemical class 0.000 abstract 3
- 230000003472 neutralizing effect Effects 0.000 abstract 2
- DKIJKONRLAWKDS-UHFFFAOYSA-N 2-(benzylsulfanylcarbothioylamino)acetic acid Chemical compound OC(=O)CNC(=S)SCC1=CC=CC=C1 DKIJKONRLAWKDS-UHFFFAOYSA-N 0.000 abstract 1
- UENWRTRMUIOCKN-UHFFFAOYSA-N benzyl thiol Chemical compound SCC1=CC=CC=C1 UENWRTRMUIOCKN-UHFFFAOYSA-N 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- AUHZEENZYGFFBQ-UHFFFAOYSA-N mesitylene Substances CC1=CC(C)=CC(C)=C1 AUHZEENZYGFFBQ-UHFFFAOYSA-N 0.000 abstract 1
- 125000001827 mesitylenyl group Chemical group [H]C1=C(C(*)=C(C([H])=C1C([H])([H])[H])C([H])([H])[H])C([H])([H])[H] 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000013078 crystal Substances 0.000 description 5
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 101100489867 Mus musculus Got2 gene Proteins 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 150000001540 azides Chemical class 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 238000010977 unit operation Methods 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2562382A JPS58144377A (ja) | 1982-02-18 | 1982-02-18 | ５−メルカプトテトラゾリル−１−酢酸の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2562382A JPS58144377A (ja) | 1982-02-18 | 1982-02-18 | ５−メルカプトテトラゾリル−１−酢酸の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58144377A true JPS58144377A (ja) | 1983-08-27 |
| JPS6155914B2 JPS6155914B2 (en, 2012) | 1986-11-29 |
Family
ID=12170998
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2562382A Granted JPS58144377A (ja) | 1982-02-18 | 1982-02-18 | ５−メルカプトテトラゾリル−１−酢酸の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS58144377A (en, 2012) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62179012U (en, 2012) * | 1986-05-01 | 1987-11-13 | ||
| JPH01228518A (ja) * | 1988-03-09 | 1989-09-12 | Matsushita Seiko Co Ltd | 換気装置用フィルター |
-
1982
- 1982-02-18 JP JP2562382A patent/JPS58144377A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6155914B2 (en, 2012) | 1986-11-29 |
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