JPS5775992A - Purification of stevioside - Google Patents
Purification of steviosideInfo
- Publication number
- JPS5775992A JPS5775992A JP15281980A JP15281980A JPS5775992A JP S5775992 A JPS5775992 A JP S5775992A JP 15281980 A JP15281980 A JP 15281980A JP 15281980 A JP15281980 A JP 15281980A JP S5775992 A JPS5775992 A JP S5775992A
- Authority
- JP
- Japan
- Prior art keywords
- stevioside
- activated charcoal
- decoloring
- activated
- purification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 title abstract 4
- 229940013618 stevioside Drugs 0.000 title abstract 4
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 title abstract 4
- 235000019202 steviosides Nutrition 0.000 title abstract 4
- 238000000746 purification Methods 0.000 title abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 239000004927 clay Substances 0.000 abstract 3
- 239000007788 liquid Substances 0.000 abstract 3
- 239000000126 substance Substances 0.000 abstract 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- 239000012535 impurity Substances 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 239000011347 resin Substances 0.000 abstract 2
- 229920005989 resin Polymers 0.000 abstract 2
- BFYCFODZOFWWAA-UHFFFAOYSA-N 2,4,6-trimethylpyridine-3-carbaldehyde Chemical compound CC1=CC(C)=C(C=O)C(C)=N1 BFYCFODZOFWWAA-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- 229920002125 Sokalan® Polymers 0.000 abstract 1
- 241000544066 Stevia Species 0.000 abstract 1
- 244000228451 Stevia rebaudiana Species 0.000 abstract 1
- 235000006092 Stevia rebaudiana Nutrition 0.000 abstract 1
- 229940037003 alum Drugs 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 239000000049 pigment Substances 0.000 abstract 1
- HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 abstract 1
Landscapes
- Saccharide Compounds (AREA)
- Compounds Of Unknown Constitution (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15281980A JPS5775992A (en) | 1980-10-30 | 1980-10-30 | Purification of stevioside |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP15281980A JPS5775992A (en) | 1980-10-30 | 1980-10-30 | Purification of stevioside |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5775992A true JPS5775992A (en) | 1982-05-12 |
| JPH0245637B2 JPH0245637B2 (enrdf_load_stackoverflow) | 1990-10-11 |
Family
ID=15548843
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP15281980A Granted JPS5775992A (en) | 1980-10-30 | 1980-10-30 | Purification of stevioside |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5775992A (enrdf_load_stackoverflow) |
Cited By (43)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8257948B1 (en) | 2011-02-17 | 2012-09-04 | Purecircle Usa | Method of preparing alpha-glucosyl Stevia composition |
| US8299224B2 (en) | 2009-10-15 | 2012-10-30 | Purecircle Sdn Bhd | High-purity Rebaudioside D |
| US8318459B2 (en) | 2011-02-17 | 2012-11-27 | Purecircle Usa | Glucosyl stevia composition |
| US8334006B2 (en) | 2005-10-11 | 2012-12-18 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8337927B2 (en) | 2005-10-11 | 2012-12-25 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8414948B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie ice cream containing the same |
| US8414950B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie table top tablet containing the same |
| US8414952B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie diet cookies containing the same |
| US8414949B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie yogurt containing the same |
| US8414951B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie soy sauce containing the same |
| US8420147B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie cake containing the same |
| US8420146B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie bread containing the same |
| US8507022B2 (en) | 2009-10-15 | 2013-08-13 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same |
| US8512790B2 (en) | 2009-10-15 | 2013-08-20 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie chocolate containing the same |
| US8568818B2 (en) | 2009-10-15 | 2013-10-29 | Pure Circle Sdn Bhd | High-purity Rebaudioside D and low-calorie carbonated drink containing the same |
| US8574656B2 (en) | 2009-10-15 | 2013-11-05 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie fruit juice containing the same |
| EP2708548A2 (en) | 2009-10-15 | 2014-03-19 | Purecircle SDN BHD | High-Purity Rebaudioside D and Applications |
| US8790730B2 (en) | 2005-10-11 | 2014-07-29 | Purecircle Usa | Process for manufacturing a sweetener and use thereof |
| US8916138B2 (en) | 2009-10-15 | 2014-12-23 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie tooth paste composition containing the same |
| CN105037459A (zh) * | 2015-07-23 | 2015-11-11 | 蚌埠市华东生物科技有限公司 | 一种能提高甜菊糖苷精制效率的絮凝剂 |
| US9752174B2 (en) | 2013-05-28 | 2017-09-05 | Purecircle Sdn Bhd | High-purity steviol glycosides |
| US9771434B2 (en) | 2011-06-23 | 2017-09-26 | Purecircle Sdn Bhd | Products from stevia rebaudiana |
| US9877501B2 (en) | 2011-06-03 | 2018-01-30 | Purecircle Sdn Bhd | Stevia composition |
| US9894922B2 (en) | 2011-05-18 | 2018-02-20 | Purecircle Sdn Bhd | Glucosyl rebaudioside C |
| US10004245B2 (en) | 2009-11-12 | 2018-06-26 | Purecircle Sdn Bhd | Granulation of a stevia sweetener |
| US10021899B2 (en) | 2011-05-31 | 2018-07-17 | Purecircle Sdn Bhd | Stevia composition |
| US10362797B2 (en) | 2011-02-10 | 2019-07-30 | Purecircle Sdn Bhd | Stevia composition |
| US10480019B2 (en) | 2011-08-10 | 2019-11-19 | Purecircle Sdn Bhd | Process for producing high-purity rubusoside |
| US10485257B2 (en) | 2012-05-22 | 2019-11-26 | Purecircle Sdn Bhd | Method of making steviol glycosides |
| US10602762B2 (en) | 2011-02-17 | 2020-03-31 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US10696706B2 (en) | 2010-03-12 | 2020-06-30 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
| US10780170B2 (en) | 2013-06-07 | 2020-09-22 | Purecircle Sdn Bhd | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US10952458B2 (en) | 2013-06-07 | 2021-03-23 | Purecircle Usa Inc | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| JPWO2021220948A1 (enrdf_load_stackoverflow) * | 2020-04-27 | 2021-11-04 | ||
| US11202461B2 (en) | 2014-09-02 | 2021-12-21 | Purecircle Sdn Bhd | Stevia extracts |
| US11291232B2 (en) | 2010-12-13 | 2022-04-05 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
| US11464246B2 (en) | 2011-09-07 | 2022-10-11 | Purecircle Sdn Bhd | Highly soluble Stevia sweetener |
| US11647771B2 (en) | 2015-10-26 | 2023-05-16 | Purecircle Usa Inc. | Steviol glycoside compositions |
| US11653686B2 (en) | 2015-12-15 | 2023-05-23 | Purecircle Usa Inc. | Steviol glycoside compositions |
| US11678685B2 (en) | 2011-02-17 | 2023-06-20 | Purecircle Sdn Bhd | Glucosyl stevia composition |
| US11690391B2 (en) | 2011-02-17 | 2023-07-04 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US11871771B2 (en) | 2011-02-17 | 2024-01-16 | Purecircle Sdn Bhd | Glucosyl Stevia composition |
| US12016355B2 (en) | 2011-02-10 | 2024-06-25 | Purecircle Sdn Bhd | Stevia composition |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5123300A (en) * | 1974-08-19 | 1976-02-24 | Toyo Sugar Refining | Sutebiasaidono bunriseiseihoho |
| JPS5247961A (en) * | 1975-10-16 | 1977-04-16 | Chugai Pharmaceutical Co Ltd | Isorating method of steviocide |
| JPS5430199A (en) * | 1977-08-08 | 1979-03-06 | Sanyo Kokusaku Pulp Co Ltd | Purification of stevia sweetening agnet |
| JPS56137866A (en) * | 1980-03-31 | 1981-10-28 | Toyo Seito Kk | Preparation of steviol glucoside having no bitter component, no puckery component, and no odor component |
-
1980
- 1980-10-30 JP JP15281980A patent/JPS5775992A/ja active Granted
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5123300A (en) * | 1974-08-19 | 1976-02-24 | Toyo Sugar Refining | Sutebiasaidono bunriseiseihoho |
| JPS5247961A (en) * | 1975-10-16 | 1977-04-16 | Chugai Pharmaceutical Co Ltd | Isorating method of steviocide |
| JPS5430199A (en) * | 1977-08-08 | 1979-03-06 | Sanyo Kokusaku Pulp Co Ltd | Purification of stevia sweetening agnet |
| JPS56137866A (en) * | 1980-03-31 | 1981-10-28 | Toyo Seito Kk | Preparation of steviol glucoside having no bitter component, no puckery component, and no odor component |
Cited By (67)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8337927B2 (en) | 2005-10-11 | 2012-12-25 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8790730B2 (en) | 2005-10-11 | 2014-07-29 | Purecircle Usa | Process for manufacturing a sweetener and use thereof |
| US10531683B2 (en) | 2005-10-11 | 2020-01-14 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8334006B2 (en) | 2005-10-11 | 2012-12-18 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
| US8568818B2 (en) | 2009-10-15 | 2013-10-29 | Pure Circle Sdn Bhd | High-purity Rebaudioside D and low-calorie carbonated drink containing the same |
| US8574656B2 (en) | 2009-10-15 | 2013-11-05 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie fruit juice containing the same |
| US8414950B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie table top tablet containing the same |
| US8414952B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie diet cookies containing the same |
| US8414949B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie yogurt containing the same |
| US8414951B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie soy sauce containing the same |
| US8420147B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie cake containing the same |
| US8420146B2 (en) | 2009-10-15 | 2013-04-16 | Purecircle Sdn Bhd | High-purity Rebaudioside D and low-calorie bread containing the same |
| US8507022B2 (en) | 2009-10-15 | 2013-08-13 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie carbonated lemon-flavored beverage containing the same |
| US8512790B2 (en) | 2009-10-15 | 2013-08-20 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie chocolate containing the same |
| US8916138B2 (en) | 2009-10-15 | 2014-12-23 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie tooth paste composition containing the same |
| US8414948B2 (en) | 2009-10-15 | 2013-04-09 | Purecircle Sdn Bhd | High-purity rebaudioside D and low-calorie ice cream containing the same |
| EP2708548A2 (en) | 2009-10-15 | 2014-03-19 | Purecircle SDN BHD | High-Purity Rebaudioside D and Applications |
| US8299224B2 (en) | 2009-10-15 | 2012-10-30 | Purecircle Sdn Bhd | High-purity Rebaudioside D |
| US10004245B2 (en) | 2009-11-12 | 2018-06-26 | Purecircle Sdn Bhd | Granulation of a stevia sweetener |
| US11773125B2 (en) | 2010-03-12 | 2023-10-03 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
| US11155570B2 (en) | 2010-03-12 | 2021-10-26 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
| US10696706B2 (en) | 2010-03-12 | 2020-06-30 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
| US11950611B2 (en) | 2010-12-13 | 2024-04-09 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
| US11291232B2 (en) | 2010-12-13 | 2022-04-05 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
| US12016355B2 (en) | 2011-02-10 | 2024-06-25 | Purecircle Sdn Bhd | Stevia composition |
| US11856974B2 (en) | 2011-02-10 | 2024-01-02 | Purecircle Sdn Bhd | Highly soluble stevia sweetener |
| US11812771B2 (en) | 2011-02-10 | 2023-11-14 | Purecircle Sdn Bhd | Stevia composition |
| US10362797B2 (en) | 2011-02-10 | 2019-07-30 | Purecircle Sdn Bhd | Stevia composition |
| US10602762B2 (en) | 2011-02-17 | 2020-03-31 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US11229228B2 (en) | 2011-02-17 | 2022-01-25 | Purecircle Sdn Bhd | Glucosyl stevia composition |
| US11957144B2 (en) | 2011-02-17 | 2024-04-16 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US8257948B1 (en) | 2011-02-17 | 2012-09-04 | Purecircle Usa | Method of preparing alpha-glucosyl Stevia composition |
| US8318459B2 (en) | 2011-02-17 | 2012-11-27 | Purecircle Usa | Glucosyl stevia composition |
| US10743572B2 (en) | 2011-02-17 | 2020-08-18 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US11871771B2 (en) | 2011-02-17 | 2024-01-16 | Purecircle Sdn Bhd | Glucosyl Stevia composition |
| US9615599B2 (en) | 2011-02-17 | 2017-04-11 | Purecircle Sdn Bhd | Glucosyl stevia composition |
| US12279635B2 (en) | 2011-02-17 | 2025-04-22 | PureCirlce Sdn. Bhd. | Glucosylated steviol glycoside as a flavor |
| US11690391B2 (en) | 2011-02-17 | 2023-07-04 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
| US11678685B2 (en) | 2011-02-17 | 2023-06-20 | Purecircle Sdn Bhd | Glucosyl stevia composition |
| US9894922B2 (en) | 2011-05-18 | 2018-02-20 | Purecircle Sdn Bhd | Glucosyl rebaudioside C |
| US10021899B2 (en) | 2011-05-31 | 2018-07-17 | Purecircle Sdn Bhd | Stevia composition |
| US11712055B2 (en) | 2011-05-31 | 2023-08-01 | Purecircle Sdn Bhd | Stevia composition |
| US11825867B2 (en) | 2011-06-03 | 2023-11-28 | Purecircle Sdn Bhd | Stevia composition |
| US9877501B2 (en) | 2011-06-03 | 2018-01-30 | Purecircle Sdn Bhd | Stevia composition |
| US9771434B2 (en) | 2011-06-23 | 2017-09-26 | Purecircle Sdn Bhd | Products from stevia rebaudiana |
| US11279773B2 (en) | 2011-06-23 | 2022-03-22 | Purecircle Sdn Bhd | Products from Stevia rabaudiana |
| US10480019B2 (en) | 2011-08-10 | 2019-11-19 | Purecircle Sdn Bhd | Process for producing high-purity rubusoside |
| US11464246B2 (en) | 2011-09-07 | 2022-10-11 | Purecircle Sdn Bhd | Highly soluble Stevia sweetener |
| US11957149B2 (en) | 2011-09-07 | 2024-04-16 | Purecircle Sdn Bhd | Highly soluble stevia sweetener |
| US10485257B2 (en) | 2012-05-22 | 2019-11-26 | Purecircle Sdn Bhd | Method of making steviol glycosides |
| US11542537B2 (en) | 2012-05-22 | 2023-01-03 | Purecircle Sdn Bhd | High-purity steviol glycosides |
| US11312984B2 (en) | 2013-05-28 | 2022-04-26 | Purecircle Sdn Bhd | High-purity steviol glycosides |
| US9752174B2 (en) | 2013-05-28 | 2017-09-05 | Purecircle Sdn Bhd | High-purity steviol glycosides |
| US12011017B2 (en) | 2013-06-07 | 2024-06-18 | Purecircle Usa Inc. | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US11957756B2 (en) | 2013-06-07 | 2024-04-16 | Purecircle Sdn Bhd | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US10780170B2 (en) | 2013-06-07 | 2020-09-22 | Purecircle Sdn Bhd | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US10952458B2 (en) | 2013-06-07 | 2021-03-23 | Purecircle Usa Inc | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
| US11856972B2 (en) | 2014-09-02 | 2024-01-02 | Purecircle Sdn Bhd | Stevia extracts |
| US12295391B2 (en) | 2014-09-02 | 2025-05-13 | Purecircle Usa Inc. | Stevia extracts enriched in rebaudioside D, E, N and/or O and process for the preparation thereof |
| US11202461B2 (en) | 2014-09-02 | 2021-12-21 | Purecircle Sdn Bhd | Stevia extracts |
| US11230567B2 (en) | 2014-09-02 | 2022-01-25 | Purecircle Usa Inc. | Stevia extracts enriched in rebaudioside D, E, N and/or O and process for the preparation thereof |
| CN105037459A (zh) * | 2015-07-23 | 2015-11-11 | 蚌埠市华东生物科技有限公司 | 一种能提高甜菊糖苷精制效率的絮凝剂 |
| US11647771B2 (en) | 2015-10-26 | 2023-05-16 | Purecircle Usa Inc. | Steviol glycoside compositions |
| US11653686B2 (en) | 2015-12-15 | 2023-05-23 | Purecircle Usa Inc. | Steviol glycoside compositions |
| WO2021220948A1 (ja) * | 2020-04-27 | 2021-11-04 | サントリーホールディングス株式会社 | ステビオール配糖体組成物の製造方法 |
| CN115996642A (zh) * | 2020-04-27 | 2023-04-21 | 三得利控股株式会社 | 甜菊醇糖苷组合物的制造方法 |
| JPWO2021220948A1 (enrdf_load_stackoverflow) * | 2020-04-27 | 2021-11-04 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0245637B2 (enrdf_load_stackoverflow) | 1990-10-11 |
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