JPS5767571A - Production of thiol carbamate derivative - Google Patents

Production of thiol carbamate derivative

Info

Publication number
JPS5767571A
JPS5767571A JP55142582A JP14258280A JPS5767571A JP S5767571 A JPS5767571 A JP S5767571A JP 55142582 A JP55142582 A JP 55142582A JP 14258280 A JP14258280 A JP 14258280A JP S5767571 A JPS5767571 A JP S5767571A
Authority
JP
Japan
Prior art keywords
thiolcarbamate
production
produce
added
aqueous solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP55142582A
Other languages
Japanese (ja)
Inventor
Kazuhiko Konno
Atsushi Go
Kiyoshi Sugaya
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Petrochemical Co Ltd
Original Assignee
Mitsubishi Petrochemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Petrochemical Co Ltd filed Critical Mitsubishi Petrochemical Co Ltd
Priority to JP55142582A priority Critical patent/JPS5767571A/en
Publication of JPS5767571A publication Critical patent/JPS5767571A/en
Pending legal-status Critical Current

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  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

PURPOSE: The same amine as that constituting the thiolcarbamate salt as well as a basic substance are added to the reaction system and a thiolcarbamic acid and an α,β-dimethylbenzylchloride are made to react in an aqueous solvent to produce the titled compound, inhibiting side-reactions.
CONSTITUTION: When the reaction of a thiolcarbamate salt of formulaI(R is H, methyl, ethyl; m is 1W2; n is 4W6; M is alkali metal) with α,α-dimethylbenzyl chloride is effected in an aqueous solvent to produce a thiolcarbamate derivative of formula II such as N-(α,α-dimethylbenzylthiolcarbonyl)pyrrolidine, a basic substance such as sodium hydroxide and an amine of formula III, which is the starting material of the thiolcarbamic acid, such as hexamethyleneimine are added by 0.5W1.5mol and 2.0W30mol%/mol of the thiolcarbamate respectively.
COPYRIGHT: (C)1982,JPO&Japio
JP55142582A 1980-10-13 1980-10-13 Production of thiol carbamate derivative Pending JPS5767571A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP55142582A JPS5767571A (en) 1980-10-13 1980-10-13 Production of thiol carbamate derivative

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP55142582A JPS5767571A (en) 1980-10-13 1980-10-13 Production of thiol carbamate derivative

Publications (1)

Publication Number Publication Date
JPS5767571A true JPS5767571A (en) 1982-04-24

Family

ID=15318653

Family Applications (1)

Application Number Title Priority Date Filing Date
JP55142582A Pending JPS5767571A (en) 1980-10-13 1980-10-13 Production of thiol carbamate derivative

Country Status (1)

Country Link
JP (1) JPS5767571A (en)

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