JPS574996A - Preparation of thiophosphoric aminosulfenylamine compound - Google Patents

Preparation of thiophosphoric aminosulfenylamine compound

Info

Publication number
JPS574996A
JPS574996A JP7807280A JP7807280A JPS574996A JP S574996 A JPS574996 A JP S574996A JP 7807280 A JP7807280 A JP 7807280A JP 7807280 A JP7807280 A JP 7807280A JP S574996 A JPS574996 A JP S574996A
Authority
JP
Japan
Prior art keywords
formula
tertiary amine
halide
thiophosphoric
primary amine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP7807280A
Other languages
Japanese (ja)
Inventor
Tetsuyoshi Suzuki
Sunao Imaki
Takezo Nakanome
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Kasei Corp
Original Assignee
Mitsubishi Kasei Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Kasei Corp filed Critical Mitsubishi Kasei Corp
Priority to JP7807280A priority Critical patent/JPS574996A/en
Publication of JPS574996A publication Critical patent/JPS574996A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE: To obtain the titled compound by reacting an aminosulphenyl thiophosphoric halide with a primary amine in the presence of a tertiary amine in an aprotic solvent.
CONSTITUTION: An aminosulfenyl halide shown by the formula I [A is group shown by the formula II (Y1WY6 are H, methyl, or ethyl; K is 0 or 1); shown by the formula III (Z and Z' are lower alkoxy); R1 is alkyl or cycloalkyl; X is halogen] is reacted with a primary amine shown by the formula R2-NH2(R2 is phenyl or lower alkyl) in the presence of a tertiary amine (e.g., triethylamine) in an aprotic solvent (e.g., benzene, n-hexane), to give the titled compound shown by the formula IV. In the amination of the sulfenyl halide, the primary amine is not used also as an acid acceptor, additionally the tertiary amine is used as the acid acceptor. The amount of the tertiary amine used is an amount to give a molar ratio to sulfenyl halide ≥0.8, the reaction temperature is preferably -20W50°C.
COPYRIGHT: (C)1982,JPO&Japio
JP7807280A 1980-06-10 1980-06-10 Preparation of thiophosphoric aminosulfenylamine compound Pending JPS574996A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP7807280A JPS574996A (en) 1980-06-10 1980-06-10 Preparation of thiophosphoric aminosulfenylamine compound

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP7807280A JPS574996A (en) 1980-06-10 1980-06-10 Preparation of thiophosphoric aminosulfenylamine compound

Publications (1)

Publication Number Publication Date
JPS574996A true JPS574996A (en) 1982-01-11

Family

ID=13651634

Family Applications (1)

Application Number Title Priority Date Filing Date
JP7807280A Pending JPS574996A (en) 1980-06-10 1980-06-10 Preparation of thiophosphoric aminosulfenylamine compound

Country Status (1)

Country Link
JP (1) JPS574996A (en)

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