JPS57126428A - Preparation of alkyl chloride - Google Patents

Preparation of alkyl chloride

Info

Publication number
JPS57126428A
JPS57126428A JP1195681A JP1195681A JPS57126428A JP S57126428 A JPS57126428 A JP S57126428A JP 1195681 A JP1195681 A JP 1195681A JP 1195681 A JP1195681 A JP 1195681A JP S57126428 A JPS57126428 A JP S57126428A
Authority
JP
Japan
Prior art keywords
alkyl
reaction
hydrochloride
amine
accelerator
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1195681A
Other languages
Japanese (ja)
Other versions
JPS6128649B2 (en
Inventor
Masao Kitamura
Naoyoshi Okajima
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SHIN NIPPON RIKA KK
New Japan Chemical Co Ltd
Original Assignee
SHIN NIPPON RIKA KK
New Japan Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SHIN NIPPON RIKA KK, New Japan Chemical Co Ltd filed Critical SHIN NIPPON RIKA KK
Priority to JP1195681A priority Critical patent/JPS57126428A/en
Publication of JPS57126428A publication Critical patent/JPS57126428A/en
Publication of JPS6128649B2 publication Critical patent/JPS6128649B2/ja
Granted legal-status Critical Current

Links

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To prepare an alkyl chloride nearly quantitatively, in high purity and extremely high rate of reaction, by reacting a ≥6C aliphatic alcohol with HCl using hydrochloride of an amine having a cyclohexane ring as a reaction accelerator.
CONSTITUTION: A ≥6C alkyl chloride is prepared by the reaction of the corresponding aliphatic alcohol (e.g. hexyl alcohol) with hydrogen chloride using a reaction accelerator comprising the hydrochloride of a cyclohexane ring-containing amine of formulaI(R1 is H or 1W3C alkyl; R2 and R3 are H, 1W3C alkyl or cycloalkyl) or formula II (n is integer 1W3), e.g. cyclohexylamine, dimethylcyclohexylamine, etc. The amount of the amine hydrochloride is 0.1W0.5mol per 1mol of the alcohol. There is no deterioration of the reaction accelerator even after repeated use. The acceleration performance of the accelerator is more than several times that of the known N-containing heterocyclic compounds, aromatic amines, etc.
COPYRIGHT: (C)1982,JPO&Japio
JP1195681A 1981-01-29 1981-01-29 Preparation of alkyl chloride Granted JPS57126428A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP1195681A JPS57126428A (en) 1981-01-29 1981-01-29 Preparation of alkyl chloride

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1195681A JPS57126428A (en) 1981-01-29 1981-01-29 Preparation of alkyl chloride

Publications (2)

Publication Number Publication Date
JPS57126428A true JPS57126428A (en) 1982-08-06
JPS6128649B2 JPS6128649B2 (en) 1986-07-01

Family

ID=11792065

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1195681A Granted JPS57126428A (en) 1981-01-29 1981-01-29 Preparation of alkyl chloride

Country Status (1)

Country Link
JP (1) JPS57126428A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03220138A (en) * 1989-11-16 1991-09-27 Wacker Chemie Gmbh Preparation of halogen alkane

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4597305B2 (en) * 2000-04-06 2010-12-15 花王株式会社 Method for producing alkyl chloride

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH03220138A (en) * 1989-11-16 1991-09-27 Wacker Chemie Gmbh Preparation of halogen alkane

Also Published As

Publication number Publication date
JPS6128649B2 (en) 1986-07-01

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