JPS5692268A - Preparation of active vitamin d3 - Google Patents
Preparation of active vitamin d3Info
- Publication number
- JPS5692268A JPS5692268A JP16946579A JP16946579A JPS5692268A JP S5692268 A JPS5692268 A JP S5692268A JP 16946579 A JP16946579 A JP 16946579A JP 16946579 A JP16946579 A JP 16946579A JP S5692268 A JPS5692268 A JP S5692268A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- agent
- hydroxycholest
- previtamin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- QYSXJUFSXHHAJI-YRZJJWOYSA-N vitamin D3 Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C\C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-YRZJJWOYSA-N 0.000 title 1
- 229940021056 vitamin d3 Drugs 0.000 title 1
- 239000003795 chemical substances by application Substances 0.000 abstract 4
- 150000001875 compounds Chemical class 0.000 abstract 3
- TWWQSIQFQAWJJU-GPPBBECHSA-N (6r)-6-[(8s,9s,10r,13r,14s,17r)-10,13-dimethyl-2,3,4,7,8,9,11,12,14,15,16,17-dodecahydro-1h-cyclopenta[a]phenanthren-17-yl]-2-methylheptan-1-ol Chemical compound C1C=C2CCCC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(CO)C)[C@@]1(C)CC2 TWWQSIQFQAWJJU-GPPBBECHSA-N 0.000 abstract 2
- 125000004453 alkoxycarbonyl group Chemical group 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- YUGCAAVRZWBXEQ-WHTXLNIXSA-N previtamin D3 Chemical compound C=1([C@@H]2CC[C@@H]([C@]2(CCC=1)C)[C@H](C)CCCC(C)C)\C=C/C1=C(C)CC[C@H](O)C1 YUGCAAVRZWBXEQ-WHTXLNIXSA-N 0.000 abstract 2
- PAKKXLLOIJSLLK-DXEOSGPYSA-N (6r)-6-[(9s,10r,13r,14r,17r)-10,13-dimethyl-2,3,4,9,11,12,14,15,16,17-decahydro-1h-cyclopenta[a]phenanthren-17-yl]-2-methylheptan-1-ol Chemical compound C1CCC[C@]2(C)[C@@H](CC[C@@]3([C@@H]([C@H](C)CCCC(CO)C)CC[C@H]33)C)C3=CC=C21 PAKKXLLOIJSLLK-DXEOSGPYSA-N 0.000 abstract 1
- 125000005194 alkoxycarbonyloxy group Chemical group 0.000 abstract 1
- 125000000746 allylic group Chemical group 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 230000001678 irradiating effect Effects 0.000 abstract 1
- 125000006239 protecting group Chemical group 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/55—Design of synthesis routes, e.g. reducing the use of auxiliary or protecting groups
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP16946579A JPS5692268A (en) | 1979-12-27 | 1979-12-27 | Preparation of active vitamin d3 |
DE8080303732T DE3070985D1 (en) | 1979-10-23 | 1980-10-22 | Process for the preparation of active-type vitamin d3 compounds and of the cholesta-5,7-diene precursors, and products so obtained |
CA000362937A CA1160217A (en) | 1979-10-23 | 1980-10-22 | Process for the preparation of active-type vitamin d.sub.3 compounds |
DK447380A DK160817C (da) | 1979-10-23 | 1980-10-22 | Fremgangsmaade til fremstilling af vitamin d3 forbindelser |
EP80303732A EP0028484B1 (en) | 1979-10-23 | 1980-10-22 | Process for the preparation of active-type vitamin d3 compounds and of the cholesta-5,7-diene precursors, and products so obtained |
US06/371,870 US4388243A (en) | 1979-10-23 | 1982-04-26 | Process for the preparation of active-type vitamin D3 compounds |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP16946579A JPS5692268A (en) | 1979-12-27 | 1979-12-27 | Preparation of active vitamin d3 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5692268A true JPS5692268A (en) | 1981-07-25 |
JPS6251266B2 JPS6251266B2 (enrdf_load_stackoverflow) | 1987-10-29 |
Family
ID=15887063
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP16946579A Granted JPS5692268A (en) | 1979-10-23 | 1979-12-27 | Preparation of active vitamin d3 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5692268A (enrdf_load_stackoverflow) |
-
1979
- 1979-12-27 JP JP16946579A patent/JPS5692268A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS6251266B2 (enrdf_load_stackoverflow) | 1987-10-29 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
EP0198901A1 (en) | PROCESS FOR THE PREPARATION OF 1-g (a) -HYDROXYVITAMIN D COMPOUNDS | |
AU4867485A (en) | Method for preparing 1-hydroxyvitamin d compounds | |
CA1160217A (en) | Process for the preparation of active-type vitamin d.sub.3 compounds | |
US5250523A (en) | Side chain unsaturated 1α-hydroxyvitanim D homologs | |
Crimmins et al. | Total synthesis of milbemycin. beta. 3 | |
Sakurai et al. | PHOTOCHEMISTRY OF DIBENZO-1, 1, 2, 2, 3, 3-HEXAMETHYL-1, 2, 3-TRISILACYCLOHEPTA-4, 6-DIENE AND THE GERMANIUM ANALOG. GENERATION OF TETRAMETHYLDISILENE BY FREE-RADICAL DISPROPORTIONATION AND THE FIRST SPECTROSCOPIC DETECTION OF DIMETHYLGERMYLENE | |
JPS5740419A (en) | Preparation of cumene | |
JPS5692268A (en) | Preparation of active vitamin d3 | |
GB2058793A (en) | Process for preparing 1-hydroxylated vitamin d compounds from 5,6-transvitamin d compounds | |
Hagiwara et al. | Organic reaction without solvent. Efficient synthesis of thiocarbonylimidazolide | |
JPS5692266A (en) | Preparation of active vitamin d3 | |
JPS5622763A (en) | 25-hydroxy-24-oxovitamin d3, or its hydroxyl-protecting derivative and its preparation | |
JPS5692267A (en) | Preparation of active vitamin d3 | |
JPS5785387A (en) | Preparation of 1-(-5'-oxohexyl)-3,7-dimethylxanthine | |
Vanelle et al. | First Tetrakis-SRN1 Reaction in Naphthoquinone Series | |
JPS577446A (en) | Production of succinosuccinic dialkyl ester | |
CA1077028A (en) | PROCESS FOR PREPARATION OF 1.alpha.,2.alpha.-DIHYDROXY-CHOLECALCIFEROL | |
Navarro et al. | Synthesis of [14, 14, 14-2H3] 12-hydroxytetradecanoic acid and [13, 14-2H2] 11-hydroxytetradecanoic acid useful as tracers to study a (11E)-desaturation reaction in Spodoptera littoralis | |
JPS5732250A (en) | Simultaneous preparation of urethane and carbonic acid ester | |
JPS5626847A (en) | Preparation of substituted salicylic acid derivative | |
Mukaiyama et al. | The stereoselective synthesis of C18-juvenile hormone analogue. | |
JPS56120627A (en) | Selective reduction of compound having acetylenic unsaturated bond | |
JPS55127333A (en) | Preparation of substituted phenols | |
JPS5277021A (en) | Preparation of s-chlorobensaldenyde | |
JPS56120626A (en) | Selective reduction of compound having acetylenic unsaturated bond |