JPS5692110A - Defluorinating method of phosphoric acid - Google Patents
Defluorinating method of phosphoric acidInfo
- Publication number
- JPS5692110A JPS5692110A JP16822179A JP16822179A JPS5692110A JP S5692110 A JPS5692110 A JP S5692110A JP 16822179 A JP16822179 A JP 16822179A JP 16822179 A JP16822179 A JP 16822179A JP S5692110 A JPS5692110 A JP S5692110A
- Authority
- JP
- Japan
- Prior art keywords
- org
- solvent
- phosphoric acid
- liq
- fluorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To remove fluorine efficiently and inexpensively from fluorine-contg. phosphoric acid of a prescribed concn. by bringing the acid into contact with a prscribed org. solvent followed by liq.-liq. separation.
CONSTITUTION: Fluorine-contg. phosphoric acid of ≤45wt% concn. as P2O5 is brought into contact with an org. solvent which does not practically extract phosphoric acid of such a concn., and liq.-liq. separation is carried out to remove the fluorine in the acid. As the org. solvent a regenerated solvent is advantageously used, and it is obtd. by bringing the liq.-liq. separated org. layer into contact with water or a soln. of inorg. salts capable of forming slightly soluble fluoride to remove the fluoride in the org. solvent. Butyl acetate or isopropyl ether is preferably used as the org. solvent. Desirable fluorine-contg. phosphoric acid is primarily purified phosphoric acid obtd. by using the washing water of the solvent in a back extracting process when wet process phosphoric acid is extracted with an org. solvent, and the org. layer is washed and back extracted with water.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP16822179A JPS5933528B2 (en) | 1979-12-26 | 1979-12-26 | Method for removing fluoridation in phosphoric acid |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP16822179A JPS5933528B2 (en) | 1979-12-26 | 1979-12-26 | Method for removing fluoridation in phosphoric acid |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5692110A true JPS5692110A (en) | 1981-07-25 |
JPS5933528B2 JPS5933528B2 (en) | 1984-08-16 |
Family
ID=15864024
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP16822179A Expired JPS5933528B2 (en) | 1979-12-26 | 1979-12-26 | Method for removing fluoridation in phosphoric acid |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5933528B2 (en) |
-
1979
- 1979-12-26 JP JP16822179A patent/JPS5933528B2/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS5933528B2 (en) | 1984-08-16 |
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