JPS5626886A - Preparation of glycidyl vinyl ether - Google Patents
Preparation of glycidyl vinyl etherInfo
- Publication number
- JPS5626886A JPS5626886A JP10122779A JP10122779A JPS5626886A JP S5626886 A JPS5626886 A JP S5626886A JP 10122779 A JP10122779 A JP 10122779A JP 10122779 A JP10122779 A JP 10122779A JP S5626886 A JPS5626886 A JP S5626886A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- reaction
- step reaction
- alkali
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Epoxy Compounds (AREA)
Abstract
PURPOSE: To prepare the titled compound useful as a raw material of various reactions, economically, in high yield, by the three-step reaction of ethylene chlorohydrin and epichlorohydrin, wherein the third step reaction is carried out in a specific solvent under specific reaction conditions.
CONSTITUTION: Ethylene chlorohydrin of formula I is reacted with epichlorohydrin of formula II to afford a compound of formula III, which is made to react in the second step reaction with an alkali (pref. an alkali metal hydroxide) as a dehydrochlorinating agent to yield a compound of formula IV and then a compound of formula V (the third step reaction). The third step reaction is carried out at 150W 200°C in a solvent having a boiling point of 160W200°C and capable of dissolving at least a part of said alkali at the reaction temperature, by supplying the compound of formula IV little by little to the reaction system and distilling out the products from the reaction system. By this process, the titled compound of formula V can be prepared in high yield, in an industrial scale, from low-cost raw materials.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP10122779A JPS5626886A (en) | 1979-08-10 | 1979-08-10 | Preparation of glycidyl vinyl ether |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP10122779A JPS5626886A (en) | 1979-08-10 | 1979-08-10 | Preparation of glycidyl vinyl ether |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5626886A true JPS5626886A (en) | 1981-03-16 |
JPS6344151B2 JPS6344151B2 (en) | 1988-09-02 |
Family
ID=14295004
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP10122779A Granted JPS5626886A (en) | 1979-08-10 | 1979-08-10 | Preparation of glycidyl vinyl ether |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5626886A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011121913A (en) * | 2009-12-11 | 2011-06-23 | Nippon Synthetic Chem Ind Co Ltd:The | Method for producing vinylimidazole-based compound |
CN103145648A (en) * | 2013-03-13 | 2013-06-12 | 安徽新远化工有限公司 | Synthetic method of allyl glycidyl ether |
-
1979
- 1979-08-10 JP JP10122779A patent/JPS5626886A/en active Granted
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011121913A (en) * | 2009-12-11 | 2011-06-23 | Nippon Synthetic Chem Ind Co Ltd:The | Method for producing vinylimidazole-based compound |
CN103145648A (en) * | 2013-03-13 | 2013-06-12 | 安徽新远化工有限公司 | Synthetic method of allyl glycidyl ether |
Also Published As
Publication number | Publication date |
---|---|
JPS6344151B2 (en) | 1988-09-02 |
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