JPS5620537A - Preparation of p-tertiary-butylbenzaldehyde - Google Patents

Preparation of p-tertiary-butylbenzaldehyde

Info

Publication number
JPS5620537A
JPS5620537A JP9747879A JP9747879A JPS5620537A JP S5620537 A JPS5620537 A JP S5620537A JP 9747879 A JP9747879 A JP 9747879A JP 9747879 A JP9747879 A JP 9747879A JP S5620537 A JPS5620537 A JP S5620537A
Authority
JP
Japan
Prior art keywords
nitrate
ceric
mixture
fatty acid
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP9747879A
Other languages
Japanese (ja)
Other versions
JPS6157818B2 (en
Inventor
Shigeru Torii
Mitsuo Akata
Toshibumi Shirakawa
Shoji Nakane
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Otsuka Chemical Co Ltd
Soda Aromatic Co Ltd
Otsuka Kagaku Yakuhin KK
Soda Koryo KK
Original Assignee
Otsuka Chemical Co Ltd
Soda Aromatic Co Ltd
Otsuka Kagaku Yakuhin KK
Soda Koryo KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Otsuka Chemical Co Ltd, Soda Aromatic Co Ltd, Otsuka Kagaku Yakuhin KK, Soda Koryo KK filed Critical Otsuka Chemical Co Ltd
Priority to JP9747879A priority Critical patent/JPS5620537A/en
Priority to GB8024137A priority patent/GB2060612B/en
Priority to DE3028757A priority patent/DE3028757C2/en
Priority to FR8016779A priority patent/FR2462411A1/en
Priority to CH581280A priority patent/CH644575A5/en
Publication of JPS5620537A publication Critical patent/JPS5620537A/en
Publication of JPS6157818B2 publication Critical patent/JPS6157818B2/ja
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00—Electrolytic production of organic compounds
    • C25B3/20—Processes
    • C25B3/23—Oxidation

Abstract

PURPOSE: To obtain the titled compound, useful as a starting material of perfumes, in high yield without the formation of by-products, by repeating the following processes: electrolytic oxidation of cerous nitrate into ceric nitrate and oxidation of p-tert-butyltoluene with ceric nitrate.
CONSTITUTION: Water containing nitrate ion or a mixture of water and a lower fatty acid is charged in the cathode cell, and a mixture of cerous (ammonium) nitrate, water and lower fatty acid in the anode cell. The cells are separated from each other with a permeably membrane, pref. an ion exchange membrane etc. The mixture is electrolyzed to give a mixture of the lower fatty acid and water containing ceric (ammonium) nitrate. Using the solution containing ceric nitrite, p-tert- butyltoluene is oxidized at 50W120°C to give the objective compound. Ceric salt is regenerated by the electrolytic oxidation of the solution containing cerous nitrate after separation of the objective compound.
COPYRIGHT: (C)1981,JPO&Japio
JP9747879A 1979-07-30 1979-07-30 Preparation of p-tertiary-butylbenzaldehyde Granted JPS5620537A (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP9747879A JPS5620537A (en) 1979-07-30 1979-07-30 Preparation of p-tertiary-butylbenzaldehyde
GB8024137A GB2060612B (en) 1979-07-30 1980-07-23 Process for preparing p-tert-butyl benzaldehyde
DE3028757A DE3028757C2 (en) 1979-07-30 1980-07-29 Process for the preparation of p-tert-butylbenzaldehyde
FR8016779A FR2462411A1 (en) 1979-07-30 1980-07-30 PROCESS FOR THE PREPARATION OF P-TERTIOBUTYLBENZALDEHYDE
CH581280A CH644575A5 (en) 1979-07-30 1980-07-30 METHOD FOR PRODUCING P-TERT.-BUTYLBENZALDEHYDE.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP9747879A JPS5620537A (en) 1979-07-30 1979-07-30 Preparation of p-tertiary-butylbenzaldehyde

Publications (2)

Publication Number Publication Date
JPS5620537A true JPS5620537A (en) 1981-02-26
JPS6157818B2 JPS6157818B2 (en) 1986-12-09

Family

ID=14193390

Family Applications (1)

Application Number Title Priority Date Filing Date
JP9747879A Granted JPS5620537A (en) 1979-07-30 1979-07-30 Preparation of p-tertiary-butylbenzaldehyde

Country Status (5)

Country Link
JP (1) JPS5620537A (en)
CH (1) CH644575A5 (en)
DE (1) DE3028757C2 (en)
FR (1) FR2462411A1 (en)
GB (1) GB2060612B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60500178A (en) * 1982-12-29 1985-02-07 ジボーダン　―　ルール（アンテルナショナル）ソシエテ　アノニム Method for producing aldehydes
JPS63143544A (en) * 1986-12-08 1988-06-15 Konica Corp Silver halide photographic sensitive material having significant color mixing preventing effect
CN106319553A (en) * 2015-07-02 2017-01-11 中国科学院大连化学物理研究所 Method for obtaining Ce(IV) by conducting photoelectric catalysis oxidation on Ce(III), Ce(IV) and application

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9319945D0 (en) * 1993-09-28 1993-11-17 Solvay Interox Ltd Oxidation of alkylaromatic compounds

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3346622A (en) * 1965-07-15 1967-10-10 Gulf Research Development Co Preparation of an aromatic ester from an alkyl-aromatic compound and a carboxylic acid in the presence of a tetravalent cerium salt and an inhibitor
GB1203434A (en) * 1967-10-23 1970-08-26 Ici Ltd Oxidation of organic materials

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60500178A (en) * 1982-12-29 1985-02-07 ジボーダン　―　ルール（アンテルナショナル）ソシエテ　アノニム Method for producing aldehydes
JPS63143544A (en) * 1986-12-08 1988-06-15 Konica Corp Silver halide photographic sensitive material having significant color mixing preventing effect
CN106319553A (en) * 2015-07-02 2017-01-11 中国科学院大连化学物理研究所 Method for obtaining Ce(IV) by conducting photoelectric catalysis oxidation on Ce(III), Ce(IV) and application

Also Published As

Publication number Publication date
GB2060612A (en) 1981-05-07
JPS6157818B2 (en) 1986-12-09
DE3028757A1 (en) 1981-02-05
GB2060612B (en) 1983-09-21
FR2462411A1 (en) 1981-02-13
CH644575A5 (en) 1984-08-15
FR2462411B1 (en) 1984-11-02
DE3028757C2 (en) 1982-09-16

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