JPS56152149A - Gas chromatograph mass spectrograph - Google Patents
Gas chromatograph mass spectrographInfo
- Publication number
- JPS56152149A JPS56152149A JP5419380A JP5419380A JPS56152149A JP S56152149 A JPS56152149 A JP S56152149A JP 5419380 A JP5419380 A JP 5419380A JP 5419380 A JP5419380 A JP 5419380A JP S56152149 A JPS56152149 A JP S56152149A
- Authority
- JP
- Japan
- Prior art keywords
- circuit
- timer
- resistor
- output
- integrating circuit
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
- H01J49/0495—Vacuum locks; Valves
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J49/00—Particle spectrometers or separator tubes
- H01J49/02—Details
- H01J49/022—Circuit arrangements, e.g. for generating deviation currents or voltages ; Components associated with high voltage supply
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
- G01N30/7206—Mass spectrometers interfaced to gas chromatograph
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Electron Tubes For Measurement (AREA)
Abstract
PURPOSE:To enable precise exhaust separation of solvent even if the degree of vacuum is changed due to the changes of column temperature or the flow of carrier gas. CONSTITUTION:A differential circuit 20 is connected through a resistor R1 to the output of a vacuum measuring circuit 12 while an integrating circuit 30 is connected through a resistor R3. Diodes D1, D2 and timer 16 are connected through a resistor R6 to the output of the integrating circuit 30. A transistor Tr1 is connected through an inverter 17 to the output of the timer 16, and a pre-cut bulb 4 is connected to the collector of said transistor Tr1. When connecting the differentiating circuit 20 and the integrating circuit 30 in series and operating the timer 16, the variation of base line and the noise due to the column temperature change can be neglected thereby only the solvent peak can be detected.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55054193A JPS6041824B2 (en) | 1980-04-25 | 1980-04-25 | Gas chromatograph mass spectrometer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55054193A JPS6041824B2 (en) | 1980-04-25 | 1980-04-25 | Gas chromatograph mass spectrometer |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS56152149A true JPS56152149A (en) | 1981-11-25 |
JPS6041824B2 JPS6041824B2 (en) | 1985-09-19 |
Family
ID=12963697
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55054193A Expired JPS6041824B2 (en) | 1980-04-25 | 1980-04-25 | Gas chromatograph mass spectrometer |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6041824B2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58161236A (en) * | 1982-03-19 | 1983-09-24 | Hitachi Ltd | Mass spectrometer directly-coupled to gas chromatograph |
US4808819A (en) * | 1987-02-03 | 1989-02-28 | Hitachi, Ltd. | Mass spectrometric apparatus |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62155315U (en) * | 1986-03-25 | 1987-10-02 |
-
1980
- 1980-04-25 JP JP55054193A patent/JPS6041824B2/en not_active Expired
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58161236A (en) * | 1982-03-19 | 1983-09-24 | Hitachi Ltd | Mass spectrometer directly-coupled to gas chromatograph |
JPH0354429B2 (en) * | 1982-03-19 | 1991-08-20 | ||
US4808819A (en) * | 1987-02-03 | 1989-02-28 | Hitachi, Ltd. | Mass spectrometric apparatus |
Also Published As
Publication number | Publication date |
---|---|
JPS6041824B2 (en) | 1985-09-19 |
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