JPS56140940A - Preparation of diol by oxo reaction - Google Patents
Preparation of diol by oxo reactionInfo
- Publication number
- JPS56140940A JPS56140940A JP4371480A JP4371480A JPS56140940A JP S56140940 A JPS56140940 A JP S56140940A JP 4371480 A JP4371480 A JP 4371480A JP 4371480 A JP4371480 A JP 4371480A JP S56140940 A JPS56140940 A JP S56140940A
- Authority
- JP
- Japan
- Prior art keywords
- diol
- solvent
- catalyst
- reaction
- oxo reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain a diol in high yield, by the oxo reaction of a specific hydrocarbon, etc., in a specific solvent in the presence of a cobalt compound and a phosphine as a catalyst, and further the separation of the solvent phase from the reaction mixture through cooling for recycling.
CONSTITUTION: A compound having an intramolecular quaternary or bridge head carbon and a double bond on one side and a double bond, a formly or hydroxyl group on the other side across said carbon, except dicyclopentadiene, is subjected to the oxo reaction in a saturated and/or aromatic hydrocarbon solvent in the presence of a cobalt compound and a phosphine as a catalyst. The resultant reaction mixture is then cooled and separated into a solvent phase containing the catalyst and a diol phase as a reaction product. Thus, the solvent and the catalyst are separated in one step. The solvent phase is recycled to the oxo reaction system, and the aimed diol is obtained in high yield.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP4371480A JPS56140940A (en) | 1980-04-03 | 1980-04-03 | Preparation of diol by oxo reaction |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP4371480A JPS56140940A (en) | 1980-04-03 | 1980-04-03 | Preparation of diol by oxo reaction |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS56140940A true JPS56140940A (en) | 1981-11-04 |
Family
ID=12671465
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP4371480A Pending JPS56140940A (en) | 1980-04-03 | 1980-04-03 | Preparation of diol by oxo reaction |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS56140940A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6028953A (en) * | 1983-07-28 | 1985-02-14 | Mitsubishi Petrochem Co Ltd | Preparation of hydroxymethylnorbornane containing polar functional group |
CN115461619A (en) * | 2021-05-31 | 2022-12-09 | Kh新化株式会社 | Pentacyclopentadecane dimethanol preparations |
-
1980
- 1980-04-03 JP JP4371480A patent/JPS56140940A/en active Pending
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6028953A (en) * | 1983-07-28 | 1985-02-14 | Mitsubishi Petrochem Co Ltd | Preparation of hydroxymethylnorbornane containing polar functional group |
JPH0412259B2 (en) * | 1983-07-28 | 1992-03-04 | Mitsubishi Petrochemical Co | |
CN115461619A (en) * | 2021-05-31 | 2022-12-09 | Kh新化株式会社 | Pentacyclopentadecane dimethanol preparations |
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