JPS5598199A - Preparation of 25-hydroxy cholesta-1,4,6-trien-3-one - Google Patents
Preparation of 25-hydroxy cholesta-1,4,6-trien-3-oneInfo
- Publication number
- JPS5598199A JPS5598199A JP291979A JP291979A JPS5598199A JP S5598199 A JPS5598199 A JP S5598199A JP 291979 A JP291979 A JP 291979A JP 291979 A JP291979 A JP 291979A JP S5598199 A JPS5598199 A JP S5598199A
- Authority
- JP
- Japan
- Prior art keywords
- formula
- compound
- oxidized
- cholesta
- trien
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- HIRJUBYXEOKIMY-REEZCCHISA-N (8s,9s,10r,13r,14s,17r)-17-[(2r)-6-hydroxy-6-methylheptan-2-yl]-10,13-dimethyl-8,9,11,12,14,15,16,17-octahydrocyclopenta[a]phenanthren-3-one Chemical compound C1=CC2=CC(=O)C=C[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@@H](CCCC(C)(C)O)C)[C@@]1(C)CC2 HIRJUBYXEOKIMY-REEZCCHISA-N 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 5
- SMEROWZSTRWXGI-UHFFFAOYSA-N Lithocholsaeure Natural products C1CC2CC(O)CCC2(C)C2C1C1CCC(C(CCC(O)=O)C)C1(C)CC2 SMEROWZSTRWXGI-UHFFFAOYSA-N 0.000 abstract 2
- 239000012280 lithium aluminium hydride Substances 0.000 abstract 2
- SMEROWZSTRWXGI-HVATVPOCSA-N lithocholic acid Chemical compound C([C@H]1CC2)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC(O)=O)C)[C@@]2(C)CC1 SMEROWZSTRWXGI-HVATVPOCSA-N 0.000 abstract 2
- LEHBURLTIWGHEM-UHFFFAOYSA-N pyridinium chlorochromate Chemical compound [O-][Cr](Cl)(=O)=O.C1=CC=[NH+]C=C1 LEHBURLTIWGHEM-UHFFFAOYSA-N 0.000 abstract 2
- UPZFLZYXYGBAPL-UHFFFAOYSA-N 2-ethyl-2-methyl-1,3-dioxolane Chemical compound CCC1(C)OCCO1 UPZFLZYXYGBAPL-UHFFFAOYSA-N 0.000 abstract 1
- 239000003810 Jones reagent Substances 0.000 abstract 1
- 229910010084 LiAlH4 Inorganic materials 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- -1 lithium aluminum hydride Chemical compound 0.000 abstract 1
- 150000007522 mineralic acids Chemical class 0.000 abstract 1
- 150000004967 organic peroxy acids Chemical class 0.000 abstract 1
- 125000006239 protecting group Chemical group 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
- LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 1
- RIOQSEWOXXDEQQ-UHFFFAOYSA-N triphenylphosphine Substances C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 RIOQSEWOXXDEQQ-UHFFFAOYSA-N 0.000 abstract 1
- QYSXJUFSXHHAJI-YRZJJWOYSA-N vitamin D3 Chemical class C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C\C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-YRZJJWOYSA-N 0.000 abstract 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/55—Design of synthesis routes, e.g. reducing the use of auxiliary or protecting groups
Landscapes
- Steroid Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP291979A JPS5598199A (en) | 1979-01-17 | 1979-01-17 | Preparation of 25-hydroxy cholesta-1,4,6-trien-3-one |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP291979A JPS5598199A (en) | 1979-01-17 | 1979-01-17 | Preparation of 25-hydroxy cholesta-1,4,6-trien-3-one |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5598199A true JPS5598199A (en) | 1980-07-25 |
| JPS6144879B2 JPS6144879B2 (enrdf_load_stackoverflow) | 1986-10-04 |
Family
ID=11542753
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP291979A Granted JPS5598199A (en) | 1979-01-17 | 1979-01-17 | Preparation of 25-hydroxy cholesta-1,4,6-trien-3-one |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5598199A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01117895A (ja) * | 1987-10-29 | 1989-05-10 | Teijin Ltd | コレスター１，４，６−トリエン−３−オン類の製造法 |
| JPH0578388A (ja) * | 1982-05-26 | 1993-03-30 | Wisconsin Alumni Res Found | ２５，２６，２７−トリノル−１α，２β−エポキシコレスタ−４，６−ジエン−３−オン−２４−酸メチルエステル |
-
1979
- 1979-01-17 JP JP291979A patent/JPS5598199A/ja active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0578388A (ja) * | 1982-05-26 | 1993-03-30 | Wisconsin Alumni Res Found | ２５，２６，２７−トリノル−１α，２β−エポキシコレスタ−４，６−ジエン−３−オン−２４−酸メチルエステル |
| JPH01117895A (ja) * | 1987-10-29 | 1989-05-10 | Teijin Ltd | コレスター１，４，６−トリエン−３−オン類の製造法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6144879B2 (enrdf_load_stackoverflow) | 1986-10-04 |
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