JPS5598178A - Preparation of delta-gluconolactone - Google Patents
Preparation of delta-gluconolactoneInfo
- Publication number
- JPS5598178A JPS5598178A JP228179A JP228179A JPS5598178A JP S5598178 A JPS5598178 A JP S5598178A JP 228179 A JP228179 A JP 228179A JP 228179 A JP228179 A JP 228179A JP S5598178 A JPS5598178 A JP S5598178A
- Authority
- JP
- Japan
- Prior art keywords
- acid
- glucose
- solvent
- gluconolactone
- organic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Pyrane Compounds (AREA)
Abstract
PURPOSE: To obtain δ-gluconolactone useful as a food additive for confectionery leavening agents and paste products simply in high yield, by treating the crude oxidation product of glucose with an acid.
CONSTITUTION: Glucose (G) is oxidized with molecular oxygen in the presence of an organic solvent, e.g. diethyl ether acetonitrile, methanol, or dimethyl formamide, in an amount of 20W200 times that of G and a catalyst comprising palladium or platinum. The resulting reaction mixture or a crude product after distilling off the solvent is dissolved in a suitable solvent, and treated with an inorganic acid, e.g. hydrochloric acid, an organic acid, e.g. p-toluenesulfonic acid, or a strongly acidic ion exchange resin to form the objective compound.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP228179A JPS5598178A (en) | 1979-01-16 | 1979-01-16 | Preparation of delta-gluconolactone |
DE2936652A DE2936652C2 (en) | 1978-09-14 | 1979-09-11 | Process for the production of gluconic acid delta lactone |
GB7931828A GB2031884B (en) | 1978-09-14 | 1979-09-13 | Process for producing glucono-delta-lactone from glucose |
US06/075,457 US4256645A (en) | 1978-09-14 | 1979-09-14 | Process for producing glucona-delta-lactone from glucose |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP228179A JPS5598178A (en) | 1979-01-16 | 1979-01-16 | Preparation of delta-gluconolactone |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5598178A true JPS5598178A (en) | 1980-07-25 |
JPS5725552B2 JPS5725552B2 (en) | 1982-05-29 |
Family
ID=11524977
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP228179A Granted JPS5598178A (en) | 1978-09-14 | 1979-01-16 | Preparation of delta-gluconolactone |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5598178A (en) |
-
1979
- 1979-01-16 JP JP228179A patent/JPS5598178A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS5725552B2 (en) | 1982-05-29 |
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