JPS5540734A - Controlling of mooney viscosity of polybutadiene - Google Patents
Controlling of mooney viscosity of polybutadieneInfo
- Publication number
- JPS5540734A JPS5540734A JP11438978A JP11438978A JPS5540734A JP S5540734 A JPS5540734 A JP S5540734A JP 11438978 A JP11438978 A JP 11438978A JP 11438978 A JP11438978 A JP 11438978A JP S5540734 A JPS5540734 A JP S5540734A
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- lithium
- mooney viscosity
- polybutadiene
- polymerizing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Polymerization Catalysts (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
Abstract
PURPOSE: To prepare a vinyl-containing polybutadiene having excellent cold-flow characteristic, and easily controllable Mooney viscosity, by polymerizing butadiene in the presence of a polar compound, a branching agent. a lithium catalyst, and a specific amount of an allene based on the catalyst.
CONSTITUTION: The objective polymer containing ≥30mol% of vinyl group, based on the monomer units, is prepared by polymerizing (A) 1,3-butadiene, in the presence of (B) one or more polar compounds such as ethers, amines, phosphines, sulfides, etc., (C) a branching agent such as a polyvinyl aromatic compound, (D) a lithium-based catalyst such as n-butyl lithium, and (E) 1W1/35mol, based on 1mol of the (D) component, of an allene derivative of formula (R is H or 1W5C hydrocarbon), pref. at 25W90°C.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11438978A JPS5540734A (en) | 1978-09-18 | 1978-09-18 | Controlling of mooney viscosity of polybutadiene |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11438978A JPS5540734A (en) | 1978-09-18 | 1978-09-18 | Controlling of mooney viscosity of polybutadiene |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5540734A true JPS5540734A (en) | 1980-03-22 |
JPS6139961B2 JPS6139961B2 (en) | 1986-09-06 |
Family
ID=14636443
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP11438978A Granted JPS5540734A (en) | 1978-09-18 | 1978-09-18 | Controlling of mooney viscosity of polybutadiene |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5540734A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5785809A (en) * | 1980-11-18 | 1982-05-28 | Asahi Chem Ind Co Ltd | Production of conjugated diene polymer |
JPS59176311A (en) * | 1983-03-25 | 1984-10-05 | Japan Synthetic Rubber Co Ltd | Production of polybutadiene |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3301840A (en) * | 1964-09-17 | 1967-01-31 | Phillips Petroleum Co | Preparation of polymers of conjugated dienes using organolithium/polar compound catalyst systems |
JPS4854188A (en) * | 1971-11-04 | 1973-07-30 | ||
JPS4938105A (en) * | 1972-08-18 | 1974-04-09 | ||
JPS5166385A (en) * | 1974-11-29 | 1976-06-08 | Japan Synthetic Rubber Co Ltd | KYOYAKUJIOREFUINKEIJUGOTAINO SEIZOHO |
JPS5183685A (en) * | 1974-12-23 | 1976-07-22 | Michelin & Cie | Yoekijugoho mataha kyojugoho |
-
1978
- 1978-09-18 JP JP11438978A patent/JPS5540734A/en active Granted
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3301840A (en) * | 1964-09-17 | 1967-01-31 | Phillips Petroleum Co | Preparation of polymers of conjugated dienes using organolithium/polar compound catalyst systems |
JPS4854188A (en) * | 1971-11-04 | 1973-07-30 | ||
JPS4938105A (en) * | 1972-08-18 | 1974-04-09 | ||
JPS5166385A (en) * | 1974-11-29 | 1976-06-08 | Japan Synthetic Rubber Co Ltd | KYOYAKUJIOREFUINKEIJUGOTAINO SEIZOHO |
JPS5183685A (en) * | 1974-12-23 | 1976-07-22 | Michelin & Cie | Yoekijugoho mataha kyojugoho |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5785809A (en) * | 1980-11-18 | 1982-05-28 | Asahi Chem Ind Co Ltd | Production of conjugated diene polymer |
JPH0147487B2 (en) * | 1980-11-18 | 1989-10-13 | Asahi Chemical Ind | |
JPS59176311A (en) * | 1983-03-25 | 1984-10-05 | Japan Synthetic Rubber Co Ltd | Production of polybutadiene |
JPH0352761B2 (en) * | 1983-03-25 | 1991-08-13 | Japan Synthetic Rubber Co Ltd |
Also Published As
Publication number | Publication date |
---|---|
JPS6139961B2 (en) | 1986-09-06 |
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