JPS55134137A - Palladium recovering method - Google Patents

Palladium recovering method

Info

Publication number
JPS55134137A
JPS55134137A JP4037279A JP4037279A JPS55134137A JP S55134137 A JPS55134137 A JP S55134137A JP 4037279 A JP4037279 A JP 4037279A JP 4037279 A JP4037279 A JP 4037279A JP S55134137 A JPS55134137 A JP S55134137A
Authority
JP
Japan
Prior art keywords
soln
cpd
arom
org
catalyst
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP4037279A
Other languages
Japanese (ja)
Other versions
JPS6059974B2 (en
Inventor
Hiroshi Itaya
Akinori Shiotani
Motozo Yoshikiyo
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Priority to JP54040372A priority Critical patent/JPS6059974B2/en
Publication of JPS55134137A publication Critical patent/JPS55134137A/en
Publication of JPS6059974B2 publication Critical patent/JPS6059974B2/en
Expired legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

PURPOSE: To separation-recover Pd as metallic Pd in a high yield by subjecting an arom. cpd. to oxidation coupling reaction in the presence of an org. Pd catalyst in a solventless state and mixing an alkali metal carbonate and a reducing agent into the resulting soln.
CONSTITUTION: An arom. cpd. such as benzene, toluene or xylene is dehydrogenation-dimerized in the presence of an org. Pd catalyst such as Pd salt of aliph. carboxylic acid in a solventless phase under a press. of 2W200kg/cm2 at a temp. of 40W300°C to form a biphenyl cpd. To the resulting soln. after the oxidation coupling reaction is added a carbonate such as Na2CO3, K2CO3 or Li2CO3, a hydrogencarbonate such as NaHCO3 or KHCO3 or other alkali metal carbonate in an amt. of 0.01W10g per kg of the soln., and they are mixed. After adding a reducing agent such as hydrogen gas, formic acid or oxalic acid the mixed soln. is agitated for 10minW10hr. Pd contained is deposited as large particles of 30μ or more and recovered in a high yield.
COPYRIGHT: (C)1980,JPO&Japio
JP54040372A 1979-04-05 1979-04-05 Palladium recovery method Expired JPS6059974B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP54040372A JPS6059974B2 (en) 1979-04-05 1979-04-05 Palladium recovery method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP54040372A JPS6059974B2 (en) 1979-04-05 1979-04-05 Palladium recovery method

Publications (2)

Publication Number Publication Date
JPS55134137A true JPS55134137A (en) 1980-10-18
JPS6059974B2 JPS6059974B2 (en) 1985-12-27

Family

ID=12578807

Family Applications (1)

Application Number Title Priority Date Filing Date
JP54040372A Expired JPS6059974B2 (en) 1979-04-05 1979-04-05 Palladium recovery method

Country Status (1)

Country Link
JP (1) JPS6059974B2 (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60102939A (en) * 1983-11-09 1985-06-07 Ube Ind Ltd Recovery and regeneration of palladium salt catalyst
JPS63319054A (en) * 1987-06-19 1988-12-27 Ube Ind Ltd Method for recovering palladium catalyst
JPS6456146A (en) * 1987-08-27 1989-03-03 Ube Industries Recovering method for palladium catalyst
JPH02163327A (en) * 1988-12-16 1990-06-22 Electroplating Eng Of Japan Co Reducing agent for recovering noble metal
JP2002115015A (en) * 2000-10-06 2002-04-19 Nippon Soda Co Ltd Method for recovering noble metal
US7054712B2 (en) 2002-08-06 2006-05-30 Fanuc Ltd Wire contact/noncontact boundary position detecting apparatus of wire cut discharge machine
WO2016167361A1 (en) * 2015-04-17 2016-10-20 アステラス製薬株式会社 METHOD FOR PRODUCING ORGANIC COMPOUND SUBSTANTIALLY FREE OF Pd, AND NOVEL METHOD FOR REMOVING Pd FROM ORGANIC COMPOUND USING HYDROGEN GAS

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60102939A (en) * 1983-11-09 1985-06-07 Ube Ind Ltd Recovery and regeneration of palladium salt catalyst
JPS63319054A (en) * 1987-06-19 1988-12-27 Ube Ind Ltd Method for recovering palladium catalyst
JPH0549345B2 (en) * 1987-06-19 1993-07-26 Ube Industries
JPS6456146A (en) * 1987-08-27 1989-03-03 Ube Industries Recovering method for palladium catalyst
JPH0549346B2 (en) * 1987-08-27 1993-07-26 Ube Industries
JPH02163327A (en) * 1988-12-16 1990-06-22 Electroplating Eng Of Japan Co Reducing agent for recovering noble metal
JP2002115015A (en) * 2000-10-06 2002-04-19 Nippon Soda Co Ltd Method for recovering noble metal
JP4567169B2 (en) * 2000-10-06 2010-10-20 日本曹達株式会社 How to recover precious metals
US7054712B2 (en) 2002-08-06 2006-05-30 Fanuc Ltd Wire contact/noncontact boundary position detecting apparatus of wire cut discharge machine
WO2016167361A1 (en) * 2015-04-17 2016-10-20 アステラス製薬株式会社 METHOD FOR PRODUCING ORGANIC COMPOUND SUBSTANTIALLY FREE OF Pd, AND NOVEL METHOD FOR REMOVING Pd FROM ORGANIC COMPOUND USING HYDROGEN GAS

Also Published As

Publication number Publication date
JPS6059974B2 (en) 1985-12-27

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