JPH11196774A - Granular formulated feed containing pelletized fatty acid and its production - Google Patents

Granular formulated feed containing pelletized fatty acid and its production

Info

Publication number
JPH11196774A
JPH11196774A JP10008227A JP822798A JPH11196774A JP H11196774 A JPH11196774 A JP H11196774A JP 10008227 A JP10008227 A JP 10008227A JP 822798 A JP822798 A JP 822798A JP H11196774 A JPH11196774 A JP H11196774A
Authority
JP
Japan
Prior art keywords
acid
weight
aliphatic monocarboxylic
fatty acid
feed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP10008227A
Other languages
Japanese (ja)
Other versions
JP4017227B2 (en
Inventor
Kazuyoshi Sato
一義 佐藤
Shunichi Takahashi
俊一 高橋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shiraishi Calcium Kaisha Ltd
Original Assignee
Shiraishi Calcium Kaisha Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shiraishi Calcium Kaisha Ltd filed Critical Shiraishi Calcium Kaisha Ltd
Priority to JP00822798A priority Critical patent/JP4017227B2/en
Publication of JPH11196774A publication Critical patent/JPH11196774A/en
Application granted granted Critical
Publication of JP4017227B2 publication Critical patent/JP4017227B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Landscapes

  • Fodder In General (AREA)

Abstract

PROBLEM TO BE SOLVED: To obtain the subject pelletized feed mixed product that has an appropriate strength, shows excellent digestion and absorption, storability and palatability and is useful as a feed for milk cows by mixing a prescribed mixture containing aliphatic monocarboxylic acid and the like, biologically effective substances and feedstuff and granulating the mixture. SOLUTION: The objective palletized feed mix product is prepared by mixing 50-80 wt.% of a aliphatic straight-chain 14-22C free monocarboxylic acid as myristic acid, 5-10 wt.% of a monovalent or divalent water-soluble metal salt as sodium salt or calcium salt, 5-10 wt.% of crude fiber source such as crushed leaves and stems containing >=20% crude fibers and 2-5 wt.% of adsorbent such as crushed product of porous natural minerals. In addition, biologically effective substances as one or more kinds of amino acids, vitamins and the like, and feedstuffs are admixed thereto and granulated or tabletted to give the objective fatty acid-containing mixed feed products. In a preferred embodiment, granulation and/or tabletting operations are carried out at a temperature of <=75 deg.C.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、脂肪酸含有高エネ
ルギー混合飼料造粒品及びその製造方法に関する。さら
に詳しくは、一般的な飼料用油脂の供給源として用いら
れる脂肪酸を高濃度に含有し、これに生物学的有効物質
を添加したペレット状の高エネルギー混合飼料造粒品、
及びその製造方法に関する。
TECHNICAL FIELD The present invention relates to a granulated product of a high energy mixed feed containing fatty acids and a method for producing the same. More specifically, a high-energy mixed feed granulated product in the form of pellets containing a high concentration of fatty acids used as a source of general feed fats and oils, and adding a biologically active substance thereto,
And its manufacturing method.

【0002】[0002]

【従来の技術】近年においては、反趨家畜の中でもとり
わけ乳牛については、遺伝改良及び飼養管理技術の進歩
により、泌乳量は年々増加する傾向にある。従来から泌
乳には大量のエネルギーを必要とし、一般的には、1キ
ログラムの牛乳を生産するには1.5Mcal前後のエネ
ルギー(正味泌乳エネルギー)が必要とされる。したが
って、泌乳量の増加に相応するエネルギー要求量を満た
すために、比較的エネルギーが高いとされるトウモロコ
シ又は大麦等の穀類、あるいは、大豆又は綿実等の油脂
含有量の多い原料などを用いて給与する飼料の調製が試
みられている。
2. Description of the Related Art In recent years, milk production among dairy cows has been increasing year by year due to genetic improvement and advancement of feeding management technology. Lactation has traditionally required a large amount of energy, and in general, the production of one kilogram of milk requires around 1.5 Mcal of energy (net lactation energy). Therefore, in order to satisfy the energy requirement corresponding to the increase in milk production, using cereals such as corn or barley, which are considered to have relatively high energy, or using raw materials having a high fat content such as soybeans or cottonseed. Attempts have been made to prepare feed for feeding.

【0003】しかしながら、これらの飼料原料の多給に
はルーメン機能,生理上に問題があり、その給与量が制
限される。すなわち、でんぷん等の多糖類がルーメン
内で急速に発酵分解され、多量の揮発性脂肪酸を生成す
るため、ルーメンpHが急激に低下してアシドーシス症
を呈し、穀類の多給を生じる問題、高油脂含有飼料と
して供される植物油脂は不飽和脂肪酸を多量に含有し、
これがルーメン内で微生物により分解,遊離され、他の
飼料を皮膜化したり、あるいはルーメン内に生息する微
生物を殺したりする問題、などにより生理,機能上に悪
影響を及ぼす。また、個々の乳牛においても乳期により
飼料摂取量にも限界があること等から、実際にはエネル
ギーは不足しているのが現状である。
[0003] However, there is a problem in the rumen function and the physiology in the large supply of these feed materials, and the supply amount is limited. In other words, polysaccharides such as starch are rapidly fermented and decomposed in the rumen to produce a large amount of volatile fatty acids, so that the pH of the rumen drops sharply, causing acidosis, and causing a large supply of cereals. Vegetable oils and fats served as containing feed contain large amounts of unsaturated fatty acids,
This is decomposed and released by microorganisms in the rumen, causing problems such as filming other feeds or killing microorganisms living in the rumen. In addition, even in individual dairy cows, there is a limit in feed intake depending on the milking period, and the actual current situation is that energy is insufficient.

【0004】このような問題に起因するエネルギー不足
を解消するに際し、現在ではパーム油又はナタネ油をC
2+,Mg2+,Na1+,K1+等の1価又は2価の金属イ
オンとケン化反応させることにより、生成された脂肪酸
塩(ケン化油脂)が高エネルギー飼料として利用されて
いる。一般に、Ca塩の脂肪酸カルシウムが多いこれら
の脂肪酸塩では、結合した金属イオンによりパーム油又
はナタネ油等の植物油脂に多量に含有する不飽和脂肪酸
のルーメン内での遊離が妨げられるため、ルーメン内に
生息する微生物に対し悪影響を及ぼさないとされてい
る。
[0004] In order to solve the energy shortage caused by such problems, palm oil or rapeseed oil is currently used in C.
Fatty acid salts (saponified fats and oils) produced by a saponification reaction with monovalent or divalent metal ions such as a 2+ , Mg 2+ , Na 1+ and K 1+ are used as high-energy feed. ing. In general, in these fatty acid salts having a large amount of fatty acid calcium of Ca salt, bound metal ions prevent release of unsaturated fatty acids contained in vegetable oils such as palm oil or rapeseed oil in a large amount in the lumen. It is not expected to have an adverse effect on the microorganisms that live in the country.

【0005】しかしながら、このような脂肪酸金属塩
(脂肪酸カルシウム)においては全くエネルギーの増減
に関与しない金属塩そのもの、更には脂肪酸と金属イオ
ンとの結合反応時に生じた水をも含有するため、同一重
量比ではエネルギーとしての絶対量は脂肪酸に比較して
15%程度減少する問題があった。また、元々嗜好性の
悪い脂肪酸に、更に、嗜好性の悪い金属イオンを含有す
るため、一層嗜好性が悪くなるという問題があった。ま
た、混合加工する上でも脂肪酸金属塩(例えば、脂肪酸
カルシウム等)の形状が平均粒径2ミリメートル以上の
粒状であるのに対し、他の生物学的有効物質の大部分が
1ミリメートル以下の粉末状であるために、これらの攪
拌混合物においては、生物学的有効物質の分散が均一に
ならず、偏りを生じる等の問題を有していた。
[0005] However, such fatty acid metal salts (fatty acid calcium) contain the metal salt itself which is not involved in the increase or decrease of energy at all, and further contain water generated during the binding reaction between the fatty acid and the metal ion. In terms of ratio, there was a problem that the absolute amount as energy was reduced by about 15% as compared with the fatty acid. In addition, there is a problem that the palatability further deteriorates because the fatty acid originally having poor palatability further contains a metal ion having poor palatability. In addition, even when mixed, the fatty acid metal salt (for example, fatty acid calcium, etc.) is in the form of granules having an average particle size of 2 mm or more, whereas most other biologically active substances are powders of 1 mm or less. In such a stirred mixture, there is a problem that the dispersion of the biologically active substance is not uniform, resulting in a bias.

【0006】一方、これらの問題を解消するに際して、
原料として一般的に粒径1ミリメートル以下の脂肪酸の
粉末品を用いて、上記の生物学的有効物質や他の嗜好性
の良好な物質との混合によれば、全体としての分散性及
び嗜好性に関しての改善効果はある程度期待できる。し
かしながら、単なる攪拌,混合処理のみでは、空気との
接触面積が大きくなり、酸化反応が進み易く、品質劣化
が生じたり、あるいはルーメン生理,機能の上でも生物
学的有効物質がルーメン内棲微生物により分解されるの
で有効利用されない等の問題が生じる。また、これらの
攪拌,混合物に造粒加工処理を施すことにより、上記問
題の解決を試みても、造粒工程時に発生する摩擦熱のた
めに、脂肪酸が融解して造粒が不可能になる。
On the other hand, in solving these problems,
According to a mixture of the above-mentioned biologically active substance and other substances having good palatability using a powdered product of a fatty acid having a particle diameter of 1 mm or less as a raw material, dispersibility and palatability as a whole are obtained. The effect of improvement can be expected to some extent. However, mere agitation or mixing alone increases the contact area with air, which facilitates the oxidation reaction, degrades the quality, or causes biologically active substances due to rumen endogenous microorganisms in rumen physiology and function. Since it is decomposed, there is a problem that it is not effectively used. In addition, even if an attempt is made to solve the above-mentioned problems by subjecting these agitation and mixture to granulation processing, fatty acids are melted due to frictional heat generated during the granulation step, and granulation becomes impossible. .

【0007】[0007]

【発明が解決しようとする課題】本発明者らは、上記問
題点,欠点に鑑み、乳牛,肉牛において不足するエネル
ギー及びその他の栄養素を安定的に補給させることを目
的に、可能な限り脂肪酸の含有率を高め、簡便な造粒処
理により、高エネルギー混合飼料を得るべく鋭意検討し
た。その結果、本発明者らは、遊離した脂肪族モノカル
ボン酸,水溶性金属塩,粗繊維供給物及び吸着材を特定
の割合で含む混合物と、生物学的有効物質と、飼料原料
とを含有させ、均一に攪拌,混合して造粒成形すること
により、可能な限り脂肪酸の含有率を高め、簡便な造粒
処理により、混合飼料の安定的な造粒及びペレット化が
可能であることを見い出した。
DISCLOSURE OF THE INVENTION In view of the above problems and disadvantages, the inventors of the present invention have proposed a method for stabilizing the supply of deficient energy and other nutrients in dairy and beef cattle to the extent possible, The content was increased, and a simple granulation process was performed to obtain a high-energy mixed feed. As a result, the present inventors have found that a mixture containing a specific proportion of free aliphatic monocarboxylic acid, a water-soluble metal salt, a crude fiber feed and an adsorbent, a biologically active substance, and a feed material are contained. By mixing and granulating by uniform stirring and mixing, the content of fatty acids is increased as much as possible, and it is possible to stably granulate and pelletize the mixed feed by simple granulation treatment. I found it.

【0008】また、本発明者らは、炭素数14〜22の
直鎖状の飽和若しくは不飽和の脂肪酸の1種又は2種以
上の混合物を50重量%以上含有し、これに対し、重量
比で1/10以上の水溶性の金属塩及び粗繊維供給物、
1/20以上の吸着材を攪拌,混合した後、造粒成形処
理を施しても造粒時に発生する摩擦熱により融解溶出
し、液状化した脂肪酸による造粒への悪影響が除外され
て、適度な強度を有するペレット製剤を高い回収率で得
られることを見い出した。更に、脂肪族モノカルボン酸
を混合物で用いる場合、該混合物の組成として、不飽和
脂肪族モノカルボン酸と飽和脂肪族モノカルボン酸とを
特定の割合で調製することにより、嗜好性,及び脂肪酸
の十二指腸以降の消化管での吸収利用性の点で優れるこ
とを見い出した。そして、本発明によれば、かかる製造
方法により得られたペレットは、粉体の攪拌,混合のみ
の処理では生物学的有効物質がルーメン内で微生物に分
解され、十二指腸以降の消化管で有効に吸収利用されな
い問題、及び、空気接触による酸化促進等の保存上の問
題を解決できることを見い出した。本発明は、かかる見
地より完成されたものである。
Further, the present inventors have disclosed that at least 50% by weight of one or more of a mixture of straight-chain saturated or unsaturated fatty acids having 14 to 22 carbon atoms is contained. 1/10 or more water-soluble metal salt and crude fiber feed,
Even if the adsorbent of 1/20 or more is stirred and mixed and then subjected to granulation molding treatment, it is melted and eluted by frictional heat generated during granulation, and the adverse effect on the granulation by the liquefied fatty acid is excluded. It has been found that a pellet preparation having a high strength can be obtained with a high recovery rate. Furthermore, when an aliphatic monocarboxylic acid is used in a mixture, the palatability and the fatty acid content of the mixture are adjusted by preparing an unsaturated aliphatic monocarboxylic acid and a saturated aliphatic monocarboxylic acid in a specific ratio. It was found to be superior in terms of its absorption and utilization in the digestive tract after the duodenum. According to the present invention, in the pellets obtained by such a production method, the biologically active substance is decomposed into microorganisms in the lumen by a process of only stirring and mixing of the powder, and is effectively used in the digestive tract after the duodenum. It has been found that the problem of not being used for absorption and the problem of storage such as acceleration of oxidation by air contact can be solved. The present invention has been completed from such a viewpoint.

【0009】[0009]

【課題を解決するための手段】すなわち、本発明は、遊
離した炭素数14〜22の直鎖状の脂肪族モノカルボン
酸を50〜80重量%、1価又は2価の水溶性金属塩を
5〜10重量%、粗繊維供給物を5〜10重量%、及び
吸着材を2〜5重量%含む混合物と、少なくとも1種以
上の生物学的有効物質と、飼料原料と、を含有すること
を特徴とするペレット状脂肪酸含有混合飼料造粒品を提
供するものである。また、本発明は、遊離した炭素数1
4〜22の直鎖状の脂肪族モノカルボン酸を50〜80
重量%、1価又は2価の水溶性金属塩を5〜10重量
%、粗繊維供給物を5〜10重量%、及び吸着材を2〜
5重量%含む混合物と、少なくとも1種以上の生物学的
有効物質と、飼料原料とを含有させ攪拌,混合の後、造
粒することを特徴とする脂肪酸含有高エネルギー混合飼
料造粒品の製造方法を提供するものである。以下、本発
明について、詳細に説明する。
That is, the present invention relates to a method for preparing a monovalent or divalent water-soluble metal salt of 50 to 80% by weight of a linear aliphatic monocarboxylic acid having 14 to 22 carbon atoms. A mixture comprising 5 to 10% by weight, 5 to 10% by weight of crude fiber feed and 2 to 5% by weight of adsorbent, at least one or more biologically active substances, and feed ingredients The present invention provides a pelletized fatty acid-containing mixed feed granulated product characterized by the following characteristics. In addition, the present invention relates to a method for producing a compound having 1
From 4 to 22 linear aliphatic monocarboxylic acids from 50 to 80
5 to 10% by weight of a monovalent or divalent water-soluble metal salt, 5 to 10% by weight of a crude fiber feed, and 2 to 2% of an adsorbent.
Production of a granulated product of a high-energy mixed feed containing fatty acids, comprising a mixture containing 5% by weight, at least one or more biologically active substances, and a feed material, followed by stirring, mixing and granulation. It provides a method. Hereinafter, the present invention will be described in detail.

【0010】[0010]

【発明の実施の形態】先ず、本発明のペレット状脂肪酸
含有高エネルギー混合飼料造粒品について説明する。本
発明の脂肪酸含有高エネルギー混合飼料造粒品は、遊離
した炭素数14〜22の直鎖状の脂肪族モノカルボン酸
(以下、「遊離脂肪酸」と略する場合がある。)を50
〜80重量%、1価又は2価の水溶性金属塩を5〜10
重量%、粗繊維供給物を5〜10重量%、及び吸着材を
2〜5重量%含む混合物と、少なくとも1種以上の生物
学的有効物質と、飼料原料とを含有する。
DESCRIPTION OF THE PREFERRED EMBODIMENTS First, a granulated product of a high-energy mixed feed containing pelleted fatty acids according to the present invention will be described. The fatty acid-containing high-energy mixed feed granulated product of the present invention contains 50 released linear aliphatic monocarboxylic acids having 14 to 22 carbon atoms (hereinafter sometimes abbreviated as "free fatty acids").
5 to 10% by weight of a monovalent or divalent water-soluble metal salt.
It contains a mixture comprising 5% by weight of crude fiber feed, 5% to 10% by weight of crude fiber feed and 2% to 5% by weight of adsorbent, at least one or more biologically active substances, and feed ingredients.

【0011】本発明で用いられる遊離脂肪酸は、遊離し
た炭素数14〜22の直鎖状の飽和若しくは不飽和の脂
肪族モノカルボン酸からなるものであり、飽和脂肪族モ
ノカルボン酸及び不飽和脂肪族モノカルボン酸の中から
選ばれた1種又は2種以上の混合物である。飽和脂肪族
モノカルボン酸としては、具体的には、例えばミリスチ
ン酸,ペンタデシル酸,パルミチン酸,ヘプタデシル
酸,ステアリン酸,ノナデカン酸等が挙げられる。これ
らカルボン酸の内、パルミチン酸,ステアリン酸は広く
汎用しており、経済的であることから好ましく用いられ
る。不飽和脂肪族モノカルボン酸としては、具体的に
は、例えばミリステオレン酸,オレイン酸,エライジン
酸,リノール酸,リノレン酸,アラキドン酸,ステアロ
ール酸,セトレイン酸等が挙げられる。これらカルボン
酸は必須脂肪酸であり、いずれの化合物であっても栄養
学的には好ましく用いられるが、操作性に優れるという
点からはオレイン酸が特に好ましく用いられる。
The free fatty acid used in the present invention comprises a straight-chain saturated or unsaturated aliphatic monocarboxylic acid having 14 to 22 carbon atoms, and includes a saturated aliphatic monocarboxylic acid and an unsaturated fatty acid. One or a mixture of two or more selected from group monocarboxylic acids. Specific examples of the saturated aliphatic monocarboxylic acid include myristic acid, pentadecylic acid, palmitic acid, heptadecylic acid, stearic acid, and nonadecanoic acid. Among these carboxylic acids, palmitic acid and stearic acid are widely used widely and are preferably used because they are economical. Specific examples of the unsaturated aliphatic monocarboxylic acid include, for example, myristoleic acid, oleic acid, elaidic acid, linoleic acid, linolenic acid, arachidonic acid, stearolic acid, and setreic acid. These carboxylic acids are essential fatty acids, and any compound is preferably used nutritionally, but oleic acid is particularly preferably used from the viewpoint of excellent operability.

【0012】上記遊離脂肪酸は、単独で用いることも、
2種類以上を組み合わせて混合物として用いることもで
きる。特に、混合物として用いる場合には、吸収利用性
の向上等の観点から、飽和脂肪族モノカルボン酸及び不
飽和脂肪族モノカルボン酸のそれぞれ1種以上を含むこ
とが好ましい。更に、遊離脂肪酸が、飽和脂肪族モノカ
ルボン酸及び不飽和脂肪族モノカルボン酸のそれぞれ1
種以上を含む混合物からなる場合には、嗜好性及び脂肪
酸の十二指腸以降の消化管での吸収利用性の向上の観点
から、該混合物の配合組成が、飽和脂肪族モノカルボン
酸81〜90重量%及び不飽和脂肪族モノカルボン酸1
0〜19重量%であることが好ましく、飽和脂肪族モノ
カルボン酸83〜87重量%及び不飽和脂肪族モノカル
ボン酸13〜17重量%であることが特に好ましい。不
飽和脂肪族モノカルボン酸が多い場合には、吸収利用性
等は向上するが、融点が低くなる分だけ加工上は不利に
なり、強度も低下する。これに対し、不飽和脂肪族モノ
カルボン酸が少ない場合には、吸収利用性等は低下する
が、加工上は有利になり、強度も向上する。
The above free fatty acids may be used alone,
Two or more kinds may be used in combination as a mixture. In particular, when used as a mixture, it is preferable to contain at least one of each of a saturated aliphatic monocarboxylic acid and an unsaturated aliphatic monocarboxylic acid from the viewpoint of improving absorption utilization. Further, the free fatty acid is one of saturated aliphatic monocarboxylic acid and unsaturated aliphatic monocarboxylic acid, respectively.
When the mixture is composed of a mixture containing at least one species, from the viewpoint of palatability and improvement in the absorption and utilization of fatty acids in the gastrointestinal tract after the duodenum, the composition of the mixture is from 81 to 90% by weight of saturated aliphatic monocarboxylic acid. And unsaturated aliphatic monocarboxylic acid 1
It is preferably from 0 to 19% by weight, particularly preferably from 83 to 87% by weight of a saturated aliphatic monocarboxylic acid and from 13 to 17% by weight of an unsaturated aliphatic monocarboxylic acid. When the amount of the unsaturated aliphatic monocarboxylic acid is large, the absorption utilization and the like are improved, but the lower melting point is disadvantageous in processing and lowers the strength. On the other hand, when the amount of unsaturated aliphatic monocarboxylic acid is small, absorption utilization and the like are reduced, but processing is advantageous and strength is improved.

【0013】一方、遊離脂肪酸は、粒径2ミリメートル
以下の粉末又は顆粒状の固形物であることが、分散性及
び嗜好性の向上の点から好ましく、粒径1.0ミリメート
ル〜1.5ミリメートルの範囲内にある固形物であること
がより好ましい。
On the other hand, the free fatty acid is preferably a powder or a granular solid having a particle size of 2 mm or less, from the viewpoint of improving dispersibility and palatability, and a particle size of 1.0 to 1.5 mm. More preferably, it is a solid within the range.

【0014】本発明で用いられる遊離脂肪酸は、混合物
と生物学的有効物質と飼料原料とを含有する本発明の混
合飼料において、該混合物中の50〜80重量%,好ま
しくは55〜75重量%,より好ましくは65〜70重
量%含まれる。上記混合物に対する遊離脂肪酸の配合割
合が50重量%未満であると、泌乳牛へのエネルギーの
供給及び生物学的有効物質のルーメンバイパス率の低下
の点で好ましくない。逆に、遊離脂肪酸の配合割合が8
0重量%を越えると、造粒加工してペレット状態を保持
するために必要な十分な強度が得られず、強度低下が生
じてしまう点で好ましくない。
The free fatty acid used in the present invention is 50 to 80% by weight, preferably 55 to 75% by weight in the mixture of the present invention containing the mixture, the biologically active substance and the feed raw material. , More preferably 65 to 70% by weight. If the mixing ratio of the free fatty acid to the above mixture is less than 50% by weight, it is not preferable in terms of supplying energy to the lactating cow and lowering the lumen bypass ratio of the biologically active substance. Conversely, the mixing ratio of free fatty acids is 8
If it exceeds 0% by weight, it is not preferable because sufficient strength necessary for granulating and maintaining a pellet state cannot be obtained, resulting in a decrease in strength.

【0015】本発明で用いられる水溶性金属塩として
は、ナトリウム塩,カリウム塩,カルシウム塩,マグネ
シウム塩等が挙げられ、具体的には、例えば水酸化カル
シウム,炭酸カルシウム,乳酸カルシウム等のカルシウ
ム塩、塩化カリウム等のカリウム塩などがある。これら
金属塩の中で、安定性及びコスト面からはカルシウム塩
が好ましく用いられる。また、これらの化合物は、単独
又は2種以上混合して、水溶性金属塩として用いること
ができる。本発明で用いられる水溶性金属塩は、混合物
と生物学的有効物質と飼料原料とを含有する本発明の混
合飼料において、該混合物中の5〜10重量%,好まし
くは6〜8重量%,より好ましくは6.5〜7.5重量%含
まれる。上記混合物に対する水溶性金属塩の配合割合が
5重量%未満であると、造粒成形処理の際に発生する摩
擦熱により脂肪酸が融解溶出し、造粒への悪影響がある
ため好ましくない。逆に、水溶性金属塩の配合割合が1
0重量%を越えると、本発明の目的の1つである嗜好性
の改善の点で好ましくない。
The water-soluble metal salt used in the present invention includes sodium salts, potassium salts, calcium salts, magnesium salts and the like. Specifically, for example, calcium salts such as calcium hydroxide, calcium carbonate and calcium lactate And potassium salts such as potassium chloride. Among these metal salts, calcium salts are preferably used from the viewpoint of stability and cost. These compounds can be used alone or in combination of two or more as a water-soluble metal salt. The water-soluble metal salt used in the present invention is 5 to 10% by weight, preferably 6 to 8% by weight of the mixture in the mixed feed of the present invention containing the mixture, the biologically active substance and the feed material. More preferably, the content is 6.5 to 7.5% by weight. If the mixing ratio of the water-soluble metal salt to the above mixture is less than 5% by weight, the fatty acid is melted and eluted due to frictional heat generated during the granulation molding treatment, which is unfavorable for granulation. Conversely, if the mixing ratio of the water-soluble metal salt is 1
If it exceeds 0% by weight, it is not preferable in view of improvement of palatability which is one of the objects of the present invention.

【0016】本発明に用いられる粗繊維供給物とは、ア
ルファルフアミール,パブリカ,又は20%以上の粗繊
維を含有する乾牧草等の粉砕物である。粗繊維供給物
は、少なくとも20%以上の粗繊維を含有する葉茎類の
粉砕物であることが好ましい。これらは、単独でも2種
以上混合しても、いずれの場合にも粗繊維供給物として
用いることができる。粗繊維供給物は、混合物と生物学
的有効物質と飼料原料とを含有する本発明の混合飼料に
おいて、該混合物中の5〜10重量%,好ましくは6〜
8重量%,より好ましくは6.5〜7.5重量%含まれる。
また、上記混合物に対する粗繊維供給物の配合割合が5
重量%未満であると、適度な強度を有するペレット製剤
を高い回収率で得られないので好ましくない。逆に、粗
繊維供給物の配合割合が10重量%を越えると、本発明
の目的の1つである生物学的有効物質を含有する高エネ
ルギー混合飼料のペレット化処理の点で好ましくない。
The crude fiber feed used in the present invention is a ground product such as alfalfa meal, publica, or hay containing 20% or more of crude fiber. The crude fiber feed is preferably a pulverized leaf stem containing at least 20% or more crude fiber. These can be used alone or as a mixture of two or more of them as crude fiber feeds. The crude fiber feed is 5 to 10% by weight, preferably 6 to 10% by weight of the mixture in the mixed feed of the present invention containing the mixture, the biologically active substance and the feed raw material.
8% by weight, more preferably 6.5 to 7.5% by weight.
Further, the mixing ratio of the crude fiber feed to the above mixture is 5%.
When the amount is less than the weight%, a pellet preparation having appropriate strength cannot be obtained at a high recovery rate, which is not preferable. Conversely, if the blending ratio of the crude fiber feed exceeds 10% by weight, it is not desirable in terms of pelletizing a high energy mixed feed containing a biologically active substance, which is one of the objects of the present invention.

【0017】本発明に用いられる吸着材とは、ゼオライ
ト,シリカ等の多孔質な天然鉱物の粉砕物又は多孔質化
合物の粉砕物である。これらの化合物は、単独でも2種
以上混合しても、いずれの場合でも吸着材として用いる
ことができる。吸着材は、混合物と生物学的有効物質と
飼料原料とを含有する本発明の混合飼料において、該混
合物中の2〜5重量%,好ましくは2.5〜4.5重量%,
より好ましくは3.5〜4.0重量%含まれる。また、上記
混合物に対する吸着材の配合割合が2重量%未満である
と、造粒成形処理の際に発生する摩擦熱により脂肪酸が
融解溶出し、造粒への悪影響があるため好ましくない。
逆に、吸着材の配合割合が5重量%を越えると、本発明
の目的の1つである生物学的有効物質を含有する高エネ
ルギー混合飼料を得るという観点からは好ましくない。
The adsorbent used in the present invention is a pulverized product of a porous natural mineral such as zeolite or silica or a pulverized product of a porous compound. These compounds may be used alone or as a mixture of two or more kinds as an adsorbent in any case. In the mixed feed of the present invention containing the mixture, the biologically active substance and the feed raw material, the adsorbent is 2 to 5% by weight of the mixture, preferably 2.5 to 4.5% by weight,
More preferably, the content is 3.5 to 4.0% by weight. If the blending ratio of the adsorbent to the above mixture is less than 2% by weight, the fatty acid is melted and eluted due to frictional heat generated during the granulation molding treatment, which is unfavorable for granulation.
Conversely, if the mixing ratio of the adsorbent exceeds 5% by weight, it is not preferable from the viewpoint of obtaining a high-energy mixed feed containing a biologically active substance, which is one of the objects of the present invention.

【0018】本発明の脂肪酸含有高エネルギー混合飼料
造粒品は、上記遊離脂肪酸,水溶性金属塩,粗繊維供給
物及び吸着材を含む混合物と、少なくとも1種以上の生
物学的有効物質と、飼料原料とを含有する。本発明で用
いられる上記生物学的有効物質とは、生体にとっての栄
養源であったり、疾病に対する治療や予防のための有用
な物質をいい、具体的には、例えばメチオニン,リジ
ン,スレオニン,トリプトファン等のアミノ酸及びその
誘導体、脂溶性あるいは水溶性ビタミン及びその誘導体
などが挙げられる。生物学的有効物質はアミノ酸類,脂
溶性ビタミン類又は水溶性ビタミン類の内のいずれか1
種以上からなることが好ましい。特に、生物学的有効物
質としては、リジン,メチオニン,スレオニン,トリプ
トファン,ビタミンE,ビタミンA,ビタミンD等を用
いることが好ましい。これらの有効物質は、単独でも2
種以上混合しても、いずれの場合でも生物学的有効物質
として有効に用いることができる。また、本発明の混合
飼料造粒品に対する生物学的有効物質の配合割合は、そ
の目的に適応した配合割合を適宜選択することが可能で
あり、何らの制限も受けないが、高エネルギー性及び嗜
好性等の観点からは、遊離脂肪酸を含む上記混合物10
0重量部に対して、好ましくは生物学的有効物質10〜
15重量部であり、より好ましくは12〜13.5重量部
である。更に、上記混合物の遊離脂肪酸としてパルミチ
ン酸,オレイン酸等を含む場合には、生物学的有効物質
としては、リジン,メチオニン,スレオニン,トリプト
ファン,ビタミンE等を用いることが好ましい。
[0018] The granulated product of high-energy mixed feed containing fatty acid of the present invention comprises a mixture comprising the above-mentioned free fatty acid, a water-soluble metal salt, a crude fiber feed and an adsorbent, at least one or more biologically active substances, Feed ingredients. The biologically active substance used in the present invention refers to a nutrient source for a living body or a substance useful for treating or preventing a disease, and specifically, for example, methionine, lysine, threonine, tryptophan. And their derivatives, fat-soluble or water-soluble vitamins and their derivatives, and the like. The biologically active substance is one of amino acids, fat-soluble vitamins or water-soluble vitamins
Preferably, it consists of more than one species. In particular, lysine, methionine, threonine, tryptophan, vitamin E, vitamin A, vitamin D, and the like are preferably used as the biologically active substance. These active substances, alone or
Even if more than one species are mixed, they can be effectively used as biologically active substances in any case. The mixing ratio of the biologically active substance to the mixed feed granulated product of the present invention can be appropriately selected from the mixing ratio suitable for the purpose, and is not subject to any limitation. From the viewpoint of palatability and the like, the mixture 10 containing free fatty acids
0 parts by weight, preferably 10 to 10 parts of the biologically active substance
It is 15 parts by weight, more preferably 12 to 13.5 parts by weight. Further, when the mixture contains palmitic acid, oleic acid, or the like as free fatty acids, it is preferable to use lysine, methionine, threonine, tryptophan, vitamin E, or the like as the biologically active substance.

【0019】本発明で用いられる上記飼料原料とは、生
体にとっての栄養源であったり、疾病に対する治療や予
防のための有用な物質をいい、通常用いられる飼料原料
を広く用いることができる。具体的には、例えば酒糠,
米糠等が挙げられ、これらの原料は単独でも2種以上混
合しても、いずれの場合でも飼料原料として用いること
ができる。また、本発明の混合飼料造粒品に対する上記
飼料原料の配合割合は、その目的に適応した配合割合を
適宜選択することが可能であり、何らの制限も受けない
が、ペレット状の高エネルギー混合飼料を得るという観
点からは、遊離脂肪酸を含む上記混合物100重量部に
対して、好ましくは飼料原料1〜5重量部であり、より
好ましくは2〜3重量部である。このような配合組成よ
り調製される本発明の混合飼料造粒品について、その給
与の対象となる動物は特に限定されないが、例えば乳牛
などのように反趨胃をもち、生産性の上で時期的にエネ
ルギー不足を生じる家畜には特に有効である。
The feed material used in the present invention refers to a nutrient source for a living body or a substance useful for treating or preventing a disease, and commonly used feed materials can be widely used. Specifically, for example, sake bran,
Rice bran and the like can be mentioned, and these raw materials can be used alone or in combination of two or more, and in any case, can be used as a feed raw material. In addition, the mixing ratio of the feed raw material to the mixed feed granulated product of the present invention can be appropriately selected from the mixing ratio suitable for the purpose, and is not subject to any limitation. From the viewpoint of obtaining a feed, the amount is preferably 1 to 5 parts by weight, more preferably 2 to 3 parts by weight, based on 100 parts by weight of the mixture containing free fatty acids. The animal to which the mixed feed granulated product of the present invention prepared from such a composition is to be fed is not particularly limited, but, for example, has a stomach such as a dairy cow, and is not suitable for productivity. It is especially effective for livestock that may have a shortage of energy.

【0020】次に、本発明の脂肪酸含有高エネルギー混
合飼料造粒品の製造方法について説明する。本発明の製
造方法は、遊離した炭素数14〜22の直鎖状の脂肪族
モノカルボン酸を50〜80重量%、1価又は2価の水
溶性金属塩を5〜10重量%、粗繊維供給物を5〜10
重量%、及び吸着材を2〜5重量%含む混合物と、少な
くとも1種以上の生物学的有効物質と、飼料原料とを含
有させ攪拌,混合の後、造粒するものである。
Next, the method for producing the high-energy mixed feed granulated product containing fatty acids of the present invention will be described. The production method of the present invention comprises the steps of: 50 to 80% by weight of a linear aliphatic monocarboxylic acid having 14 to 22 carbon atoms released; 5 to 10% by weight of a monovalent or divalent water-soluble metal salt; Supply 5-10
A mixture containing 2% to 5% by weight of an adsorbent, at least one or more biologically active substances, and feed materials is stirred, mixed, and granulated.

【0021】本発明の製造方法では、先ず、上記遊離脂
肪酸等を特定の割合で含む混合物と、少なくとも1種以
上の生物学的有効物質と、飼料原料とを均一に攪拌,混
合する。ここでは、上記混合物について、遊離脂肪酸を
50重量%以上含有し、これに対し、重量比で1/10
以上の水溶性の金属塩及び粗繊維供給物、更には1/2
0以上の吸着材を含有させることが必要である。すなわ
ち、本発明では、遊離脂肪酸を50〜80重量%、水溶
性金属塩を5〜10重量%、粗繊維供給物を5〜10重
量%、及び吸着材を2〜5重量%含む混合物を用いる。
このような特定の配合割合で粉末混合物を造粒すれば、
造粒時に発生する摩擦熱で混合物が融解溶出してしま
い、液状化した脂肪酸によって造粒に悪影響を及ぼすこ
とが排除できる。
In the production method of the present invention, first, a mixture containing the free fatty acids and the like in a specific ratio, at least one or more biologically active substances, and a feed material are uniformly stirred and mixed. Here, the above mixture contains 50% by weight or more of free fatty acids, and the weight ratio is 1/10
The above water-soluble metal salt and crude fiber feed, and furthermore, 1/2
It is necessary to contain zero or more adsorbents. That is, in the present invention, a mixture containing 50 to 80% by weight of a free fatty acid, 5 to 10% by weight of a water-soluble metal salt, 5 to 10% by weight of a crude fiber feed, and 2 to 5% by weight of an adsorbent is used. .
If the powder mixture is granulated at such a specific mixing ratio,
It can be excluded that the mixture melts and elutes due to frictional heat generated during granulation, and adversely affects granulation due to liquefied fatty acids.

【0022】次いで、得られた粉末状の混合物につい
て、造粒成形処理を施す。粉末混合物の造粒成形処理
は、通常の造粒方法を広く用いることができ、特に限定
されるものではない。具体的には、例えば一般に用いら
れている押し出し造粒機により加工することができる。
加工条件についても、特に限定されることなく粉末混合
物の配合組成等に応じて、適宜変更することが可能であ
るが、75℃以下で加工することが好ましい。一方、造
粒(ペレット化)するために75℃を越えると、油成分
(遊離脂肪酸等)の流出等により製造率(歩留まり)低
下が起こりかねず、また有効成分の分解等が起こるので
好ましくない。このような本発明の特定の配合による混
合飼料造粒品の製造方法によれば、適度な強度を有する
ペレット製剤として混合飼料が高い回収率で得られる。
Next, the obtained powdery mixture is subjected to a granulation molding treatment. The granulation of the powder mixture can be performed by a wide range of conventional granulation methods, and is not particularly limited. Specifically, it can be processed by, for example, a generally used extrusion granulator.
The processing conditions are also not particularly limited, and can be appropriately changed according to the composition of the powder mixture and the like. However, the processing is preferably performed at 75 ° C. or lower. On the other hand, if the temperature exceeds 75 ° C. for granulation (pelletization), the production rate (yield) may decrease due to the outflow of oil components (free fatty acids and the like), and the decomposition of the active ingredients may occur, which is not preferable. . According to the method for producing a mixed feed granulated product according to the specific composition of the present invention, a mixed feed can be obtained at a high recovery rate as a pellet preparation having appropriate strength.

【0023】すなわち、造粒に際して、遊離脂肪酸等の
油成分のみではペレット化しにくいので、製造率(歩留
まり)が低下するとともに、造粒品の強度低下等をも招
き、好ましい混合飼料が得られない。そこで本発明で
は、造粒(ペレット化)工程を容易にして製造率を向上
させるため、上記油成分に加えて水溶性金属塩を必須の
構成成分として含ませることとしている。これによっ
て、本発明の製造方法によれば、ペレット状の混合飼料
造粒品を効率良く得られるとともに、得られる造粒品の
機械的強度が増加する等の優れた効果が発揮される。以
下、実施例により本発明をより詳細に説明するが、本発
明はこれらの実施例によって何ら制限されるものではな
い。
That is, during granulation, it is difficult to pelletize only oil components such as free fatty acids, so that the production rate (yield) is reduced, the strength of the granulated product is also reduced, and a favorable mixed feed cannot be obtained. . Therefore, in the present invention, a water-soluble metal salt is included as an essential component in addition to the oil component in order to facilitate the granulation (pelletization) process and improve the production rate. As a result, according to the production method of the present invention, pelletized mixed feed granulated products can be efficiently obtained, and excellent effects such as an increase in mechanical strength of the obtained granulated products are exhibited. Hereinafter, the present invention will be described in more detail with reference to examples, but the present invention is not limited to these examples.

【0024】[0024]

【実施例】実施例1〜6、比較例1〜6及び参考例1,
2 本実施例、比較例及び参考例では、以下の原料を用いて
混合飼料を調製した。遊離脂肪酸については、飽和脂肪
族モノカルボン酸としてパルミチン酸及びステアリン
酸、不飽和脂肪族モノカルボン酸としてオレイン酸を用
いた。水溶性金属塩としては、粒径2ミリメートル以上
の脂肪酸カルシウム,水酸化カルシウム又は炭酸カルシ
ウムを用いた。粗繊維供給物としてはアルファルミー
ル、吸着材としてはゼオライトを用いた。生物学的有効
物質としては、リジン,メチオニン,スレオニン及びト
リプトファンの4種類のアミノ酸とビタミンEとを用い
た。飼料原料としては、酒糠及び米糠を用いた。下記表
1に、実施例1〜6、比較例1〜6及び参考例1,2で
用いた11種の混合飼料の配合組成を示す。
EXAMPLES Examples 1-6, Comparative Examples 1-6 and Reference Example 1,
2 In this example, comparative examples and reference examples, mixed feeds were prepared using the following raw materials. As for free fatty acids, palmitic acid and stearic acid were used as saturated aliphatic monocarboxylic acids, and oleic acid was used as unsaturated aliphatic monocarboxylic acids. As the water-soluble metal salt, fatty acid calcium, calcium hydroxide or calcium carbonate having a particle size of 2 mm or more was used. Alfal meal was used as the crude fiber feed, and zeolite was used as the adsorbent. As the biologically active substance, four kinds of amino acids, lysine, methionine, threonine and tryptophan, and vitamin E were used. Sake bran and rice bran were used as feed materials. Table 1 below shows the composition of the 11 types of mixed feed used in Examples 1 to 6, Comparative Examples 1 to 6 and Reference Examples 1 and 2.

【0025】[0025]

【表1】 [Table 1]

【0026】配合に際しては、各成分を均一に攪拌,混
合した。次いで、実施例1〜6、比較例2〜6及び参考
例1,2においては、得られた粉末混合物を押し出し造
粒機により、ペレット製剤(混合飼料造粒品)に加工し
た。得られたペレット製剤(実施例1〜6、比較例2〜
6及び参考例1,2)、及び表1の比較例1に示す粉末
混合物の計12種類の混合飼料について、それぞれ製
剤回収率,製剤強度,嗜好性,製品の安定性,
脂肪酸消化率,生物学的有効物質の安定性,反趨胃
内における生物学的有効物質の安定性,製剤中の生物
学的有効物質の分散性、についての試験,評価を行っ
た。
At the time of compounding, the components were uniformly stirred and mixed. Next, in Examples 1 to 6, Comparative Examples 2 to 6, and Reference Examples 1 and 2, the obtained powder mixture was processed into a pellet preparation (mixed feed granulated product) by an extrusion granulator. The obtained pellet preparation (Examples 1 to 6, Comparative Examples 2 to
6 and Reference Examples 1 and 2) and a total of 12 kinds of mixed feeds of the powder mixture shown in Comparative Example 1 in Table 1, respectively, the formulation recovery rate, formulation strength, palatability, product stability,
Tests and evaluations on fatty acid digestibility, stability of biologically active substances, stability of biologically active substances in the stomach, and dispersibility of biologically active substances in pharmaceutical preparations were performed.

【0027】各試験,評価項目の詳細を以下に示す。 製剤回収率:(製剤回収率)=(造粒冷却後に回収で
きた製剤の全重量(kg))/(各配合組成混合粉末重量(k
g))×100 製剤強度: ペレット造粒後、冷却乾燥し、その後破
砕機にて測定した。 嗜好性 : 給与両100gを完全に摂食した牛のみ
をカウントして、その割合を嗜好性の目安とした。 製品の安定性: インキュベーター内(37℃)にて
1カ月間静置し、過酸化物価を測定し製品劣化の目安に
した。 第一胃にフィステル,十二指腸及び回腸にカニューレ
を装着したホルスタイン種乳牛のルーメンへ製剤を直接
投与し、回腸にて回収された脂肪酸を給与全脂肪酸から
差し引いた分の給与全脂肪酸に対する割合を消化率とし
た。 (脂肪酸消化率)={(給与全脂肪酸)−(回腸にて回
収された脂肪酸)}/(給与全脂肪酸)×100 in vitro での安定性(表3): ルーメン等張液
(pH=6.7)に37℃恒温で3時間の浸漬攪拌処理を行
い、処理前、処理後の各種アミノ酸及びビタミンEの含
有量を測定して残存率(%)とし、安定性の指標とし
た。 in vivoでの安定性(表4): フィステル装着牛を
用いてナイロンバック法により製剤をルーメンに直接投
入し、3時間後,6時間後,12時間後,及び処理前に
おける各種アミノ酸の含有量を測定して残存率(%)と
し、安定性の指標とした。 生物学的有効物質の分散率(表5):(分散率)(%)
={(実測値)/(理論値)}×100 上記〜の各試験項目について、得られた試験結果を
下記表2〜表5に示す。
The details of each test and evaluation items are shown below. Formulation recovery rate: (formulation recovery rate) = (total weight (kg) of formulation recovered after cooling granulation) / (weight of mixed powder of each composition (k
g)) × 100 Formulation strength: After granulation of pellets, they were cooled and dried, and then measured with a crusher. Preference: Only cows that completely consumed both 100 g of the saliva were counted, and the ratio was used as a guide to the preference. Product stability: The product was allowed to stand for 1 month in an incubator (37 ° C.), and the peroxide value was measured and used as a measure of product deterioration. Digestion rate is the ratio of the total fatty acid to the total fatty acid obtained by subtracting the fatty acid recovered from the ileum from the total fatty acid fed to the rumen of a Holstein dairy cow with a fistula in the rumen and a cannula in the duodenum and ileum. And (Fatty acid digestibility) = {(total fatty acid fed) − (fatty acid recovered in ileum)} / (total fatty acid fed) × 100 Stability in vitro (Table 3): Rumen isotonic solution (pH = 6.7) ) Was subjected to immersion and stirring for 3 hours at a constant temperature of 37 ° C., and the contents of various amino acids and vitamin E before and after the treatment were measured to obtain a residual ratio (%), which was used as an index of stability. In vivo stability (Table 4): Using a cow equipped with a fistula, the preparation was directly injected into the rumen by the nylon bag method, and the contents of various amino acids before, after 3, 6 and 12 hours, and before treatment Was measured to obtain a residual rate (%), which was used as an index of stability. Dispersion rate of biologically active substance (Table 5): (Dispersion rate) (%)
= {(Actual value) / (theoretical value)} × 100 The test results obtained for each of the above test items are shown in Tables 2 to 5 below.

【0028】[0028]

【表2】 [Table 2]

【0029】[0029]

【表3】 [Table 3]

【0030】[0030]

【表4】 [Table 4]

【0031】[0031]

【表5】 [Table 5]

【0032】上記表2〜表5に示す試験結果により、以
下のことがわかった。すなわち、本発明の脂肪酸含有高
エネルギー混合飼料造粒品(実施例1〜6)は、製剤の
基本特性となる上記試験,評価対象8項目の全てにおい
て、十分満足しうる性能を有することがわかった。これ
に対して、造粒しない粉末混合物(比較例1)では、空
気による製品劣化が生じ易く保存上問題があるととも
に、嗜好性の点で満足できる性能を有していなかった。
遊離脂肪酸を含有しない比較例3の造粒品では、エネル
ギー面で劣るために高エネルギー混合飼料としては満足
できるものではなかった。水溶性金属塩を含有しない比
較例2の造粒品では、エネルギー面では優れるが製剤回
収率及び強度の点で満足できる性能を有していなかっ
た。粗繊維供給物を含有しない比較例4及び6の造粒品
では、製剤の嗜好性の点で満足できる性能を有していな
かった。吸着材を含有しない比較例5及び6の造粒品で
は、製剤の嗜好性及び強度の点で満足できる性能を有し
ていなかった。
From the test results shown in Tables 2 to 5, the following was found. That is, it is found that the fatty acid-containing high-energy mixed feed granulated product of the present invention (Examples 1 to 6) has sufficiently satisfactory performance in all of the above-mentioned tests and eight evaluation items which are the basic characteristics of the preparation. Was. On the other hand, the powder mixture that was not granulated (Comparative Example 1) was liable to cause deterioration of the product due to air, had a problem in storage, and did not have satisfactory performance in terms of palatability.
The granulated product of Comparative Example 3 containing no free fatty acid was not satisfactory as a high-energy mixed feed because of its inferior energy. The granulated product of Comparative Example 2 containing no water-soluble metal salt was excellent in energy, but did not have satisfactory performance in terms of preparation recovery rate and strength. The granulated products of Comparative Examples 4 and 6 containing no crude fiber feed did not have satisfactory performance in terms of the palatability of the preparation. The granulated products of Comparative Examples 5 and 6 containing no adsorbent did not have satisfactory performance in terms of the palatability and strength of the preparation.

【0033】[0033]

【発明の効果】本発明によれば、可能な限り脂肪酸の含
有率を高め、簡便な造粒処理により、高エネルギーな混
合飼料を提供することが可能であり、乳牛,肉牛におい
て不足するエネルギー及びその他の栄養素を安定的に補
給させることができる。また、本発明の製造方法によれ
ば、混合飼料を攪拌,混合した後、造粒成形処理を施し
ても造粒時に発生する摩擦熱により、脂肪酸が融解溶出
し、液状化した脂肪酸によって造粒に悪影響が生じるこ
とを排除することができるとともに、適度な強度を有す
るペレット製剤を高い回収率で得られる。更に、本発明
の製造方法により得られたペレットは、乳牛等の家畜に
用いた場合の消化,吸収性に優れ、また、空気接触によ
る酸化劣化が防止され保存性に優れる等の利点をも有し
ており、その産業上の意義は極めて大きい。
According to the present invention, it is possible to increase the content of fatty acids as much as possible and to provide a high-energy mixed feed by a simple granulation treatment. Other nutrients can be supplied stably. Further, according to the production method of the present invention, even after the mixed feed is stirred and mixed, the fatty acid is melted and eluted due to frictional heat generated at the time of granulation even when the granulated molding treatment is performed, and granulated with the liquefied fatty acid. Adverse effects can be excluded, and a pellet preparation having an appropriate strength can be obtained at a high recovery rate. Furthermore, the pellets obtained by the production method of the present invention have advantages such as excellent digestibility and absorbability when used for livestock such as dairy cows, and prevention of oxidative deterioration due to air contact and excellent storage stability. And its industrial significance is extremely large.

Claims (11)

【特許請求の範囲】[Claims] 【請求項1】 遊離した炭素数14〜22の直鎖状の脂
肪族モノカルボン酸を50〜80重量%、1価又は2価
の水溶性金属塩を5〜10重量%、粗繊維供給物を5〜
10重量%、及び吸着材を2〜5重量%含む混合物と、
少なくとも1種以上の生物学的有効物質と、飼料原料と
を含有することを特徴とするペレット状脂肪酸含有混合
飼料造粒品。
1. A crude fiber feed comprising 50 to 80% by weight of a free linear aliphatic monocarboxylic acid having 14 to 22 carbon atoms and 5 to 10% by weight of a monovalent or divalent water-soluble metal salt. To 5
A mixture containing 10% by weight, and 2 to 5% by weight of an adsorbent;
A pelleted fatty acid-containing mixed feed granulated product comprising at least one or more biologically active substances and a feed material.
【請求項2】 上記脂肪族モノカルボン酸として、ミリ
スチン酸,パルミチン酸,ステアリン酸の内、いずれか
1つの遊離した飽和脂肪族モノカルボン酸を含むことを
特徴とする請求項1記載のペレット状脂肪酸含有混合飼
料造粒品。
2. The pellet according to claim 1, wherein said aliphatic monocarboxylic acid contains any one of free saturated aliphatic monocarboxylic acids among myristic acid, palmitic acid and stearic acid. Mixed feed granules containing fatty acids.
【請求項3】 上記脂肪族モノカルボン酸として、オレ
イン酸の遊離した不飽和脂肪族モノカルボン酸を含むこ
とを特徴とする請求項1記載のペレット状脂肪酸含有混
合飼料造粒品。
3. The pelletized fatty acid-containing mixed feed granulated product according to claim 1, wherein the aliphatic monocarboxylic acid contains unsaturated aliphatic monocarboxylic acid in which oleic acid is released.
【請求項4】 上記脂肪族モノカルボン酸が、飽和脂肪
族モノカルボン酸及び不飽和脂肪族モノカルボン酸のそ
れぞれ1種以上を含む混合物からなるものであって、該
混合物の配合組成が、飽和脂肪族モノカルボン酸81〜
90重量%及び不飽和脂肪族モノカルボン酸10〜19
重量%であることを特徴とする請求項1記載のペレット
状脂肪酸含有混合飼料造粒品。
4. The composition according to claim 1, wherein the aliphatic monocarboxylic acid comprises a mixture containing at least one of a saturated aliphatic monocarboxylic acid and an unsaturated aliphatic monocarboxylic acid. Aliphatic monocarboxylic acids 81-
90% by weight and unsaturated aliphatic monocarboxylic acid 10-19
The pelletized fatty acid-containing mixed feed granulated product according to claim 1, wherein the content is weight%.
【請求項5】 上記脂肪族モノカルボン酸が粒径2ミリ
メートル以下の粉末又は顆粒状の固形物であることを特
徴とする請求項1記載のペレット状脂肪酸含有混合飼料
造粒品。
5. The pelletized fatty acid-containing mixed feed granulated product according to claim 1, wherein the aliphatic monocarboxylic acid is a powder or a granular solid having a particle size of 2 mm or less.
【請求項6】 上記水溶性金属塩として、ナトリウム
塩,カリウム塩,カルシウム塩又はマグネシウム塩の
内、いずれか1つの該水溶性金属塩を含むことを特徴と
する請求項1記載のペレット状脂肪酸含有混合飼料造粒
品。
6. The pellet-like fatty acid according to claim 1, wherein the water-soluble metal salt contains any one of a sodium salt, a potassium salt, a calcium salt and a magnesium salt. Containing mixed feed granulated product.
【請求項7】 上記粗繊維供給物が少なくとも20%以
上の粗繊維を含有する葉茎類の粉砕物であることを特徴
とする請求項1記載のペレット状脂肪酸含有混合飼料造
粒品。
7. The pelletized fatty acid-containing mixed feed granulated product according to claim 1, wherein the crude fiber supply is a pulverized leaf stem containing at least 20% or more of crude fiber.
【請求項8】 上記吸着材が多孔質天然鉱物又は多孔質
化合物の粉砕物であることを特徴とする請求項1記載の
脂肪酸含有高エネルギー混合飼料造粒品。
8. The granulated product of a high-energy mixed feed containing fatty acids according to claim 1, wherein the adsorbent is a pulverized product of a porous natural mineral or a porous compound.
【請求項9】 上記生物学的有効物質がアミノ酸類,脂
溶性ビタミン類又は水溶性ビタミン類の内のいずれか1
種以上からなることを特徴とする請求項1記載のペレッ
ト状脂肪酸含有混合飼料造粒品。
9. The method according to claim 1, wherein the biologically active substance is any one of amino acids, fat-soluble vitamins and water-soluble vitamins.
The pelletized fatty acid-containing mixed feed granulated product according to claim 1, comprising at least one seed.
【請求項10】 遊離した炭素数14〜22の直鎖状の
脂肪族モノカルボン酸を50〜80重量%、1価又は2
価の水溶性金属塩を5〜10重量%、粗繊維供給物を5
〜10重量%、及び吸着材を2〜5重量%含む混合物
と、少なくとも1種以上の生物学的有効物質と、飼料原
料とを含有させ攪拌,混合の後、造粒することを特徴と
するペレット状脂肪酸含有混合飼料造粒品の製造方法。
10. A monocyclic or monohydric aliphatic monocarboxylic acid having 14 to 22 carbon atoms, which is 50 to 80% by weight.
5 to 10% by weight of the water-soluble metal salt of
A mixture containing 10 to 10% by weight and an adsorbent of 2 to 5% by weight, at least one or more biologically active substances, and feed materials, followed by stirring, mixing, and granulation. A method for producing a pelleted fatty acid-containing mixed feed granulated product.
【請求項11】 上記造粒する際に、75℃以下の加工
温度で行うことを特徴とする請求項10記載のペレット
状脂肪酸含有混合飼料造粒品の製造方法。
11. The method according to claim 10, wherein the granulation is performed at a processing temperature of 75 ° C. or less.
JP00822798A 1998-01-20 1998-01-20 Pelletized fatty acid-containing mixed feed granulated product and method for producing the same Expired - Lifetime JP4017227B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP00822798A JP4017227B2 (en) 1998-01-20 1998-01-20 Pelletized fatty acid-containing mixed feed granulated product and method for producing the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP00822798A JP4017227B2 (en) 1998-01-20 1998-01-20 Pelletized fatty acid-containing mixed feed granulated product and method for producing the same

Publications (2)

Publication Number Publication Date
JPH11196774A true JPH11196774A (en) 1999-07-27
JP4017227B2 JP4017227B2 (en) 2007-12-05

Family

ID=11687288

Family Applications (1)

Application Number Title Priority Date Filing Date
JP00822798A Expired - Lifetime JP4017227B2 (en) 1998-01-20 1998-01-20 Pelletized fatty acid-containing mixed feed granulated product and method for producing the same

Country Status (1)

Country Link
JP (1) JP4017227B2 (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011234679A (en) * 2010-05-11 2011-11-24 Meiji Shiryo Kk Method for increasing content of highly-unsaturated fatty acid in milk of ruminant livestock and medicine or animal feeding stuff used in the method
CN103098752A (en) * 2012-12-17 2013-05-15 潘凌烊 Method for manufacturing Taxus poultry products
CN103098751A (en) * 2012-12-17 2013-05-15 潘凌烊 Method for manufacturing ginseng poultry products
CN105592711A (en) * 2013-07-30 2016-05-18 拜内梅尔克公司 Feed for lactating ruminants
JP2016525371A (en) * 2013-07-30 2016-08-25 ベネミルク オーワイBenemilk Oy Ruminant mineral licking composition and method of making and using the same
JP2016526906A (en) * 2013-07-30 2016-09-08 ベネミルク オーワイBenemilk Oy Solid diet composition for ruminant and production method using the same
JP2017511126A (en) * 2014-03-13 2017-04-20 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se Pelletized ruminant feed enhanced with ingredients available for rumen
JP2018510618A (en) * 2015-02-02 2018-04-19 ベネミルク オーワイBenemilk Oy Animal feed composition and production method thereof
US11219227B2 (en) 2009-11-02 2022-01-11 Energy Booster Newco, Llc Partial calcification of free fatty acid mixtures, livestock feed compositions including them, and methods of making same

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0280804A (en) * 1988-09-13 1990-03-20 Kojima Shoten:Kk Assembly unit
JPH0214019B2 (en) * 1982-04-02 1990-04-05 Nippon Soda Co
JPH04122037A (en) * 1990-09-13 1992-04-22 Sharp Corp Package method of semiconductor chip
JPH0523114A (en) * 1991-01-14 1993-02-02 Ajinomoto Co Inc Feed additive composition for ruminant
JPH07115916A (en) * 1993-10-29 1995-05-09 Nippon Oil & Fats Co Ltd Feed composition
JPH08336360A (en) * 1995-03-17 1996-12-24 Kanagawa Kagaku Kenkyusho:Kk Feed composition for ruminant and feeding using the same
JPH09187228A (en) * 1995-06-15 1997-07-22 Nippon Soda Co Ltd Additive to feed for ruminant
JPH09299038A (en) * 1996-05-16 1997-11-25 Nof Corp Production of feed composition
JPH114659A (en) * 1997-06-16 1999-01-12 Nof Corp Production of feed composition

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0214019B2 (en) * 1982-04-02 1990-04-05 Nippon Soda Co
JPH0280804A (en) * 1988-09-13 1990-03-20 Kojima Shoten:Kk Assembly unit
JPH04122037A (en) * 1990-09-13 1992-04-22 Sharp Corp Package method of semiconductor chip
JPH0523114A (en) * 1991-01-14 1993-02-02 Ajinomoto Co Inc Feed additive composition for ruminant
JPH07115916A (en) * 1993-10-29 1995-05-09 Nippon Oil & Fats Co Ltd Feed composition
JPH08336360A (en) * 1995-03-17 1996-12-24 Kanagawa Kagaku Kenkyusho:Kk Feed composition for ruminant and feeding using the same
JPH09187228A (en) * 1995-06-15 1997-07-22 Nippon Soda Co Ltd Additive to feed for ruminant
JPH09299038A (en) * 1996-05-16 1997-11-25 Nof Corp Production of feed composition
JPH114659A (en) * 1997-06-16 1999-01-12 Nof Corp Production of feed composition

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11219227B2 (en) 2009-11-02 2022-01-11 Energy Booster Newco, Llc Partial calcification of free fatty acid mixtures, livestock feed compositions including them, and methods of making same
JP2011234679A (en) * 2010-05-11 2011-11-24 Meiji Shiryo Kk Method for increasing content of highly-unsaturated fatty acid in milk of ruminant livestock and medicine or animal feeding stuff used in the method
CN103098752A (en) * 2012-12-17 2013-05-15 潘凌烊 Method for manufacturing Taxus poultry products
CN103098751A (en) * 2012-12-17 2013-05-15 潘凌烊 Method for manufacturing ginseng poultry products
CN105592711A (en) * 2013-07-30 2016-05-18 拜内梅尔克公司 Feed for lactating ruminants
JP2016525371A (en) * 2013-07-30 2016-08-25 ベネミルク オーワイBenemilk Oy Ruminant mineral licking composition and method of making and using the same
JP2016526907A (en) * 2013-07-30 2016-09-08 ベネミルク オーワイBenemilk Oy Feed for lactating ruminants
JP2016526906A (en) * 2013-07-30 2016-09-08 ベネミルク オーワイBenemilk Oy Solid diet composition for ruminant and production method using the same
JP2017511126A (en) * 2014-03-13 2017-04-20 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se Pelletized ruminant feed enhanced with ingredients available for rumen
JP2018510618A (en) * 2015-02-02 2018-04-19 ベネミルク オーワイBenemilk Oy Animal feed composition and production method thereof

Also Published As

Publication number Publication date
JP4017227B2 (en) 2007-12-05

Similar Documents

Publication Publication Date Title
CA2372646C (en) Method for manufacturing rumen bypass feed supplement
US8182851B2 (en) Ruminant feedstock dietary supplement
US6656494B1 (en) Method of feeding reproductive female pigs and feeds for reproductive female pigs
US4904473A (en) Ruminant feed antacid containing potassium, sodium and chlorine
US5456927A (en) Ruminant feed supplement product
US5635198A (en) Granular agent for ruminants and process for producing the same
US5928687A (en) Rumen by-pass feed supplement
JPH09172979A (en) Feed additive for ruminant containing new compound salt of phosphoric acid and amino acid and antacid
US4857332A (en) Composition and method for increasing milk fat production in ruminants
US4976963A (en) Ruminant feed antacid containing potassium, sodium and chlorine
JPH09172980A (en) Feed additive for ruminant containing new compound salt of phosphoric acid and amino acid and water-soluble macromolecular substance
JP4017227B2 (en) Pelletized fatty acid-containing mixed feed granulated product and method for producing the same
US5633004A (en) Granular agent for ruminants and process for producing the same
US6203829B1 (en) Feed additives for ruminants
US8178138B2 (en) Ruminant feedstock dietary supplement
EP0478783B1 (en) Feed additive for ruminant
US5776483A (en) Feed additive for ruminants
US6924382B2 (en) Rumen bypass calcium salts of C18:1 and C18:2 fatty acids
CA2124925C (en) Preparation of dietary fatty acid salt products
JP2869799B2 (en) Ruminant feed additives
US20220211076A1 (en) Additive composition for ruminant feeds
RU2770924C2 (en) Compositions and methods intended for improvement of nitrogen assimilation in ruminant animal
JPH0453454A (en) Protein feed for ruminant
JPH1014500A (en) Production of feed composition
JPH01218558A (en) Feed additive for ruminant

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20041109

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20060915

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20061106

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20070309

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20070507

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20070824

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20070918

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100928

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110928

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20120928

Year of fee payment: 5

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130928

Year of fee payment: 6

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term