JPH09512354A - 非線形結晶及びそれらの利用 - Google Patents
非線形結晶及びそれらの利用Info
- Publication number
- JPH09512354A JPH09512354A JP8525444A JP52544496A JPH09512354A JP H09512354 A JPH09512354 A JP H09512354A JP 8525444 A JP8525444 A JP 8525444A JP 52544496 A JP52544496 A JP 52544496A JP H09512354 A JPH09512354 A JP H09512354A
- Authority
- JP
- Japan
- Prior art keywords
- single crystal
- crystals
- general formula
- crystal
- lno
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000013078 crystal Substances 0.000 title claims abstract description 69
- 230000003287 optical effect Effects 0.000 claims abstract description 7
- 229910052688 Gadolinium Inorganic materials 0.000 claims abstract description 5
- 229910052747 lanthanoid Inorganic materials 0.000 claims abstract description 5
- 150000002602 lanthanoids Chemical class 0.000 claims abstract description 5
- 229910052727 yttrium Inorganic materials 0.000 claims abstract description 5
- 229910052746 lanthanum Inorganic materials 0.000 claims abstract description 4
- 229910052765 Lutetium Inorganic materials 0.000 claims abstract description 3
- 238000002844 melting Methods 0.000 claims description 12
- 230000008018 melting Effects 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 8
- 238000002425 crystallisation Methods 0.000 claims description 5
- 230000008025 crystallization Effects 0.000 claims description 5
- 239000002019 doping agent Substances 0.000 claims 1
- 238000000034 method Methods 0.000 description 7
- 230000000694 effects Effects 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 230000009021 linear effect Effects 0.000 description 4
- 235000019796 monopotassium phosphate Nutrition 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229910052779 Neodymium Inorganic materials 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229910000311 lanthanide oxide Inorganic materials 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- BTBUEUYNUDRHOZ-UHFFFAOYSA-N Borate Chemical compound [O-]B([O-])[O-] BTBUEUYNUDRHOZ-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- DYAHQFWOVKZOOW-UHFFFAOYSA-N Sarin Chemical compound CC(C)OP(C)(F)=O DYAHQFWOVKZOOW-UHFFFAOYSA-N 0.000 description 1
- -1 Yttrium compound Chemical class 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 1
- 230000000763 evoking effect Effects 0.000 description 1
- 230000005281 excited state Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- UIWYJDYFSGRHKR-UHFFFAOYSA-N gadolinium atom Chemical compound [Gd] UIWYJDYFSGRHKR-UHFFFAOYSA-N 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 229910021644 lanthanide ion Inorganic materials 0.000 description 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 description 1
- QEFYFXOXNSNQGX-UHFFFAOYSA-N neodymium atom Chemical compound [Nd] QEFYFXOXNSNQGX-UHFFFAOYSA-N 0.000 description 1
- 230000009022 nonlinear effect Effects 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000004857 zone melting Methods 0.000 description 1
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/35—Non-linear optics
- G02F1/355—Non-linear optics characterised by the materials used
- G02F1/3551—Crystals
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B15/00—Single-crystal growth by pulling from a melt, e.g. Czochralski method
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/35—Non-linear optics
- G02F1/37—Non-linear optics for second-harmonic generation
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/35—Non-linear optics
- G02F1/39—Non-linear optics for parametric generation or amplification of light, infrared or ultraviolet waves
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01S—DEVICES USING THE PROCESS OF LIGHT AMPLIFICATION BY STIMULATED EMISSION OF RADIATION [LASER] TO AMPLIFY OR GENERATE LIGHT; DEVICES USING STIMULATED EMISSION OF ELECTROMAGNETIC RADIATION IN WAVE RANGES OTHER THAN OPTICAL
- H01S3/00—Lasers, i.e. devices using stimulated emission of electromagnetic radiation in the infrared, visible or ultraviolet wave range
- H01S3/10—Controlling the intensity, frequency, phase, polarisation or direction of the emitted radiation, e.g. switching, gating, modulating or demodulating
- H01S3/106—Controlling the intensity, frequency, phase, polarisation or direction of the emitted radiation, e.g. switching, gating, modulating or demodulating by controlling devices placed within the cavity
- H01S3/108—Controlling the intensity, frequency, phase, polarisation or direction of the emitted radiation, e.g. switching, gating, modulating or demodulating by controlling devices placed within the cavity using non-linear optical devices, e.g. exhibiting Brillouin or Raman scattering
- H01S3/109—Frequency multiplication, e.g. harmonic generation
- H01S3/1095—Frequency multiplication, e.g. harmonic generation self doubling, e.g. lasing and frequency doubling by the same active medium
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Nonlinear Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Inorganic Insulating Materials (AREA)
- Lasers (AREA)
- Optical Modulation, Optical Deflection, Nonlinear Optics, Optical Demodulation, Optical Logic Elements (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Compounds Of Unknown Constitution (AREA)
- Saccharide Compounds (AREA)
Abstract
Description
Claims (1)
- 【特許請求の範囲】 1.一般式 M4LnO(BO3)3 (この式中、MはCa、又はSrもしくはBaで部分的に置換されたCaであり 、LnはY、Gd、La及びLuを含む群のランタニドのうちの一つである)の 一致溶融組成物の結晶化により得られた非線形単結晶。 2.前記一般式において、CaがSrもしくはBaで部分的に置換されている 場合に、置換された元素の含有量がもはや溶融が一致溶融にならないものに限定 される、請求の範囲第1項記載の単結晶。 3.一般式が Ca4-xSrxLnO(BO3)3 であり、式中のxが0.5未満である、請求の範囲第1項記載の単結晶。 4.一般式が Ca4-yBayLnO(BO3)3 であり、式中のyが0.5未満である、請求の範囲第1項記載の単結晶。 5.当該単結晶がドープされていて、一般式 M4Ln1-zNdzO(BO3)3 (この式中、MとLnは上に示した意味を有し、zは最大で0.2に等しい)を 満たしている、請求の範囲第1項から第4項までの1項に記載の単結晶。 6.一般式 M4Ln1-zNdzO(BO3)3 (この式中、MとLnは請求の範囲第1項〜第5項で定義されている意味のうち の一つを有する)の単結晶の利用。 7.MがCaであり、LnがGd又はLaであり、ドーパントがNdである、 請求の範囲第6項に記載の単結晶の自己周波数2倍化レーザーの作製への利用。 8.当該結晶を分割レーザー(separate laser)のための周波数2倍器として 使用する、請求の範囲第1項から第4項までの1項に記載の単結晶の利用。 9.請求の範囲第1項から第4項までの1項に記載の単結晶の光パラメトリッ ク発振器としての利用。 10.請求の範囲第1項から第4項までの1項に記載の単結晶の二つの分割レー ザーのための周波数ミキサーとしての利用。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR95/01963 | 1995-02-21 | ||
FR9501963A FR2730828B1 (fr) | 1995-02-21 | 1995-02-21 | Cristaux non lineaires et leurs applications |
PCT/FR1996/000255 WO1996026464A1 (fr) | 1995-02-21 | 1996-02-16 | Cristaux non lineaires et leurs applications |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH09512354A true JPH09512354A (ja) | 1997-12-09 |
JP3875265B2 JP3875265B2 (ja) | 2007-01-31 |
Family
ID=9476340
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP52544496A Expired - Lifetime JP3875265B2 (ja) | 1995-02-21 | 1996-02-16 | 非線形結晶及びそれらの利用 |
Country Status (11)
Country | Link |
---|---|
US (1) | US6083319A (ja) |
EP (1) | EP0756719B1 (ja) |
JP (1) | JP3875265B2 (ja) |
CN (1) | CN1150427C (ja) |
AT (1) | ATE249061T1 (ja) |
DE (1) | DE69629770T2 (ja) |
FR (1) | FR2730828B1 (ja) |
HU (1) | HU219305B (ja) |
PL (1) | PL316947A1 (ja) |
RU (1) | RU2169802C2 (ja) |
WO (1) | WO1996026464A1 (ja) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE69933017T2 (de) * | 1998-03-27 | 2007-03-15 | Japan Science And Technology Agency, Kawaguchi | WELLENLÄNGENUMWANDLUNGSKRISTALL, VERFAHREN und Gerät ZUR ERZEUGUNG VON LASERSTRAHLEN |
US6185231B1 (en) | 1999-02-02 | 2001-02-06 | University Of Central Florida | Yb-doped:YCOB laser |
US6185236B1 (en) | 1999-02-02 | 2001-02-06 | University Of Central Florida | Self frequency double nd-doped: YCOB LASER |
US6676853B1 (en) * | 1999-10-27 | 2004-01-13 | Sumitomo Chemical Company, Limited | Phosphor for vacuum ultraviolet excitation material |
US7179405B2 (en) | 2002-10-01 | 2007-02-20 | The Regents Of The University Of California | Nonlinear optical crystal optimized for Ytterbium laser host wavelengths |
US7378042B2 (en) * | 2002-10-01 | 2008-05-27 | Lawrence Livermore National Security, Llc | Nonlinear optical crystal optimized for Ytterbium laser host wavelengths |
US20050190805A1 (en) * | 2003-06-30 | 2005-09-01 | Scripsick Michael P. | Doped stoichiometric lithium niobate and lithium tantalate for self-frequency conversion lasers |
US7622851B2 (en) * | 2006-01-17 | 2009-11-24 | The Penn State Research Foundation | High temperature piezoelectric material |
CN101514489B (zh) * | 2008-02-22 | 2012-03-07 | 中国科学院理化技术研究所 | 含稀土离子的氟硼酸盐、晶体及晶体的生长方法和用途 |
CN101798707B (zh) * | 2009-02-11 | 2012-06-13 | 中国科学院理化技术研究所 | 非线性光学晶体BaMgBO3F及其制备方法和用途 |
CN101942699A (zh) * | 2010-09-03 | 2011-01-12 | 山东大学 | 一种具有倍频效应的硼酸钙氧盐晶体的生长方法 |
US10133148B2 (en) * | 2015-04-13 | 2018-11-20 | University Of Houston System | Nonlinear optical material and methods of fabrication |
CN109378691B (zh) * | 2018-12-11 | 2021-06-01 | 山东大学 | 一种基于声子带边发射的全固态大功率板条激光器 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5027361A (en) * | 1988-06-21 | 1991-06-25 | Board Of Trustees Of Leland Stanford, Jr., University | Efficient laser harmonic generation employing a low-loss external optical resonator |
US5030851A (en) * | 1990-07-13 | 1991-07-09 | Hoya Optics Inc. | (REx Y1-x Al3 (BO3)4 crystals in electrooptic and nonlinear devices |
US5243615A (en) * | 1991-11-20 | 1993-09-07 | Laserscope | High-powered intracavity non-linear optic laser |
CN1027514C (zh) * | 1992-04-23 | 1995-01-25 | 中国科学技术大学 | 三硼酸铯单晶生长方法及用其制作的非线性光学器件 |
US5343327A (en) * | 1993-11-05 | 1994-08-30 | University Of Central Florida | RbNbB2 O6 crystal and its nonlinear optical devices |
US5611946A (en) * | 1994-02-18 | 1997-03-18 | New Wave Research | Multi-wavelength laser system, probe station and laser cutter system using the same |
US5592325A (en) * | 1994-07-29 | 1997-01-07 | Litton Systems, Inc. | Method and apparatus for laser beam management with frequency converting compounds |
-
1995
- 1995-02-21 FR FR9501963A patent/FR2730828B1/fr not_active Expired - Lifetime
-
1996
- 1996-02-16 US US08/722,150 patent/US6083319A/en not_active Expired - Lifetime
- 1996-02-16 JP JP52544496A patent/JP3875265B2/ja not_active Expired - Lifetime
- 1996-02-16 PL PL96316947A patent/PL316947A1/xx unknown
- 1996-02-16 RU RU96122651/12A patent/RU2169802C2/ru active
- 1996-02-16 EP EP96904152A patent/EP0756719B1/fr not_active Expired - Lifetime
- 1996-02-16 CN CNB961901152A patent/CN1150427C/zh not_active Expired - Lifetime
- 1996-02-16 AT AT96904152T patent/ATE249061T1/de not_active IP Right Cessation
- 1996-02-16 HU HU9602910A patent/HU219305B/hu unknown
- 1996-02-16 DE DE69629770T patent/DE69629770T2/de not_active Expired - Lifetime
- 1996-02-16 WO PCT/FR1996/000255 patent/WO1996026464A1/fr active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
RU2169802C2 (ru) | 2001-06-27 |
FR2730828A1 (fr) | 1996-08-23 |
WO1996026464A1 (fr) | 1996-08-29 |
CN1146812A (zh) | 1997-04-02 |
EP0756719B1 (fr) | 2003-09-03 |
EP0756719A1 (fr) | 1997-02-05 |
CN1150427C (zh) | 2004-05-19 |
DE69629770T2 (de) | 2004-07-01 |
US6083319A (en) | 2000-07-04 |
FR2730828B1 (fr) | 1997-04-30 |
DE69629770D1 (de) | 2003-10-09 |
HUP9602910A3 (en) | 1998-04-28 |
HU219305B (en) | 2001-03-28 |
HUP9602910A2 (en) | 1997-05-28 |
PL316947A1 (en) | 1997-02-17 |
ATE249061T1 (de) | 2003-09-15 |
JP3875265B2 (ja) | 2007-01-31 |
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