JPH06234079A - Production of copper plate with cooling hole - Google Patents
Production of copper plate with cooling holeInfo
- Publication number
- JPH06234079A JPH06234079A JP5690992A JP5690992A JPH06234079A JP H06234079 A JPH06234079 A JP H06234079A JP 5690992 A JP5690992 A JP 5690992A JP 5690992 A JP5690992 A JP 5690992A JP H06234079 A JPH06234079 A JP H06234079A
- Authority
- JP
- Japan
- Prior art keywords
- copper plate
- groove
- stainless steel
- austenitic stainless
- steel pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Pressure Welding/Diffusion-Bonding (AREA)
- Blast Furnaces (AREA)
Abstract
Description
【０００１】[0001]
【産業上の利用分野】本発明は、冷却板や電極として用
いられる冷却孔付き銅板に於いて、その冷却孔を任意の
形状に、しかも容易に製作出来る製造方法に関するもの
である。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method of manufacturing a copper plate with cooling holes, which is used as a cooling plate or an electrode, in which the cooling holes can be formed in an arbitrary shape and can be easily manufactured.
【０００２】[0002]
【従来の技術】この種の冷却孔付き銅板の製造方法とし
ては、従来から図２に示す様に、冷却孔となるべき溝３
を有する銅板１と銅板２とを、両銅板の接合面４にろう
材を施してろう付けすることにより行われていた。2. Description of the Related Art As a conventional method of manufacturing a copper plate with cooling holes of this type, as shown in FIG.
The copper plate 1 and the copper plate 2 having the above are brazed by applying a brazing material to the joint surface 4 of both copper plates.
【０００３】[0003]
【発明が解決しようとする課題】上記従来方法で製造さ
れた冷却孔き銅板は、ろう付けにより接合面４の全面に
渡って充分な接合を行うことが難しく、従って充分な気
密性、水密性を安定して得ることが困難であった。また
接合部の強度はろう材の強度により律せられるため、充
分でなかった。この様な理由から、経済的にも安定した
品質のものを確実に得ることが難しく、コスト、歩留り
の面でも問題があった。The cooling perforated copper sheet produced by the above-mentioned conventional method is difficult to perform sufficient joining over the entire joining surface 4 by brazing, and thus, sufficient airtightness and watertightness. Was difficult to obtain stably. Further, the strength of the joint portion is limited by the strength of the brazing filler metal, and thus was not sufficient. For these reasons, it is difficult to obtain economically stable quality with certainty, and there are problems in terms of cost and yield.
【０００４】本発明は上記問題を解消し、任意形状の冷
却孔を有する銅板を容易でしかも安定的に製造すること
が出来る製造方法を提供することを目的としている。An object of the present invention is to solve the above problems and to provide a manufacturing method capable of easily and stably manufacturing a copper plate having a cooling hole of an arbitrary shape.
【０００５】[0005]
【課題を解決するための手段】上記目的を達成するため
に、本発明は下記の如き手段を採用するものである。即
ち、図１に示す様に、一対の銅板の中少なくとも一方の
銅板１の表面に、最終的に冷却孔となるべき溝３を形成
し、該溝３内にオーステナイト系ステンレス鋼製パイプ
５を配設し、他方の銅板２と合わせてキャニングした後
に、熱間等方圧加圧装置により拡散接合させて一体化し
た後、該オーステナイト系ステンレス鋼製パイプを硫酸
溶液中で除去することで冷却孔付き銅板を製造する方法
である。In order to achieve the above object, the present invention employs the following means. That is, as shown in FIG. 1, a groove 3 to be a cooling hole finally is formed on the surface of at least one of the pair of copper plates, and an austenitic stainless steel pipe 5 is formed in the groove 3. After arranging and performing canning together with the other copper plate 2, it is diffusion-bonded by a hot isotropic pressure pressurizer and integrated, and then cooled by removing the austenitic stainless steel pipe in a sulfuric acid solution. It is a method of manufacturing a copper plate with holes.
【０００６】なお、最終的に得られる冷却孔は、必ずし
も一体化した銅板の端面で開口する必要はなく、一体化
した銅板の表面に開口させることも出来る。この様な場
合には、溝３を銅板１の端まで形成させずに途中までと
し、その溝３の始端及び終端の位置に、あるいは該位置
と相対する銅板２上の位置に孔をあけることで開口部と
することが可能である。The cooling holes finally obtained do not necessarily have to be opened at the end faces of the integrated copper plate, but can be opened at the surface of the integrated copper plate. In such a case, the groove 3 is not formed up to the end of the copper plate 1 but is formed halfway, and holes are formed at the start and end positions of the groove 3 or at positions on the copper plate 2 opposite to the position. Can be used as the opening.
【０００７】本発明方法に於いて、溝３の内にオーステ
ナイト系ステンレス鋼製パイプ５を配設するのは次の様
な理由による。即ち、銅板１と銅板２とを熱間等方圧加
圧装置により拡散接合する場合に、これらの接合強度を
充分なものにし、気密性、水密性を確保するためには、
熱間等方圧加圧処理の温度及び圧力を高くするのがよ
い。しかし乍ら、これらの条件を高くすると、冷却孔と
なるべき溝３が熱間等方圧加圧処理中に変形、消失して
しまう。これは熱間等方圧加圧処理時には銅板１及び２
はキャニングされ、溝３内は真空とされているからであ
る。そこで、この様な変形、消失を防止するために、銅
板よりも高温で強度を有するオーステナイト系ステンレ
ス鋼製パイプ５を溝３を支えることを目的として配設す
るものである。なお、このパイプは、銅板よりも高温強
度に優れるものであれば、他の鋼材でも良いが特に細径
のものが入手し易いとの理由から、オーステナイト系ス
テンレス鋼製とした。In the method of the present invention, the austenitic stainless steel pipe 5 is arranged in the groove 3 for the following reason. That is, in the case where the copper plate 1 and the copper plate 2 are diffusion-bonded by the hot isostatic pressing device, in order to secure sufficient bonding strength between them and to secure airtightness and watertightness,
It is preferable to increase the temperature and pressure of the hot isostatic pressing process. However, if these conditions are raised, the groove 3 to be the cooling hole is deformed and disappears during the hot isostatic pressing. This is due to the copper plates 1 and 2 during hot isostatic pressing.
The reason is that the inside of the groove 3 is canned and the inside of the groove 3 is evacuated. Therefore, in order to prevent such deformation and disappearance, an austenitic stainless steel pipe 5 having strength at a temperature higher than that of the copper plate is provided for the purpose of supporting the groove 3. This pipe is made of austenitic stainless steel because other steel materials may be used as long as it has higher strength at high temperature than a copper plate, but one with a particularly small diameter is easily available.
【０００８】また、オーステナイト系ステンレス鋼を、
パイプ材の形状で用いたのは、硫酸により除去するとき
に、もしこれを棒材あるいは線材とした場合には、その
端面のみからの溶解により除去されることとなり、非常
に長時間を必要とするものに対して、パイプ材であれ
ば、パイプ材内面全面から溶解が進行し、パイプ材の肉
厚が薄くなっていくという方向での除去となり、短時間
での除去が可能となるからである。Further, austenitic stainless steel is
The shape of the pipe used is that when it is removed with sulfuric acid, if it is made into a rod or wire, it will be removed by dissolution from only its end face, and it will take a very long time. On the other hand, if it is a pipe material, it will be removed in the direction that the melting progresses from the entire inner surface of the pipe material and the wall thickness of the pipe material becomes thinner, which enables removal in a short time. is there.
【０００９】オーステナイト系ステンレス鋼製パイプを
除去するのに硫酸を用いたのは、塩酸、硝酸などの他の
溶液では、パイプと共に銅板も溶解するのに対し、硫酸
を用いた場合には、パイプのみが溶解し、銅板は溶解し
ないという結果が得られたからである。なお、オーステ
ナイト系ステンレス鋼製パイプを除去するのは、冷却効
率を高めるためである。つまり、オーステナイト系ステ
ンレス鋼製パイプが残存していると、銅板と冷却媒体と
の間に熱伝導度の良くない層が存在することになり、冷
却効率が低下することになるからである。Sulfuric acid was used to remove the austenitic stainless steel pipe because copper is dissolved together with the pipe in other solutions such as hydrochloric acid and nitric acid, whereas sulfuric acid is used in the pipe. This is because only the result was obtained, and the copper plate was not. The reason why the austenitic stainless steel pipe is removed is to enhance the cooling efficiency. That is, if the austenitic stainless steel pipe remains, a layer having poor thermal conductivity exists between the copper plate and the cooling medium, and the cooling efficiency decreases.
【００１０】[0010]
【実施例】以下本発明の実施例について述べる。１００
mm×１００mm，厚さ５mmの銅板表面上に、深さ及び幅２
mmの溝を形成し、その溝内に外径１．５mm，肉厚０．２
mmのオーステナイト系ステンレス鋼製パイプを配設し、
１００mm×１００mm，厚さ２mmの銅板と合わせてキャニ
ングした後、熱間等方圧加圧装置により拡散接合させ
た。このとき熱間等方圧加圧処理条件は、温度７００
℃，圧力３００kgf/cm2 ，時間２時間である。EXAMPLES Examples of the present invention will be described below. 100
2 mm depth and width on the surface of a copper plate of mm x 100 mm and thickness of 5 mm
mm groove is formed, the outer diameter is 1.5 mm, and the wall thickness is 0.2.
mm austenitic stainless steel pipe is installed,
After performing canning together with a copper plate of 100 mm × 100 mm and a thickness of 2 mm, diffusion bonding was performed by a hot isostatic pressing device. At this time, the hot isostatic pressing condition is that the temperature is 700
° C., a pressure 300 kgf / cm 2, the time 2 hours.
【００１１】その後、液温７０℃の１０％硫酸溶液中に
浸漬し、オーステナイト系ステンレス鋼製パイプを除去
した。この時、パイプの溶解速度を速めるために、定量
ポンプを用い、該硫酸溶液をパイプ内に供給した。その
結果、該パイプは、約２４時間で除去することが出来
た。パイプ除去後、一体化した銅板を切断し断面を観察
した結果パイプのみが完全に除去され、銅板は溶解して
ないことを確認した。また、銅板どうしの接合は、曲げ
試験により、充分に接合されていることを確認した。Then, it was immersed in a 10% sulfuric acid solution having a liquid temperature of 70 ° C. to remove the austenitic stainless steel pipe. At this time, in order to accelerate the dissolution rate of the pipe, the sulfuric acid solution was supplied into the pipe using a metering pump. As a result, the pipe could be removed in about 24 hours. After removing the pipe, the integrated copper plate was cut and the cross section was observed. As a result, it was confirmed that only the pipe was completely removed and the copper plate was not melted. Further, it was confirmed by a bending test that the copper plates were joined to each other sufficiently.
【００１２】[0012]
【発明の効果】以上説明して来た如く、本発明方法によ
れば、冷却孔となるべき溝の形成は、銅板表面に行うの
でその形状、大きさは自由に選定することが出来、該溝
内にオーステナイト系ステンレス鋼製パイプを配設して
熱間等方圧加圧装置で拡散接合するので溝が変形あるい
は消失することなくパイプのみを硫酸にて溶解除去すれ
ば完全な冷却孔が開いた銅板を得ることが出来る。ま
た、銅板どおしの接合も充分で確実に気密性、水密性を
有する冷却孔を得ることが出来る。なお、本発明方法は
一対の銅板を熱間等方圧加圧処理により拡散接合する方
法を採用するので、処理時に於ける圧力は全方位からか
かるため、複雑な形状に対しても、変形させることなく
拡散接合が出来、従って平坦な銅板のみでなく、わん曲
した銅板など、複雑な形状のものも製造出来るという利
点がある。As described above, according to the method of the present invention, since the groove to be the cooling hole is formed on the surface of the copper plate, its shape and size can be freely selected. An austenitic stainless steel pipe is placed in the groove and diffusion bonding is performed with a hot isotropic pressure pressurizer.Therefore, if the pipe is melted and removed with sulfuric acid without deformation or disappearance of the groove, a perfect cooling hole You can get an open copper plate. Moreover, the joining of copper plates is sufficient, and a cooling hole having airtightness and watertightness can be reliably obtained. Since the method of the present invention adopts a method of diffusion bonding a pair of copper plates by hot isostatic pressing, the pressure at the time of processing is applied from all directions, so that even a complicated shape is deformed. There is an advantage that diffusion bonding can be performed without using it, so that not only a flat copper plate but also a curved copper plate having a complicated shape can be manufactured.
【図１】本発明方法の概略を示す説明図である。FIG. 1 is an explanatory view showing the outline of the method of the present invention.
【図２】従来方法の概略を示す説明図である。FIG. 2 is an explanatory diagram showing an outline of a conventional method.
１ 銅板 ２ 銅板 ３ 溝 ５ オーステナイト系ステンレス鋼製パイプ 1 Copper plate 2 Copper plate 3 Groove 5 Austenitic stainless steel pipe
─────────────────────────────────────────────────────
─────────────────────────────────────────────────── ───
【手続補正書】[Procedure amendment]
【提出日】平成５年１０月１４日[Submission date] October 14, 1993
【手続補正１】[Procedure Amendment 1]
【補正対象書類名】明細書[Document name to be amended] Statement
【補正対象項目名】図面の詳細な説明[Name of item to be corrected] Detailed explanation of the drawing
【補正方法】変更[Correction method] Change
【補正内容】[Correction content]
【図面の簡単な説明】[Brief description of drawings]
【図１】本発明方法の概略を示す説明図である。FIG. 1 is an explanatory view showing the outline of the method of the present invention.
【符号の説明】 １ 銅板 ２ 銅板 ３ 溝 ５ オーステナイト系ステンレス鋼製パイプ[Explanation of symbols] 1 copper plate 2 copper plate 3 groove 5 austenitic stainless steel pipe
Claims (1)
面に溝を形成し、該溝内にオーステナイト系ステンレス
鋼製パイプを配設し、他方の銅板と熱間等方圧加圧装置
により拡散接合して一体化させた後、該オーステナイト
系ステンレス鋼製パイプを硫酸溶液中で除去することで
冷却孔を形成することを特徴とする冷却孔付き銅板の製
造方法。1. A groove is formed on at least one copper plate surface of a pair of copper plates, an austenitic stainless steel pipe is arranged in the groove, and the other copper plate is diffused by a hot isostatic pressing device. A method for manufacturing a copper plate with cooling holes, comprising forming cooling holes by removing the austenitic stainless steel pipe in a sulfuric acid solution after joining and integrating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5690992A JP3188745B2 (en) | 1992-02-07 | 1992-02-07 | Manufacturing method of copper plate with cooling holes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5690992A JP3188745B2 (en) | 1992-02-07 | 1992-02-07 | Manufacturing method of copper plate with cooling holes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH06234079A true JPH06234079A (en) | 1994-08-23 |
| JP3188745B2 JP3188745B2 (en) | 2001-07-16 |
Family
ID=13040590
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5690992A Expired - Lifetime JP3188745B2 (en) | 1992-02-07 | 1992-02-07 | Manufacturing method of copper plate with cooling holes |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP3188745B2 (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1998001584A1 (en) * | 1996-07-09 | 1998-01-15 | Nippon Steel Corporation | Stave for cooling of blast furnace walls and method of manufacturing same |
| WO2003010341A1 (en) * | 2001-07-24 | 2003-02-06 | Nippon Steel Corporation | Shaft furnace-use stave cooler |
| KR101360127B1 (en) * | 2006-04-18 | 2014-02-11 | 풀 부르스 에스.에이. | Method of manufacturing a stave cooler for a metallurgical furnace and a resulting stave cooler |
| JP2014517179A (en) * | 2011-03-10 | 2014-07-17 | ウオーターズ・テクノロジーズ・コーポレイシヨン | System and method for cooling a chromatography pump head |
| JP2015528888A (en) * | 2012-07-09 | 2015-10-01 | ケイエムイー・ジャーマニー・ゲゼルシャフト・ミト・ベシュレンクテル・ハフツング・ウント・コンパニー・コマンデイトゲゼルシャフト | Cooling element for melting furnace |
| US20150283647A1 (en) * | 2012-10-18 | 2015-10-08 | Asahi Co., Ltd. | Method of manufacturing composite metal material, method of manufacturing mold, method of manufacturing metal product, and composite metal material |
-
1992
- 1992-02-07 JP JP5690992A patent/JP3188745B2/en not_active Expired - Lifetime
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1998001584A1 (en) * | 1996-07-09 | 1998-01-15 | Nippon Steel Corporation | Stave for cooling of blast furnace walls and method of manufacturing same |
| GB2331142A (en) * | 1996-07-09 | 1999-05-12 | Nippon Steel Corp | Stave for cooling of blast furnace walls and method of manufacturing same |
| AU709347B2 (en) * | 1996-07-09 | 1999-08-26 | Nippon Steel Corporation | Stave for cooling blast furnace wall and method for producing the same |
| US6126893A (en) * | 1996-07-09 | 2000-10-03 | Nippon Steel Corporation | Stave for cooling of blast furnace walls and method of manufacturing same |
| WO2003010341A1 (en) * | 2001-07-24 | 2003-02-06 | Nippon Steel Corporation | Shaft furnace-use stave cooler |
| KR101360127B1 (en) * | 2006-04-18 | 2014-02-11 | 풀 부르스 에스.에이. | Method of manufacturing a stave cooler for a metallurgical furnace and a resulting stave cooler |
| JP2014517179A (en) * | 2011-03-10 | 2014-07-17 | ウオーターズ・テクノロジーズ・コーポレイシヨン | System and method for cooling a chromatography pump head |
| US9492764B2 (en) | 2011-03-10 | 2016-11-15 | Waters Technologies Corporation | System and method of cooling a pump head used in chromatography |
| JP2015528888A (en) * | 2012-07-09 | 2015-10-01 | ケイエムイー・ジャーマニー・ゲゼルシャフト・ミト・ベシュレンクテル・ハフツング・ウント・コンパニー・コマンデイトゲゼルシャフト | Cooling element for melting furnace |
| US10082336B2 (en) | 2012-07-09 | 2018-09-25 | Kme Germany Gmbh & Co. Kg | Cooling element for a melting furnace |
| US20150283647A1 (en) * | 2012-10-18 | 2015-10-08 | Asahi Co., Ltd. | Method of manufacturing composite metal material, method of manufacturing mold, method of manufacturing metal product, and composite metal material |
| US9604307B2 (en) * | 2012-10-18 | 2017-03-28 | Asahi Co., Ltd. | Method of manufacturing composite metal material, method of manufacturing mold, method of manufacturing metal product, and composite metal material |
Also Published As
| Publication number | Publication date |
|---|---|
| JP3188745B2 (en) | 2001-07-16 |
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