JPH0557973B2 - - Google Patents
Info
- Publication number
- JPH0557973B2 JPH0557973B2 JP60040023A JP4002385A JPH0557973B2 JP H0557973 B2 JPH0557973 B2 JP H0557973B2 JP 60040023 A JP60040023 A JP 60040023A JP 4002385 A JP4002385 A JP 4002385A JP H0557973 B2 JPH0557973 B2 JP H0557973B2
- Authority
- JP
- Japan
- Prior art keywords
- chloride
- alkyl
- reaction
- alcohol
- zinc chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 claims description 43
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 26
- 235000005074 zinc chloride Nutrition 0.000 claims description 22
- 239000011592 zinc chloride Substances 0.000 claims description 22
- 238000006243 chemical reaction Methods 0.000 claims description 19
- 150000001348 alkyl chlorides Chemical class 0.000 claims description 15
- 125000005233 alkylalcohol group Chemical group 0.000 claims description 14
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 10
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 239000007789 gas Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 238000006555 catalytic reaction Methods 0.000 claims description 2
- 239000007791 liquid phase Substances 0.000 claims description 2
- 239000012071 phase Substances 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 238000005660 chlorination reaction Methods 0.000 claims 1
- 230000002194 synthesizing effect Effects 0.000 claims 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 16
- 239000000047 product Substances 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- 239000000243 solution Substances 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 4
- 238000004821 distillation Methods 0.000 description 4
- 239000012452 mother liquor Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- SNMVRZFUUCLYTO-UHFFFAOYSA-N n-propyl chloride Chemical compound CCCCl SNMVRZFUUCLYTO-UHFFFAOYSA-N 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000012374 esterification agent Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 229960004592 isopropanol Drugs 0.000 description 1
- ULYZAYCEDJDHCC-UHFFFAOYSA-N isopropyl chloride Chemical compound CC(C)Cl ULYZAYCEDJDHCC-UHFFFAOYSA-N 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 235000011007 phosphoric acid Nutrition 0.000 description 1
- 150000003016 phosphoric acids Chemical class 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60040023A JPS61200933A (ja) | 1985-02-28 | 1985-02-28 | 塩化アルキルの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60040023A JPS61200933A (ja) | 1985-02-28 | 1985-02-28 | 塩化アルキルの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61200933A JPS61200933A (ja) | 1986-09-05 |
| JPH0557973B2 true JPH0557973B2 (de) | 1993-08-25 |
Family
ID=12569303
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60040023A Granted JPS61200933A (ja) | 1985-02-28 | 1985-02-28 | 塩化アルキルの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61200933A (de) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103265399A (zh) * | 2013-05-20 | 2013-08-28 | 张家港市振方化工有限公司 | 基于催化剂的氯代特戊烷制备工艺 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57156423A (en) * | 1981-02-26 | 1982-09-27 | Hoechst Ag | Manufacture of gas containing methylchloride |
-
1985
- 1985-02-28 JP JP60040023A patent/JPS61200933A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS57156423A (en) * | 1981-02-26 | 1982-09-27 | Hoechst Ag | Manufacture of gas containing methylchloride |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS61200933A (ja) | 1986-09-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2102379C1 (ru) | Способ получения уксусной кислоты | |
| US5935541A (en) | Process for manufacture of lithium hexafluorophosphate | |
| US4299981A (en) | Preparation of formic acid by hydrolysis of methyl formate | |
| JPS6125013B2 (de) | ||
| US3923884A (en) | Process for producing DL-tartaric acid | |
| US4003984A (en) | Production of sulfuryl fluoride | |
| JPH0557973B2 (de) | ||
| JPH02169550A (ja) | ジアルキルカーボネートの連続製造法 | |
| JPH03184933A (ja) | ヘミアセタール化合物の製造方法 | |
| US4480127A (en) | Process for the production of variable amounts of DPA and aniline using only phenol and ammonia as the feedstock | |
| KR860001889B1 (ko) | 2,3-디클로로프로피오니트릴의 제법 | |
| US4808761A (en) | Demethanolization of aqueous CH3 OH/HCl solutions | |
| JP2747780B2 (ja) | 非対称ジエステルの製造方法 | |
| JP3175334B2 (ja) | Ｎ−（α−アルコキシエチル）−カルボン酸アミドの製造法 | |
| WO1992018452A1 (en) | Preparation of trialkylacetic acids, particularly of pivalic acid, using lewis acid catalysis | |
| US4005125A (en) | Preparation of haloalkyl esters | |
| JPH07116096B2 (ja) | 高純度０−トルイル酸の製造方法 | |
| EP0241755A1 (de) | Verfahren zur kontinuierlichen Herstellung von Phthalodinitril | |
| JP2533980B2 (ja) | 過プロピオン酸の製造方法 | |
| US3957730A (en) | Recovery of pure 2-methyl-2-hydroxy-heptanone-6 | |
| JP3028100B2 (ja) | ２，６−ナフタレンジカルボン酸ジメチルの製造法 | |
| JPH01165560A (ja) | アミノ酸のエステル化方法 | |
| JPS59157045A (ja) | ヘキサフルオロアセトン水和物の脱水方法 | |
| JPS58144328A (ja) | 塩化アルキルの製造方法 | |
| JP2003300918A (ja) | ジアルキルカーボネートとグリコールの連続同時製造方法 |