JPH0522691B2 - - Google Patents
Info
- Publication number
- JPH0522691B2 JPH0522691B2 JP16976084A JP16976084A JPH0522691B2 JP H0522691 B2 JPH0522691 B2 JP H0522691B2 JP 16976084 A JP16976084 A JP 16976084A JP 16976084 A JP16976084 A JP 16976084A JP H0522691 B2 JPH0522691 B2 JP H0522691B2
- Authority
- JP
- Japan
- Prior art keywords
- palladium acetate
- palladium
- acetic acid
- mixture
- nitrogen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 33
- YJVFFLUZDVXJQI-UHFFFAOYSA-L palladium(ii) acetate Chemical compound [Pd+2].CC([O-])=O.CC([O-])=O YJVFFLUZDVXJQI-UHFFFAOYSA-L 0.000 claims description 22
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 11
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 229910017604 nitric acid Inorganic materials 0.000 claims description 8
- 239000011261 inert gas Substances 0.000 claims description 7
- 229910052763 palladium Inorganic materials 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 21
- 229910052757 nitrogen Inorganic materials 0.000 description 10
- 239000013078 crystal Substances 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000007800 oxidant agent Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 229910002651 NO3 Inorganic materials 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- -1 nitrate radicals Chemical compound 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16976084A JPS6147440A (ja) | 1984-08-14 | 1984-08-14 | 酢酸パラジウムの調製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP16976084A JPS6147440A (ja) | 1984-08-14 | 1984-08-14 | 酢酸パラジウムの調製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6147440A JPS6147440A (ja) | 1986-03-07 |
| JPH0522691B2 true JPH0522691B2 (enExample) | 1993-03-30 |
Family
ID=15892341
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP16976084A Granted JPS6147440A (ja) | 1984-08-14 | 1984-08-14 | 酢酸パラジウムの調製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6147440A (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5045015B2 (ja) * | 2006-07-28 | 2012-10-10 | セイコーエプソン株式会社 | ギ酸銅の製造方法、銅粒子の製造方法および配線基板の製造方法 |
| CN102320951A (zh) * | 2011-06-13 | 2012-01-18 | 陕西瑞科新材料股份有限公司 | 一种醋酸钯三聚体的制备方法 |
| EP2987571B1 (de) * | 2014-08-19 | 2018-08-15 | Heraeus Deutschland GmbH & Co. KG | Verfahren zur Herstellung von aktivem Palladium(0)-Pulver, aktives Palladium(0)-Pulver und seiner Verwendung für die Herstellung eines Palladiumsalzes |
-
1984
- 1984-08-14 JP JP16976084A patent/JPS6147440A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6147440A (ja) | 1986-03-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3726915A (en) | Phthalic acid purification with copper activated palladium on carbon catalysts | |
| JPS63222011A (ja) | 多結晶シリコンの製造方法 | |
| JPH0522691B2 (enExample) | ||
| JPS6019905B2 (ja) | ピリジン及び置換ピリジンの製造方法 | |
| US4465635A (en) | Manufacture of palladous carboxylates | |
| US3076030A (en) | Process for the preparation of acetylaminophenols | |
| JPH03173840A (ja) | クロロトリフルオロエチレンの製造方法 | |
| JP3410121B2 (ja) | アンモニアの精製方法 | |
| JPS5836910A (ja) | リン酸から有機不純物を除去する方法 | |
| JPS5833846B2 (ja) | ホルムアルデヒドの製法 | |
| US4372934A (en) | Production of isocyanic acid | |
| JPH0413663A (ja) | ジカルボン酸イミド誘導体の製造法 | |
| JPH03249945A (ja) | 二酸化炭素変換用アモルファス合金触媒 | |
| JP3522785B2 (ja) | 二酸化炭素の精製方法 | |
| JPS6185363A (ja) | ピリジンの製法 | |
| SU691396A1 (ru) | Способ очистки фосфорной кислоты | |
| JPS6271549A (ja) | 担持金属触媒の粒子径の制御方法 | |
| JPH0411988A (ja) | 滅菌用浄化剤の製造方法 | |
| JP2732611B2 (ja) | 排気浄化触媒製造用ロジウム含有溶液の調製方法 | |
| JPH0556184B2 (enExample) | ||
| JPH057216Y2 (enExample) | ||
| CN113651737A (zh) | 一种催化选择性制备2,4’-二羟基二苯砜的方法 | |
| JPH0853720A (ja) | コレクターメタル中の白金族金属の溶解方法 | |
| JPS5869718A (ja) | パラジウム・ド−プ・銀触媒でｈｃｎを接触酸化するｈｎｃｏの製造法 | |
| JPS5810382B2 (ja) | トリアミノグアニジンシヨウサンエンノ セイホウ |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |