JPH04197402A - 混合物の向流分離方法及び装置 - Google Patents
混合物の向流分離方法及び装置Info
- Publication number
- JPH04197402A JPH04197402A JP2325566A JP32556690A JPH04197402A JP H04197402 A JPH04197402 A JP H04197402A JP 2325566 A JP2325566 A JP 2325566A JP 32556690 A JP32556690 A JP 32556690A JP H04197402 A JPH04197402 A JP H04197402A
- Authority
- JP
- Japan
- Prior art keywords
- solid particles
- interest
- solution
- component
- column
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000926 separation method Methods 0.000 title claims description 61
- 239000000203 mixture Substances 0.000 title claims description 8
- 239000002245 particle Substances 0.000 claims abstract description 172
- 239000007787 solid Substances 0.000 claims abstract description 126
- 239000007788 liquid Substances 0.000 claims description 73
- 238000000034 method Methods 0.000 claims description 21
- 238000000605 extraction Methods 0.000 claims description 19
- 239000003480 eluent Substances 0.000 claims description 18
- 230000000630 rising effect Effects 0.000 claims description 10
- 238000005086 pumping Methods 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims 1
- 230000001174 ascending effect Effects 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 70
- 239000002994 raw material Substances 0.000 description 28
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 18
- 229930091371 Fructose Natural products 0.000 description 15
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 15
- 239000005715 Fructose Substances 0.000 description 15
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 239000007864 aqueous solution Substances 0.000 description 11
- 238000005406 washing Methods 0.000 description 9
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 8
- 239000008103 glucose Substances 0.000 description 8
- 238000011084 recovery Methods 0.000 description 8
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 7
- 239000003456 ion exchange resin Substances 0.000 description 7
- 229920003303 ion-exchange polymer Polymers 0.000 description 7
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
- 229910052588 hydroxylapatite Inorganic materials 0.000 description 6
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 description 6
- 239000002002 slurry Substances 0.000 description 6
- 230000002378 acidificating effect Effects 0.000 description 5
- 230000009471 action Effects 0.000 description 5
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 102000018832 Cytochromes Human genes 0.000 description 4
- 108010052832 Cytochromes Proteins 0.000 description 4
- 239000010954 inorganic particle Substances 0.000 description 4
- 239000008057 potassium phosphate buffer Substances 0.000 description 4
- 239000011347 resin Substances 0.000 description 4
- 229920005989 resin Polymers 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical group [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 239000007853 buffer solution Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010828 elution Methods 0.000 description 2
- 229940088598 enzyme Drugs 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 230000002093 peripheral effect Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 238000007873 sieving Methods 0.000 description 2
- 239000000758 substrate Substances 0.000 description 2
- 229920000936 Agarose Polymers 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 241000021559 Dicerandra Species 0.000 description 1
- 239000007836 KH2PO4 Substances 0.000 description 1
- 235000010654 Melissa officinalis Nutrition 0.000 description 1
- 102000016943 Muramidase Human genes 0.000 description 1
- 108010014251 Muramidase Proteins 0.000 description 1
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 241000269821 Scombridae Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000013522 chelant Substances 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000004042 decolorization Methods 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000007863 gel particle Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 229960000274 lysozyme Drugs 0.000 description 1
- 235000010335 lysozyme Nutrition 0.000 description 1
- 239000004325 lysozyme Substances 0.000 description 1
- 235000020640 mackerel Nutrition 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 239000011268 mixed slurry Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002808 molecular sieve Substances 0.000 description 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 description 1
- 235000019796 monopotassium phosphate Nutrition 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 239000011146 organic particle Substances 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/02—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor with moving adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/18—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns
- B01D15/1892—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to flow patterns the sorbent material moving as a whole, e.g. continuous annular chromatography, true moving beds or centrifugal chromatography
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Extraction Or Liquid Replacement (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2325566A JPH04197402A (ja) | 1990-11-29 | 1990-11-29 | 混合物の向流分離方法及び装置 |
| DE19914193006 DE4193006T (enrdf_load_stackoverflow) | 1990-11-29 | 1991-11-29 | |
| PCT/JP1991/001663 WO1992009352A1 (fr) | 1990-11-29 | 1991-11-29 | Procede et dispositif pour decomposer un melange par contre-courant |
| GB9216071A GB2255916A (en) | 1990-11-29 | 1992-07-28 | Method of and device for counter-flow separation of mixture |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2325566A JPH04197402A (ja) | 1990-11-29 | 1990-11-29 | 混合物の向流分離方法及び装置 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH04197402A true JPH04197402A (ja) | 1992-07-17 |
Family
ID=18178321
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2325566A Pending JPH04197402A (ja) | 1990-11-29 | 1990-11-29 | 混合物の向流分離方法及び装置 |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JPH04197402A (enrdf_load_stackoverflow) |
| DE (1) | DE4193006T (enrdf_load_stackoverflow) |
| GB (1) | GB2255916A (enrdf_load_stackoverflow) |
| WO (1) | WO1992009352A1 (enrdf_load_stackoverflow) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ZA945796B (en) * | 1993-08-13 | 1995-03-14 | Barnard Stewart Silver | Method and apparatus for extracting with liquids soluble substances from subdivided solids |
| US5891433A (en) * | 1993-08-13 | 1999-04-06 | Silver; Barnard Stewart | Extracting soluble substances from subdivided solids with a water-base liquid extraction medium |
| CN100364634C (zh) * | 2005-11-23 | 2008-01-30 | 黑龙江省计算中心 | 双螺旋连续逆流提取装置 |
| ITMI20120298A1 (it) * | 2012-02-28 | 2013-08-29 | Asi Apparecchiature Scient Innovative S | Dispositivo e procedimento per rilevare la presenza di particelle fluorescenti disperse in concentrazioni molto basse in un mezzo liquido contenuto in una cuvetta. |
| NO343574B1 (en) * | 2017-05-22 | 2019-04-08 | M&M Engine As | Method for filtration of polluted liquid, and a filtration apparatus |
| CN108554293A (zh) * | 2017-12-07 | 2018-09-21 | 滁州恒通磁电科技有限公司 | 一种磁瓦成型原料拌料装置 |
| CN109381889A (zh) * | 2018-11-26 | 2019-02-26 | 吴斌 | 一种固液易分离的生物碱萃取装置 |
| CN109794079A (zh) * | 2019-03-02 | 2019-05-24 | 孙志良 | 一种超声强化超临界流体萃取装置 |
| CN110270129A (zh) * | 2019-08-05 | 2019-09-24 | 翔宇药业股份有限公司 | 一种自动化提取装置及其在复方红衣补血口服液生产中的应用 |
| CN112619470A (zh) * | 2020-12-17 | 2021-04-09 | 黄海亮 | 一种畜牧饲料加工用均匀混合搅拌装置 |
| CN117046152B (zh) * | 2023-09-18 | 2024-05-10 | 陇西一方制药有限公司 | 一种连续逆流提取机组专用清场器 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63315139A (ja) * | 1987-06-19 | 1988-12-22 | Mitsubishi Heavy Ind Ltd | 撹拌処理装置 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5140027B1 (enrdf_load_stackoverflow) * | 1970-07-31 | 1976-11-01 | ||
| JPS493460A (enrdf_load_stackoverflow) * | 1972-04-28 | 1974-01-12 | ||
| JPS5059338U (enrdf_load_stackoverflow) * | 1973-10-05 | 1975-06-02 | ||
| LU76626A1 (enrdf_load_stackoverflow) * | 1977-01-21 | 1978-09-13 |
-
1990
- 1990-11-29 JP JP2325566A patent/JPH04197402A/ja active Pending
-
1991
- 1991-11-29 WO PCT/JP1991/001663 patent/WO1992009352A1/ja active Application Filing
- 1991-11-29 DE DE19914193006 patent/DE4193006T/de not_active Ceased
-
1992
- 1992-07-28 GB GB9216071A patent/GB2255916A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63315139A (ja) * | 1987-06-19 | 1988-12-22 | Mitsubishi Heavy Ind Ltd | 撹拌処理装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| WO1992009352A1 (fr) | 1992-06-11 |
| GB9216071D0 (en) | 1992-09-23 |
| DE4193006T (enrdf_load_stackoverflow) | 1992-12-10 |
| GB2255916A (en) | 1992-11-25 |
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