JPH0148900B2 - - Google Patents
Info
- Publication number
- JPH0148900B2 JPH0148900B2 JP12593981A JP12593981A JPH0148900B2 JP H0148900 B2 JPH0148900 B2 JP H0148900B2 JP 12593981 A JP12593981 A JP 12593981A JP 12593981 A JP12593981 A JP 12593981A JP H0148900 B2 JPH0148900 B2 JP H0148900B2
- Authority
- JP
- Japan
- Prior art keywords
- chlorophenyl
- trans
- solvent
- distilled
- organic solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 claims description 9
- 239000003960 organic solvent Substances 0.000 claims description 5
- -1 (4-chlorophenyl)-4-methylthiazoline-2-thione Chemical compound 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000007800 oxidant agent Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 9
- 150000001875 compounds Chemical class 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- WQDUMFSSJAZKTM-UHFFFAOYSA-N Sodium methoxide Chemical compound [Na+].[O-]C WQDUMFSSJAZKTM-UHFFFAOYSA-N 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 3
- 235000011118 potassium hydroxide Nutrition 0.000 description 3
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- TXAWBKBMGZKBNN-UHFFFAOYSA-N 1-(4-chlorophenyl)propan-1-ol Chemical compound CCC(O)C1=CC=C(Cl)C=C1 TXAWBKBMGZKBNN-UHFFFAOYSA-N 0.000 description 1
- ULGZDMOVFRHVEP-RWJQBGPGSA-N Erythromycin Chemical compound O([C@@H]1[C@@H](C)C(=O)O[C@@H]([C@@]([C@H](O)[C@@H](C)C(=O)[C@H](C)C[C@@](C)(O)[C@H](O[C@H]2[C@@H]([C@H](C[C@@H](C)O2)N(C)C)O)[C@H]1C)(C)O)CC)[C@H]1C[C@@](C)(OC)[C@@H](O)[C@H](C)O1 ULGZDMOVFRHVEP-RWJQBGPGSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012442 inert solvent Substances 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Thiazole And Isothizaole Compounds (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12593981A JPS5829775A (ja) | 1981-08-13 | 1981-08-13 | トランス―5―(4―クロロフェニル)―4―メチル―2―チアゾリドンの製造方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12593981A JPS5829775A (ja) | 1981-08-13 | 1981-08-13 | トランス―5―(4―クロロフェニル)―4―メチル―2―チアゾリドンの製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5829775A JPS5829775A (ja) | 1983-02-22 |
JPH0148900B2 true JPH0148900B2 (es) | 1989-10-20 |
Family
ID=14922701
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP12593981A Granted JPS5829775A (ja) | 1981-08-13 | 1981-08-13 | トランス―5―(4―クロロフェニル)―4―メチル―2―チアゾリドンの製造方法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5829775A (es) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106632131A (zh) * | 2016-09-29 | 2017-05-10 | 温州大学 | 一种噻螨酮及其制备方法 |
CN114315752A (zh) * | 2021-12-01 | 2022-04-12 | 江苏禾本生化有限公司 | 一种噻螨酮中间体的光氧化工艺 |
-
1981
- 1981-08-13 JP JP12593981A patent/JPS5829775A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS5829775A (ja) | 1983-02-22 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
SU620206A3 (ru) | Способ получени производных оксима или их солей | |
JPS6318588B2 (es) | ||
JPH0148900B2 (es) | ||
JPS6024781B2 (ja) | シス−2−ヒドロキシ−2−フエニル−r−1−シクロヘキサンカルボン酸の製造法 | |
JPH0141152B2 (es) | ||
JPS6145613B2 (es) | ||
JPS6341909B2 (es) | ||
JPS629098B2 (es) | ||
JP4582286B2 (ja) | スルホオキシアルキニルチオフェン化合物及びその製造法 | |
JPH0534347B2 (es) | ||
JP2743198B2 (ja) | シクロペンタン類 | |
JPH0452272B2 (es) | ||
JPS5944315B2 (ja) | 2−ペンチニルエ−テルの製造法 | |
EP0464218B1 (en) | Process for producing isoxazole derivative | |
US4173707A (en) | Cyclopentanol derivatives | |
EP0166650B1 (fr) | Procédé d'ouverture du cycle des gem dicyanoépoxydes et nouveaux composés obtenus par ce procédé | |
JP4018816B2 (ja) | シクロヘプテノン誘導体及びその製造方法並びにそれを利用してシクロヘプトイミダゾール誘導体を製造する方法 | |
JPH0148902B2 (es) | ||
CN113382982A (zh) | 一种辛波莫德的制备方法 | |
JPH0237339B2 (es) | ||
JPH0415222B2 (es) | ||
JPH027583B2 (es) | ||
JPS58134059A (ja) | α−アミノメチルベンジルアルコ−ル誘導体の製造法 | |
JPS6045613B2 (ja) | シス−3−ヘキセン−1,6−ジオ−ルの製造法 | |
JPS6126894B2 (es) |