JPH0132167B2 - - Google Patents
Info
- Publication number
- JPH0132167B2 JPH0132167B2 JP11099985A JP11099985A JPH0132167B2 JP H0132167 B2 JPH0132167 B2 JP H0132167B2 JP 11099985 A JP11099985 A JP 11099985A JP 11099985 A JP11099985 A JP 11099985A JP H0132167 B2 JPH0132167 B2 JP H0132167B2
- Authority
- JP
- Japan
- Prior art keywords
- aqueous solution
- inorganic cation
- fine powder
- inorganic
- sicl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007864 aqueous solution Substances 0.000 claims description 33
- 239000000843 powder Substances 0.000 claims description 29
- -1 inorganic cation salts Chemical class 0.000 claims description 27
- 229910001411 inorganic cation Inorganic materials 0.000 claims description 25
- 238000006243 chemical reaction Methods 0.000 claims description 20
- 229910003902 SiCl 4 Inorganic materials 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 11
- RLOWWWKZYUNIDI-UHFFFAOYSA-N phosphinic chloride Chemical compound ClP=O RLOWWWKZYUNIDI-UHFFFAOYSA-N 0.000 claims description 7
- 150000001768 cations Chemical class 0.000 claims description 6
- 238000006460 hydrolysis reaction Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 150000001767 cationic compounds Chemical class 0.000 claims description 3
- 229910052761 rare earth metal Inorganic materials 0.000 claims description 2
- VLTRZXGMWDSKGL-UHFFFAOYSA-M perchlorate Inorganic materials [O-]Cl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-M 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 239000007789 gas Substances 0.000 description 10
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 9
- 229910004298 SiO 2 Inorganic materials 0.000 description 9
- 239000000443 aerosol Substances 0.000 description 9
- 239000006199 nebulizer Substances 0.000 description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 8
- 239000002994 raw material Substances 0.000 description 8
- 229910017493 Nd 2 O 3 Inorganic materials 0.000 description 6
- 239000000919 ceramic Substances 0.000 description 6
- 239000011521 glass Substances 0.000 description 5
- 150000002500 ions Chemical class 0.000 description 5
- 229910020366 ClO 4 Inorganic materials 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 4
- 229910010272 inorganic material Inorganic materials 0.000 description 4
- 239000011147 inorganic material Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000011882 ultra-fine particle Substances 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000002019 doping agent Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 150000004703 alkoxides Chemical class 0.000 description 1
- 239000006121 base glass Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000000087 laser glass Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 239000005304 optical glass Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 150000003839 salts Chemical group 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Landscapes
- Silicon Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11099985A JPS61270208A (ja) | 1985-05-23 | 1985-05-23 | 多成分系無機微粉末の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11099985A JPS61270208A (ja) | 1985-05-23 | 1985-05-23 | 多成分系無機微粉末の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61270208A JPS61270208A (ja) | 1986-11-29 |
| JPH0132167B2 true JPH0132167B2 (enExample) | 1989-06-29 |
Family
ID=14549833
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11099985A Granted JPS61270208A (ja) | 1985-05-23 | 1985-05-23 | 多成分系無機微粉末の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61270208A (enExample) |
-
1985
- 1985-05-23 JP JP11099985A patent/JPS61270208A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS61270208A (ja) | 1986-11-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Saravanapavan et al. | Mesoporous calcium silicate glasses. I. Synthesis | |
| Xu et al. | Modern inorganic synthetic chemistry | |
| JP3233298B2 (ja) | 高純度溶融シリカガラスの非多孔質物体を作成する方法 | |
| EP0225884B1 (en) | Multiconstituent optical fiber and method for producing same | |
| Polishchuk et al. | Oxyfluoride glasses (a review) | |
| JPS63162537A (ja) | 気相誘導ゲルから形成したガラス基体及びその生成プロセス | |
| Guizard et al. | Sol-gel transition in zirconia systems using physical and chemical processes | |
| JP4035440B2 (ja) | 大きい寸法を有する乾燥ゲルおよびこれによって導かれるガラスを製造するためのゾル−ゲル法 | |
| US4432781A (en) | Method for manufacturing fused quartz glass | |
| US6360564B1 (en) | Sol-gel method of preparing powder for use in forming glass | |
| Uhlmann et al. | The ceramist as chemist-opportunities for new materials | |
| Leng-Ward et al. | Oxynitride glasses and their glass-ceramic derivatives | |
| JPH0132167B2 (enExample) | ||
| JP2524174B2 (ja) | 光学機能性を有する石英ガラスの製造方法 | |
| EP0581358B1 (en) | Method for preparing boron-containing porous gels | |
| JP2001220158A (ja) | 焼結シリカガラス成形体 | |
| EP0034053A2 (en) | Method of producing phosphate glass and optical bodies formed therefrom | |
| JPH03150262A (ja) | コージェライトの製造方法 | |
| JPS6246936A (ja) | エ−ロゾル流の製造法 | |
| JPS6144823B2 (enExample) | ||
| JPH01192707A (ja) | 酸化物成形体の製造方法 | |
| JP2768624B2 (ja) | 耐熱性シリカ質発泡体及びその製造方法 | |
| JPS6253450B2 (enExample) | ||
| Frolova et al. | Investigation of zirconia-germania glasses and solids prepared by sol-gel technique | |
| JPS62288129A (ja) | 光フアイバ用ガラス母材の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |