JP7225217B2 - 金属ナノワイヤの連続フロー製造 - Google Patents

金属ナノワイヤの連続フロー製造 Download PDF

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JP7225217B2
JP7225217B2 JP2020513696A JP2020513696A JP7225217B2 JP 7225217 B2 JP7225217 B2 JP 7225217B2 JP 2020513696 A JP2020513696 A JP 2020513696A JP 2020513696 A JP2020513696 A JP 2020513696A JP 7225217 B2 JP7225217 B2 JP 7225217B2
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nanowires
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silver
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JP2021503039A (ja
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アルビンド クルカルニ、アモール
ビピン デシュパンデ、ジェイディープ
アショック ケイト、プラチ
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カウンシル オブ サイエンティフィック アンド インダストリアル リサーチ
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0547—Nanofibres or nanotubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2418—Feeding means
    • B01J2219/2419—Feeding means for the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2423—Separation means, e.g. membrane inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2201/00—Treatment under specific atmosphere
    • B22F2201/40—Metal compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2202/00—Treatment under specific physical conditions
    • B22F2202/17—Treatment under specific physical conditions use of centrifugal or vortex forces
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2203/00—Controlling
    • B22F2203/11—Controlling temperature, temperature profile
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2301/00—Metallic composition of the powder or its coating
    • B22F2301/25—Noble metals, i.e. Ag Au, Ir, Os, Pd, Pt, Rh, Ru
    • B22F2301/255—Silver or gold
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2304/00—Physical aspects of the powder
    • B22F2304/05—Submicron size particles
    • B22F2304/056—Particle size above 100 nm up to 300 nm
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
JP2020513696A 2017-09-06 2018-09-06 金属ナノワイヤの連続フロー製造 Active JP7225217B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IN201711031533 2017-09-06
IN201711031533A IN201711031533A (enExample) 2017-09-06 2018-09-06
PCT/IN2018/050576 WO2019049172A1 (en) 2017-09-06 2018-09-06 CONTINUOUS FLOW PRODUCTION OF METALLIC NANOWELS

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JP2021503039A JP2021503039A (ja) 2021-02-04
JP7225217B2 true JP7225217B2 (ja) 2023-02-20

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US (1) US20210060656A1 (enExample)
EP (1) EP3678804B1 (enExample)
JP (1) JP7225217B2 (enExample)
KR (1) KR102497069B1 (enExample)
CN (1) CN111225755A (enExample)
ES (1) ES2927254T3 (enExample)
IN (1) IN201711031533A (enExample)
WO (1) WO2019049172A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7438348B2 (ja) * 2019-11-15 2024-02-26 カウンシル オブ サイエンティフィック アンド インダストリアル リサーチ 気泡塔型反応器を使用した、金属ナノワイヤの合成のための連続流動法
CN112024905A (zh) * 2020-07-08 2020-12-04 南京大学 一种基于连续流技术规模化合成纳米银线的方法
KR102537063B1 (ko) * 2021-11-02 2023-05-26 경희대학교 산학협력단 금속계 나노소재의 제조방법, 이로부터 제조된 금속계 나노소재, 촉매 및 검출장치
CN114833334B (zh) * 2022-04-02 2023-08-15 有研工程技术研究院有限公司 可连续制备微米级球形金粉的方法
DE102023101927A1 (de) 2023-01-26 2024-08-01 Karlsruher Institut für Technologie, Körperschaft des öffentlichen Rechts Verfahren zur kontinuierlichen Cluster- und Nanopartikelsynthese
CN116698671B (zh) * 2023-06-05 2023-11-21 南京工业大学 一种磁纳米毛刷及其制备方法
CN118905237B (zh) * 2024-07-24 2025-09-23 泉州师范学院 一种超长银纳米线的制备方法

Citations (5)

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JP2013007070A (ja) 2011-06-22 2013-01-10 Nippon Steel & Sumikin Chemical Co Ltd ニッケルナノ粒子の連続製造装置及び連続製造方法
JP2013007082A (ja) 2011-06-23 2013-01-10 Nippon Steel & Sumikin Chemical Co Ltd 金属ナノ粒子の連続製造装置及び連続製造方法
JP2014511435A (ja) 2011-02-15 2014-05-15 ケアストリーム ヘルス インク ナノワイヤ調製方法、組成物、および物品
JP2015526836A (ja) 2012-06-05 2015-09-10 コミサリア ア レネルジィ アトミーク エ オ ゼネ ルジイ アルテアナティーフCommissariata L’Energie Atomique Et Aux Energies Alternatives 銀ナノワイヤをベースとする透明導体材料の電気的および光学的性能を改善する方法
JP2015180772A (ja) 2014-03-07 2015-10-15 Dowaホールディングス株式会社 銀ナノワイヤの製造方法並びに銀ナノワイヤおよびそれを用いたインク

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US7824466B2 (en) 2005-01-14 2010-11-02 Cabot Corporation Production of metal nanoparticles
US8048192B2 (en) * 2005-12-30 2011-11-01 General Electric Company Method of manufacturing nanoparticles
KR100877522B1 (ko) * 2007-05-15 2009-01-09 삼성전기주식회사 금속 나노입자의 제조장치 및 제조방법
TWI379908B (en) * 2008-12-02 2012-12-21 Chung Shan Inst Of Science Method for continuously fabricating silver nanowire
DE102009015470A1 (de) * 2008-12-12 2010-06-17 Byk-Chemie Gmbh Verfahren zur Herstellung von Metallnanopartikeln und auf diese Weise erhaltene Metallnanopartikel und ihre Verwendung
US20100242679A1 (en) 2009-03-29 2010-09-30 Yi-Hsiuan Yu Method for continuously fabricating silver nanowire
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KR20130014279A (ko) * 2011-07-29 2013-02-07 엘지이노텍 주식회사 나노 와이어 및 이의 제조방법
TWI585032B (zh) * 2012-06-28 2017-06-01 無限科技全球公司 用於製造奈米結構的方法
CN104511596B (zh) * 2013-09-30 2017-01-18 中科院广州化学有限公司 一种纳米银线的连续制备方法及其装置
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JP2014511435A (ja) 2011-02-15 2014-05-15 ケアストリーム ヘルス インク ナノワイヤ調製方法、組成物、および物品
JP2013007070A (ja) 2011-06-22 2013-01-10 Nippon Steel & Sumikin Chemical Co Ltd ニッケルナノ粒子の連続製造装置及び連続製造方法
JP2013007082A (ja) 2011-06-23 2013-01-10 Nippon Steel & Sumikin Chemical Co Ltd 金属ナノ粒子の連続製造装置及び連続製造方法
JP2015526836A (ja) 2012-06-05 2015-09-10 コミサリア ア レネルジィ アトミーク エ オ ゼネ ルジイ アルテアナティーフCommissariata L’Energie Atomique Et Aux Energies Alternatives 銀ナノワイヤをベースとする透明導体材料の電気的および光学的性能を改善する方法
JP2015180772A (ja) 2014-03-07 2015-10-15 Dowaホールディングス株式会社 銀ナノワイヤの製造方法並びに銀ナノワイヤおよびそれを用いたインク

Also Published As

Publication number Publication date
KR102497069B1 (ko) 2023-02-06
WO2019049172A1 (en) 2019-03-14
ES2927254T3 (es) 2022-11-03
KR20200051682A (ko) 2020-05-13
US20210060656A1 (en) 2021-03-04
WO2019049172A4 (en) 2019-05-09
IN201711031533A (enExample) 2024-02-23
JP2021503039A (ja) 2021-02-04
CN111225755A (zh) 2020-06-02
EP3678804B1 (en) 2022-06-15
EP3678804A1 (en) 2020-07-15

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