JP7112431B2 - 塩基性ｐＨ調節剤を含む均質化された植物性材料 - Google Patents
塩基性ｐＨ調節剤を含む均質化された植物性材料 Download PDFInfo
- Publication number
- JP7112431B2 JP7112431B2 JP2019563096A JP2019563096A JP7112431B2 JP 7112431 B2 JP7112431 B2 JP 7112431B2 JP 2019563096 A JP2019563096 A JP 2019563096A JP 2019563096 A JP2019563096 A JP 2019563096A JP 7112431 B2 JP7112431 B2 JP 7112431B2
- Authority
- JP
- Japan
- Prior art keywords
- plant material
- aerosol
- homogenized
- homogenized plant
- generating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000463 material Substances 0.000 title claims description 272
- 239000003002 pH adjusting agent Substances 0.000 title claims description 35
- 241000196324 Embryophyta Species 0.000 claims description 178
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 113
- 239000000443 aerosol Substances 0.000 claims description 60
- 239000002002 slurry Substances 0.000 claims description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 39
- 238000000034 method Methods 0.000 claims description 25
- 150000002632 lipids Chemical class 0.000 claims description 20
- 238000005266 casting Methods 0.000 claims description 17
- 238000001035 drying Methods 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 13
- -1 alkaline earth metal bicarbonates Chemical class 0.000 claims description 10
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 7
- 230000008018 melting Effects 0.000 claims description 7
- 150000003839 salts Chemical class 0.000 claims description 4
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims description 3
- 238000005520 cutting process Methods 0.000 claims description 3
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 3
- 239000000347 magnesium hydroxide Substances 0.000 claims description 3
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 3
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- 229910000316 alkaline earth metal phosphate Inorganic materials 0.000 claims description 2
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 2
- 239000001506 calcium phosphate Substances 0.000 claims description 2
- 229910000389 calcium phosphate Inorganic materials 0.000 claims description 2
- 235000011010 calcium phosphates Nutrition 0.000 claims description 2
- QWDJLDTYWNBUKE-UHFFFAOYSA-L magnesium bicarbonate Chemical compound [Mg+2].OC([O-])=O.OC([O-])=O QWDJLDTYWNBUKE-UHFFFAOYSA-L 0.000 claims description 2
- 239000002370 magnesium bicarbonate Substances 0.000 claims description 2
- 229910000022 magnesium bicarbonate Inorganic materials 0.000 claims description 2
- 235000014824 magnesium bicarbonate Nutrition 0.000 claims description 2
- 235000012254 magnesium hydroxide Nutrition 0.000 claims description 2
- GVALZJMUIHGIMD-UHFFFAOYSA-H magnesium phosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GVALZJMUIHGIMD-UHFFFAOYSA-H 0.000 claims description 2
- 239000004137 magnesium phosphate Substances 0.000 claims description 2
- 229910000157 magnesium phosphate Inorganic materials 0.000 claims description 2
- 229960002261 magnesium phosphate Drugs 0.000 claims description 2
- 235000010994 magnesium phosphates Nutrition 0.000 claims description 2
- 235000021317 phosphate Nutrition 0.000 claims description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims description 2
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 2
- 241000208125 Nicotiana Species 0.000 claims 2
- 230000001568 sexual effect Effects 0.000 claims 1
- 244000061176 Nicotiana tabacum Species 0.000 description 111
- 239000000758 substrate Substances 0.000 description 49
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 35
- 229960002715 nicotine Drugs 0.000 description 35
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 35
- 238000010438 heat treatment Methods 0.000 description 27
- 239000005418 vegetable material Substances 0.000 description 27
- 239000011230 binding agent Substances 0.000 description 18
- 230000008569 process Effects 0.000 description 14
- 229920003043 Cellulose fiber Polymers 0.000 description 12
- 239000000835 fiber Substances 0.000 description 12
- 239000000796 flavoring agent Substances 0.000 description 11
- 239000003795 chemical substances by application Substances 0.000 description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 9
- 229930013930 alkaloid Natural products 0.000 description 8
- 230000000723 chemosensory effect Effects 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 6
- 235000019634 flavors Nutrition 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 5
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 5
- 235000013355 food flavoring agent Nutrition 0.000 description 5
- 150000003797 alkaloid derivatives Chemical class 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 238000001816 cooling Methods 0.000 description 4
- 229940041616 menthol Drugs 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 229920002907 Guar gum Polymers 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 235000019504 cigarettes Nutrition 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 238000002788 crimping Methods 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 235000011187 glycerol Nutrition 0.000 description 3
- 239000000665 guar gum Substances 0.000 description 3
- 235000010417 guar gum Nutrition 0.000 description 3
- 229960002154 guar gum Drugs 0.000 description 3
- 210000000214 mouth Anatomy 0.000 description 3
- 229920001277 pectin Polymers 0.000 description 3
- 238000004537 pulping Methods 0.000 description 3
- 235000003441 saturated fatty acids Nutrition 0.000 description 3
- 150000004671 saturated fatty acids Chemical class 0.000 description 3
- 239000001993 wax Substances 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- KMZHZAAOEWVPSE-UHFFFAOYSA-N 2,3-dihydroxypropyl acetate Chemical compound CC(=O)OCC(O)CO KMZHZAAOEWVPSE-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- VZWGRQBCURJOMT-UHFFFAOYSA-N Dodecyl acetate Chemical compound CCCCCCCCCCCCOC(C)=O VZWGRQBCURJOMT-UHFFFAOYSA-N 0.000 description 2
- MWAYRGBWOVHDDZ-UHFFFAOYSA-N Ethyl vanillate Chemical compound CCOC(=O)C1=CC=C(O)C(OC)=C1 MWAYRGBWOVHDDZ-UHFFFAOYSA-N 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N Formic acid Chemical compound OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 229920000161 Locust bean gum Polymers 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- UYXTWWCETRIEDR-UHFFFAOYSA-N Tributyrin Chemical compound CCCC(=O)OCC(OC(=O)CCC)COC(=O)CCC UYXTWWCETRIEDR-UHFFFAOYSA-N 0.000 description 2
- 229920002522 Wood fibre Polymers 0.000 description 2
- 239000011149 active material Substances 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 239000007961 artificial flavoring substance Substances 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 2
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- ZDJFDFNNEAPGOP-UHFFFAOYSA-N dimethyl tetradecanedioate Chemical compound COC(=O)CCCCCCCCCCCCC(=O)OC ZDJFDFNNEAPGOP-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- MMXKVMNBHPAILY-UHFFFAOYSA-N ethyl laurate Chemical compound CCCCCCCCCCCC(=O)OCC MMXKVMNBHPAILY-UHFFFAOYSA-N 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 238000000265 homogenisation Methods 0.000 description 2
- 235000010420 locust bean gum Nutrition 0.000 description 2
- 239000000711 locust bean gum Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 229920001206 natural gum Polymers 0.000 description 2
- 235000010987 pectin Nutrition 0.000 description 2
- 239000001814 pectin Substances 0.000 description 2
- 210000003370 receptor cell Anatomy 0.000 description 2
- 230000035807 sensation Effects 0.000 description 2
- 235000019615 sensations Nutrition 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000005846 sugar alcohols Polymers 0.000 description 2
- YAPQBXQYLJRXSA-UHFFFAOYSA-N theobromine Chemical compound CN1C(=O)NC(=O)C2=C1N=CN2C YAPQBXQYLJRXSA-UHFFFAOYSA-N 0.000 description 2
- 235000019505 tobacco product Nutrition 0.000 description 2
- URAYPUMNDPQOKB-UHFFFAOYSA-N triacetin Chemical compound CC(=O)OCC(OC(C)=O)COC(C)=O URAYPUMNDPQOKB-UHFFFAOYSA-N 0.000 description 2
- PYMYPHUHKUWMLA-UHFFFAOYSA-N 2,3,4,5-tetrahydroxypentanal Chemical compound OCC(O)C(O)C(O)C=O PYMYPHUHKUWMLA-UHFFFAOYSA-N 0.000 description 1
- 244000215068 Acacia senegal Species 0.000 description 1
- 244000247812 Amorphophallus rivieri Species 0.000 description 1
- 235000001206 Amorphophallus rivieri Nutrition 0.000 description 1
- 229930003347 Atropine Natural products 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000167854 Bourreria succulenta Species 0.000 description 1
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 240000008886 Ceratonia siliqua Species 0.000 description 1
- 235000013912 Ceratonia siliqua Nutrition 0.000 description 1
- 244000223760 Cinnamomum zeylanicum Species 0.000 description 1
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 240000000491 Corchorus aestuans Species 0.000 description 1
- 235000011777 Corchorus aestuans Nutrition 0.000 description 1
- 235000010862 Corchorus capsularis Nutrition 0.000 description 1
- 229920002307 Dextran Polymers 0.000 description 1
- 239000004386 Erythritol Substances 0.000 description 1
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 description 1
- 229920000896 Ethulose Polymers 0.000 description 1
- 239000001856 Ethyl cellulose Substances 0.000 description 1
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 1
- 239000001859 Ethyl hydroxyethyl cellulose Substances 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 240000001238 Gaultheria procumbens Species 0.000 description 1
- 235000007297 Gaultheria procumbens Nutrition 0.000 description 1
- UXDDRFCJKNROTO-UHFFFAOYSA-N Glycerol 1,2-diacetate Chemical compound CC(=O)OCC(CO)OC(C)=O UXDDRFCJKNROTO-UHFFFAOYSA-N 0.000 description 1
- 229920000084 Gum arabic Polymers 0.000 description 1
- 244000020551 Helianthus annuus Species 0.000 description 1
- 235000003222 Helianthus annuus Nutrition 0.000 description 1
- RKUNBYITZUJHSG-UHFFFAOYSA-N Hyosciamin-hydrochlorid Natural products CN1C(C2)CCC1CC2OC(=O)C(CO)C1=CC=CC=C1 RKUNBYITZUJHSG-UHFFFAOYSA-N 0.000 description 1
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 description 1
- 229920002752 Konjac Polymers 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 235000005135 Micromeria juliana Nutrition 0.000 description 1
- 108050002069 Olfactory receptors Proteins 0.000 description 1
- 102000012547 Olfactory receptors Human genes 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- MIYFJEKZLFWKLZ-UHFFFAOYSA-N Phenylmethyl benzeneacetate Chemical compound C=1C=CC=CC=1COC(=O)CC1=CC=CC=C1 MIYFJEKZLFWKLZ-UHFFFAOYSA-N 0.000 description 1
- 239000004373 Pullulan Substances 0.000 description 1
- 229920001218 Pullulan Polymers 0.000 description 1
- 240000002114 Satureja hortensis Species 0.000 description 1
- 235000007315 Satureja hortensis Nutrition 0.000 description 1
- 229920001800 Shellac Polymers 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 240000004584 Tamarindus indica Species 0.000 description 1
- 235000004298 Tamarindus indica Nutrition 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N Tetraethylene glycol, Natural products OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 description 1
- 235000009499 Vanilla fragrans Nutrition 0.000 description 1
- 244000263375 Vanilla tahitensis Species 0.000 description 1
- 235000012036 Vanilla tahitensis Nutrition 0.000 description 1
- 235000010489 acacia gum Nutrition 0.000 description 1
- 239000000205 acacia gum Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000012387 aerosolization Methods 0.000 description 1
- 230000004931 aggregating effect Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- RKUNBYITZUJHSG-SPUOUPEWSA-N atropine Chemical compound O([C@H]1C[C@H]2CC[C@@H](C1)N2C)C(=O)C(CO)C1=CC=CC=C1 RKUNBYITZUJHSG-SPUOUPEWSA-N 0.000 description 1
- 229960000396 atropine Drugs 0.000 description 1
- 229960002903 benzyl benzoate Drugs 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229960001948 caffeine Drugs 0.000 description 1
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 235000010216 calcium carbonate Nutrition 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 239000004204 candelilla wax Substances 0.000 description 1
- 235000013868 candelilla wax Nutrition 0.000 description 1
- 229940073532 candelilla wax Drugs 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 239000004203 carnauba wax Substances 0.000 description 1
- 235000013869 carnauba wax Nutrition 0.000 description 1
- 229940082483 carnauba wax Drugs 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 235000010980 cellulose Nutrition 0.000 description 1
- 235000019693 cherries Nutrition 0.000 description 1
- 235000017803 cinnamon Nutrition 0.000 description 1
- 239000009194 citrus pectin Substances 0.000 description 1
- 229940040387 citrus pectin Drugs 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 235000019700 dicalcium phosphate Nutrition 0.000 description 1
- PEUGOJXLBSIJQS-UHFFFAOYSA-N diethyl octanedioate Chemical compound CCOC(=O)CCCCCCC(=O)OCC PEUGOJXLBSIJQS-UHFFFAOYSA-N 0.000 description 1
- IZMOTZDBVPMOFE-UHFFFAOYSA-N dimethyl dodecanedioate Chemical compound COC(=O)CCCCCCCCCCC(=O)OC IZMOTZDBVPMOFE-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 description 1
- 229940009714 erythritol Drugs 0.000 description 1
- 235000019414 erythritol Nutrition 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 235000019325 ethyl cellulose Nutrition 0.000 description 1
- 229920001249 ethyl cellulose Polymers 0.000 description 1
- 235000019326 ethyl hydroxyethyl cellulose Nutrition 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 210000001932 glossopharyngeal nerve Anatomy 0.000 description 1
- 235000013773 glyceryl triacetate Nutrition 0.000 description 1
- 108091005708 gustatory receptors Proteins 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 239000008172 hydrogenated vegetable oil Substances 0.000 description 1
- 229920013818 hydroxypropyl guar gum Polymers 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000000252 konjac Substances 0.000 description 1
- 235000010485 konjac Nutrition 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 235000014380 magnesium carbonate Nutrition 0.000 description 1
- 229920000609 methyl cellulose Polymers 0.000 description 1
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 1
- 239000001923 methylcellulose Substances 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 210000003928 nasal cavity Anatomy 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 description 1
- 235000019423 pullulan Nutrition 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 235000013874 shellac Nutrition 0.000 description 1
- 239000004208 shellac Substances 0.000 description 1
- ZLGIYFNHBLSMPS-ATJNOEHPSA-N shellac Chemical compound OCCCCCC(O)C(O)CCCCCCCC(O)=O.C1C23[C@H](C(O)=O)CCC2[C@](C)(CO)[C@@H]1C(C(O)=O)=C[C@@H]3O ZLGIYFNHBLSMPS-ATJNOEHPSA-N 0.000 description 1
- 229940113147 shellac Drugs 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- 239000011122 softwood Substances 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 229960004559 theobromine Drugs 0.000 description 1
- 238000011282 treatment Methods 0.000 description 1
- 229960002622 triacetin Drugs 0.000 description 1
- 150000003626 triacylglycerols Chemical class 0.000 description 1
- 239000001069 triethyl citrate Substances 0.000 description 1
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
- 235000013769 triethyl citrate Nutrition 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- 210000003901 trigeminal nerve Anatomy 0.000 description 1
- JFJZZMVDLULRGK-URLMMPGGSA-O tubocurarine Chemical compound C([C@H]1[N+](C)(C)CCC=2C=C(C(=C(OC3=CC=C(C=C3)C[C@H]3C=4C=C(C(=CC=4CCN3C)OC)O3)C=21)O)OC)C1=CC=C(O)C3=C1 JFJZZMVDLULRGK-URLMMPGGSA-O 0.000 description 1
- 229960001844 tubocurarine Drugs 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 210000001186 vagus nerve Anatomy 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
- 229920001285 xanthan gum Polymers 0.000 description 1
- 239000000230 xanthan gum Substances 0.000 description 1
- 235000010493 xanthan gum Nutrition 0.000 description 1
- 229940082509 xanthan gum Drugs 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
- A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/165—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes comprising as heat source a carbon fuel or an oxidized or thermally degraded carbonaceous fuel, e.g. carbohydrates, cellulosic material
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/42—Treatment of tobacco products or tobacco substitutes by chemical substances by organic and inorganic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
- A24C5/01—Making cigarettes for simulated smoking devices
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/20—Cigarettes specially adapted for simulated smoking devices
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/22—Cigarettes with integrated combustible heat sources, e.g. with carbonaceous heat sources
Landscapes
- General Chemical & Material Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Toxicology (AREA)
- Molecular Biology (AREA)
- Manufacture Of Tobacco Products (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Paper (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP17172907 | 2017-05-24 | ||
| EP17172907.2 | 2017-05-24 | ||
| PCT/EP2018/063403 WO2018215479A1 (en) | 2017-05-24 | 2018-05-22 | Homogenised botanical material comprising a basic ph modifier |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2020520638A JP2020520638A (ja) | 2020-07-16 |
| JP7112431B2 true JP7112431B2 (ja) | 2022-08-03 |
Family
ID=58772803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2019563096A Active JP7112431B2 (ja) | 2017-05-24 | 2018-05-22 | 塩基性ｐＨ調節剤を含む均質化された植物性材料 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US20210153541A1 (ru) |
| EP (1) | EP3629776B1 (ru) |
| JP (1) | JP7112431B2 (ru) |
| KR (1) | KR102638408B1 (ru) |
| CN (1) | CN110573031B (ru) |
| BR (1) | BR112019022284A2 (ru) |
| MX (1) | MX2019013605A (ru) |
| RU (1) | RU2770198C2 (ru) |
| UA (1) | UA125525C2 (ru) |
| WO (1) | WO2018215479A1 (ru) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP4316271A3 (en) * | 2018-09-17 | 2024-03-27 | COMAS - COSTRUZIONI MACCHINE SPECIALI - S.p.A. | Method for the production of reconstituted tobacco |
| KR20220017901A (ko) * | 2019-06-10 | 2022-02-14 | 필립모리스 프로덕츠 에스.에이. | 에어로졸 발생 물품용 안정적 래퍼 |
| GB201917475D0 (en) * | 2019-11-29 | 2020-01-15 | Nicoventures Trading Ltd | Aerosol generation |
| KR20220116453A (ko) * | 2019-12-18 | 2022-08-23 | 필립모리스 프로덕츠 에스.에이. | 알칼로이드 함유 재료 시트를 제조하기 위한 방법 |
| US20210195938A1 (en) * | 2019-12-27 | 2021-07-01 | Nicoventures Trading Limited | Substrate with multiple aerosol forming materials for aerosol delivery device |
| KR102622043B1 (ko) * | 2021-04-09 | 2024-01-08 | 주식회사 케이티앤지 | 과립형 담배 매질 및 이를 포함하는 에어로졸 생성 물품 |
| JPWO2022230886A1 (ru) * | 2021-04-26 | 2022-11-03 | ||
| KR102676406B1 (ko) * | 2021-05-20 | 2024-06-19 | 주식회사 케이티앤지 | 담배 매질 및 그를 포함하는 에어로졸 생성 물품 |
| KR20230167895A (ko) * | 2022-06-03 | 2023-12-12 | 주식회사 케이티앤지 | 니코틴 전이가 방지된 흡연물품 및 이를 포함하는 에어로졸 생성 시스템 |
| WO2024149850A1 (en) * | 2023-01-11 | 2024-07-18 | Swm Holdco Luxembourg | Reconstituted plant sheet comprising stabilized nicotine |
| FR3144743A1 (fr) * | 2023-01-11 | 2024-07-12 | Swm Luxembourg | Feuille de plante reconstituée comprenant de la nicotine stabilisée |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016156598A1 (en) | 2015-04-01 | 2016-10-06 | Philip Morris Products S.A. | Homogenized tobacco material and method of production of homogenized tobacco material |
| WO2016184977A1 (en) | 2015-05-20 | 2016-11-24 | British American Tobacco (Investments) Limited | Aerosol generating material and devices including the same |
| WO2017077112A1 (en) | 2015-11-05 | 2017-05-11 | Philip Morris Products S.A. | Homogenized tobacco material with meltable lipid |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB983928A (en) | 1962-05-03 | 1965-02-24 | British American Tobacco Co | Improvements relating to the production of tobacco smoking materials |
| US4033359A (en) * | 1970-03-23 | 1977-07-05 | Imperial Chemical Industries Limited | Smoking mixture |
| GB1299641A (en) * | 1970-03-23 | 1972-12-13 | Ici Ltd | Improved smoking mixture |
| US3894544A (en) | 1972-06-02 | 1975-07-15 | Tamag Basel Ag | Process for producing tobacco structures |
| US3860012A (en) | 1973-05-21 | 1975-01-14 | Kimberly Clark Co | Method of producing a reconstituted tobacco product |
| US4109663A (en) * | 1974-10-17 | 1978-08-29 | Takeda Chemical Industries, Ltd. | Tobacco product containing a thermo-gelable β-1,3-glucan-type polysaccharide |
| SE8405479D0 (sv) * | 1984-11-01 | 1984-11-01 | Nilsson Sven Erik | Sett att administrera flyktiga, fysiologiskt, aktiva emnen och anordning for detta |
| EP0419975A3 (en) * | 1989-09-29 | 1991-08-07 | R.J. Reynolds Tobacco Company | Cigarette and smokable filler material therefor |
| US5101839A (en) * | 1990-08-15 | 1992-04-07 | R. J. Reynolds Tobacco Company | Cigarette and smokable filler material therefor |
| ES2095228T3 (es) * | 1989-09-29 | 1997-02-16 | Reynolds Tobacco Co R | Cigarrillo y su material de relleno fumable. |
| US5415186A (en) * | 1990-08-15 | 1995-05-16 | R. J. Reynolds Tobacco Company | Substrates material for smoking articles |
| US5396911A (en) * | 1990-08-15 | 1995-03-14 | R. J. Reynolds Tobacco Company | Substrate material for smoking articles |
| JP3681410B2 (ja) | 1992-04-09 | 2005-08-10 | フィリップ・モーリス・プロダクツ・インコーポレイテッド | 再構成タバコシート及びその製造法及び使用法 |
| AR002035A1 (es) | 1995-04-20 | 1998-01-07 | Philip Morris Prod | Un cigarrillo, un cigarrillo y encendedor adaptados para cooperar entre si, un metodo para mejorar la entrega de aerosol de un cigarrillo, un material continuo de tabaco, un cigarrillo operativo, un metodo para manufacturar un material continuo, el material asi obtenido, un calentador, un metodo para formar un calentador y un sistema electrico para fumar |
| GB9712815D0 (en) * | 1997-06-19 | 1997-08-20 | British American Tobacco Co | Smoking article and smoking material therefor |
| CH691156A5 (fr) | 1998-05-19 | 2001-05-15 | Philip Morris Prod | Ligne d'alimentation d'une machine de production de filtres de cigarettes. |
| GB0324525D0 (en) * | 2003-10-21 | 2003-11-26 | British American Tobacco Co | Smoking articles and smokable filler material therefor |
| US7428905B2 (en) * | 2004-07-30 | 2008-09-30 | R.J. Reynolds Tobacco Company | Method of making smokeable tobacco substitute filler having an increased fill value |
| US8887737B2 (en) * | 2005-07-29 | 2014-11-18 | Philip Morris Usa Inc. | Extraction and storage of tobacco constituents |
| KR101606312B1 (ko) | 2007-08-10 | 2016-03-24 | 필립모리스 프로덕츠 에스.에이. | 증류식 흡연 물품 |
| JP5732043B2 (ja) * | 2009-04-24 | 2015-06-10 | オムヤ インターナショナル アーゲー | 活性成分を放出制御するための粒状物質 |
| US9848634B2 (en) * | 2009-06-30 | 2017-12-26 | Philip Morris Products S.A. | Smokeless tobacco product |
| EP2526787A1 (en) * | 2011-05-26 | 2012-11-28 | Philip Morris Products S.A. | Methods for reducing the formation of tobacco specific nitrosamines in tobacco homogenates |
| CA2837953C (en) | 2011-05-31 | 2020-06-16 | Philip Morris Products S.A. | Rods for use in smoking articles |
| US9420825B2 (en) * | 2012-02-13 | 2016-08-23 | R.J. Reynolds Tobacco Company | Whitened tobacco composition |
| US20140166028A1 (en) * | 2012-12-14 | 2014-06-19 | Richard C. Fuisz | Enhanced Delivery of Nicotine, THC, Tobacco, Cannabidiol or Base Alkaloid from an Electronic Cigarette or Other Vapor or Smoke Producing Device Through Use of an Absorption Conditioning Unit |
| GB201314917D0 (en) * | 2013-08-21 | 2013-10-02 | British American Tobacco Co | Treated Tobacco and processes for preparing the same, Devices including the same and uses thereof |
| CN104013603A (zh) * | 2014-05-13 | 2014-09-03 | 上海烟草集团有限责任公司 | 一种烟碱缓释贴剂 |
| PT3160275T (pt) * | 2014-06-27 | 2018-11-30 | Philip Morris Products Sa | Artigo para fumar compreendendo uma fonte de calor combustível e suporte método para o seu fabrico |
| US20170055576A1 (en) * | 2015-08-31 | 2017-03-02 | R. J. Reynolds Tobacco Company | Smoking article |
-
2018
- 2018-05-22 RU RU2019136369A patent/RU2770198C2/ru active
- 2018-05-22 US US16/611,869 patent/US20210153541A1/en active Pending
- 2018-05-22 JP JP2019563096A patent/JP7112431B2/ja active Active
- 2018-05-22 BR BR112019022284A patent/BR112019022284A2/pt active Search and Examination
- 2018-05-22 WO PCT/EP2018/063403 patent/WO2018215479A1/en active Application Filing
- 2018-05-22 EP EP18724585.7A patent/EP3629776B1/en active Active
- 2018-05-22 MX MX2019013605A patent/MX2019013605A/es unknown
- 2018-05-22 UA UAA201907889A patent/UA125525C2/uk unknown
- 2018-05-22 CN CN201880028343.5A patent/CN110573031B/zh active Active
- 2018-05-22 KR KR1020197035766A patent/KR102638408B1/ko active IP Right Grant
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2016156598A1 (en) | 2015-04-01 | 2016-10-06 | Philip Morris Products S.A. | Homogenized tobacco material and method of production of homogenized tobacco material |
| WO2016184977A1 (en) | 2015-05-20 | 2016-11-24 | British American Tobacco (Investments) Limited | Aerosol generating material and devices including the same |
| WO2017077112A1 (en) | 2015-11-05 | 2017-05-11 | Philip Morris Products S.A. | Homogenized tobacco material with meltable lipid |
Also Published As
| Publication number | Publication date |
|---|---|
| KR102638408B1 (ko) | 2024-02-21 |
| UA125525C2 (uk) | 2022-04-13 |
| WO2018215479A1 (en) | 2018-11-29 |
| BR112019022284A2 (pt) | 2020-05-19 |
| RU2019136369A (ru) | 2021-06-24 |
| CN110573031B (zh) | 2022-04-05 |
| EP3629776A1 (en) | 2020-04-08 |
| RU2019136369A3 (ru) | 2021-09-14 |
| CN110573031A (zh) | 2019-12-13 |
| US20210153541A1 (en) | 2021-05-27 |
| EP3629776B1 (en) | 2021-02-17 |
| KR20200010295A (ko) | 2020-01-30 |
| JP2020520638A (ja) | 2020-07-16 |
| RU2770198C2 (ru) | 2022-04-14 |
| MX2019013605A (es) | 2019-12-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP7245172B2 (ja) | 均質化された植物性材料を含む加熱式エアロゾル発生物品 | |
| JP7112431B2 (ja) | 塩基性ｐＨ調節剤を含む均質化された植物性材料 | |
| KR102568612B1 (ko) | 니코틴 함유 시트의 제조 방법 | |
| JP7518145B2 (ja) | ニコチン含有シート | |
| JP7453967B2 (ja) | クローブ含有エアロゾル発生基体 | |
| KR102037697B1 (ko) | 용융 가능한 지질이 있는 균질화 담배 물질 | |
| JP7518144B2 (ja) | ニコチンおよびセルロース含有シート | |
| KR102705128B1 (ko) | 오일 첨가제를 포함하는 에어로졸 발생 기재 | |
| JP2021505126A (ja) | 二重プラグを備えるエアロゾル発生基体を有するエアロゾル発生物品 | |
| KR20180073579A (ko) | 휘발성 물질의 전달이 개선된 균질화 담배 재료 | |
| JP2022516013A (ja) | 形成された流体通路を有するたばこ材料を含むロッドを有するエアロゾル発生物品 | |
| JP2024504401A (ja) | タバコ媒質、及びそれを含むエアロゾル生成物品 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20210512 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20220620 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20220623 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20220722 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 7112431 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |