JP6886529B2 - 封止材フィルム用のリン酸トリアリルを含む非極性エチレン系組成物 - Google Patents
封止材フィルム用のリン酸トリアリルを含む非極性エチレン系組成物 Download PDFInfo
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- JP6886529B2 JP6886529B2 JP2019565946A JP2019565946A JP6886529B2 JP 6886529 B2 JP6886529 B2 JP 6886529B2 JP 2019565946 A JP2019565946 A JP 2019565946A JP 2019565946 A JP2019565946 A JP 2019565946A JP 6886529 B2 JP6886529 B2 JP 6886529B2
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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Description
元素周期表へのいずれの参照も、CRC Press,Inc.,1990−1991によって公開されたものへの参照とする。この元素周期表における元素族への参照は、族の番号付与の新しい表記法による。
(A)0.850g/cc〜0.890g/ccの密度を有する非極性エチレン系ポリマーと、(B)有機過酸化物と、(C)シランカップリング剤と、(D)リン酸トリアリルを含む助剤とを含む組成物を使用して、封止材フィルムを形成する。
本組成物は、非極性エチレン系ポリマーを含む。
(i)0.850g/cc、または0.855g/cc、または0.860g/cc、または0.865g/cc、または0.870g/ccから、0.875g/cc、または0.880g/cc、または0.885g/cc、または0.890g/cc、または0.900g/ccの密度、
(ii)2g/10分、または5g/10分、または10g/10分、または12g/10分から、30g/10分、または35g/10分、または40g/10分、または45g/10分、または50g/10分のメルトインデックス、および/または
(iii)40℃、または45℃、または50℃、または55℃から、60℃、または65℃、または70℃、または80℃、または90℃、または95℃、または100℃、または110℃、または120℃、または125℃の融点(Tm)。
本組成物は、有機過酸化物を含む。好適な有機過酸化物の非限定的な例としては、過酸化ジクミル、過酸化ラウリル、過酸化ベンゾイル、過安息香酸第三ブチル、過酸化ジ(第三ブチル)、クメンヒドロペルオキシド、2,5−ジメチル−2,5−ジ(t−ブチル−ペルオキシ)ヘキシン−3、2,−5−ジ−メチル−2,5−ジ(t−ブチル−ペルオキシ)ヘキサン、第三ブチルヒドロペルオキシド、過炭酸イソプロピル、アルファ,アルファ’−ビス(第三ブチルペルオキシ)ジイソプロピルベンゼン、ペルオキシ−2−エチルヘキシル−モノカルボン酸t−ブチル、1,1−ビス(t−ブチルペルオキシ)−3,5,5−トリメチルシクロヘキサン、2,5−ジメチル−2,5−ジヒドロキシ過酸化物、過酸化t−ブチルクミル、アルファ,アルファ’−ビス(t−ブチルペルオキシ)−p−ジイソプロピルベンゼン等が挙げられる。
本組成物は、シランカップリング剤を含む。一実施形態では、シランカップリング剤は、少なくとも1つのアルコキシ基を含む。好適なシランカップリング剤の非限定的な例としては、γ−クロロプロピルトリメトキシシラン、ビニルトリメトキシシラン、ビニルトリエトキシシラン、ビニル−トリス−(β−メトキシ)シラン、γ−メタクリルオキシプロピルトリメトキシシラン、β−(3,4−エトキシ−シクロヘキシル)エチルトリメトキシシラン、γ−グリシドオキシプロピルトリメトキシシラン、γ−メルカプトプロピルトリメトキシシラン、γ−アミノプロピルトリメトキシシラン、N−β−(アミノエチル)−γ−アミノプロピルトリメトキシシラン、および3−(トリメトキシシリル)プロピルメタクリレートが挙げられる。
一実施形態では、本組成物は、1つ以上の任意の添加剤を含む。好適な添加剤の非限定的な例としては、酸化防止剤、ブロッキング防止剤、安定剤、着色剤、紫外線(UV)吸収剤または安定剤、難燃剤、相溶化剤、充填剤、および加工助剤が挙げられる。
本組成物は、封止材フィルムに形成される。上記のいずれかの実施形態または2つ以上の実施形態の組み合わせに記載の組成物等の組成物を使用して、封止材フィルムを形成する。
本開示の組成物は、電子デバイスモジュール、特に電子デバイスモジュールの構築に使用される封止材フィルムを構築するために使用される。封止材フィルムは、電子デバイスの1つ以上の「スキン」として使用され、すなわち、電子デバイスの片面または両面に、例えば、前面封止材フィルムもしくは裏面封止材フィルムとして、または前面封止材フィルムおよび裏面封止材フィルムの両方として適用され、例えば、電子デバイスがその材料内に完全に封入される。
(i)120N/cm超、または130N/cm、または140N/cm、または150N/cm、または160N/cm、または170N/cmから、180N/cm、または190N/cm、または195N/cm、または200N/cmの初期ガラス接着力、および/または
(ii)60℃で、2.0×1015Ω.cm以上、または2.1×1015Ω.cm、または2.2×1015Ω.cm、または2.5×1015Ω.cm、または3.0×1015Ω.cm、または4.0×1015Ω.cm、または5.0×1015Ω.cm、または6.0×1015Ω.cm、または7.0×1015Ω.cm、または8.0×1015Ω.cm、または9.0×1015Ω.cmから、9.5×1015Ω.cm、または1.0×1016Ω.cm、または1.2×1016Ω.cm、または1.4×1016Ω.cm、または1.5×1016Ω.cmの体積抵抗率。
(i)140N/cm超〜190N/cmの初期ガラス接着力、および/または
(ii)60℃で2.1×1015Ω.cm以上〜1.0×1016Ω.cmの体積抵抗率。
EVA:0.955g/ccの密度(ASTM D792に従って測定される)、6.0g/10分のメルトインデックス(MI)(190℃、2.16kgでASTM D1238に従って測定される)、およびコポリマーの総重量に基づいて28重量%の酢酸ビニル含有量を有するエチレン/酢酸ビニルコポリマー(DuPontからElvax 260として入手可能)
組成物を、以下の表1に従って、第一に、表1に記載の所望のパーセンテージで、有機過酸化物、シランカップリング剤、および助剤(複数可)をガラス瓶内で予混合することによって調製する。実施例に応じて(表1を参照のこと)、EVAまたはPOEの乾燥ポリマーペレットをガラス瓶に入れる。硬化パッケージ(すなわち、有機過酸化物、シランカップリング剤、および助剤(複数可))のペレット中での均一分布および完全な浸漬を確保するために、ガラス瓶を40℃のオーブンに入れ、15分間毎に定期的に撹拌する。
Claims (14)
- 組成物を含む封止材フィルムであって、前記組成物が、
(A)0.850g/cc〜0.890g/ccの密度を有する非極性エチレン系ポリマーと、
(B)有機過酸化物と、
(C)シランカップリング剤と、
(D)リン酸トリアリルを含む助剤と、を含む、封止材フィルム。 - 前記非極性エチレン系ポリマーが、エチレン/アルファ−オレフィンコポリマーである、請求項1に記載の封止材フィルム。
- 前記非極性エチレン系ポリマーが、エチレン/アルファ−オレフィンランダムコポリマーおよびエチレン/アルファ−オレフィンブロックコポリマーからなる群から選択される、請求項2に記載の封止材フィルム。
- 前記組成物が、
(A)前記組成物の総重量に基づいて50重量%〜99重量%の前記非極性エチレン系ポリマーと、
(B)前記組成物の総重量に基づいて0.1重量%〜5重量%の前記有機過酸化物と、
(C)前記組成物の総重量に基づいて0.01重量%〜2重量%の前記シランカップリング剤と、
(D)前記組成物の総重量に基づいて0.01重量%〜1.5重量%の前記助剤と、を含む、請求項1〜3のいずれかに記載の封止材フィルム。 - 前記助剤が、前記組成物の総重量に基づいて0.2重量%〜1.0重量%の量で存在する、請求項4に記載の封止材フィルム。
- 前記助剤が、リン酸トリアリルおよび少なくとも1つの他の化合物を含む、請求項1〜5のいずれかに記載の封止材フィルム。
- 前記助剤が、前記助剤の総重量に基づいて20重量%超〜100重量%未満のリン酸トリアリルを含む、請求項1〜6のいずれかに記載の封止材フィルム。
- 前記助剤が、リン酸トリアリルと、(i)シアヌル酸トリアリルおよびイソシアヌル酸トリアリルの少なくとも一方との混合物を含む、請求項1〜7のいずれかに記載の封止材フィルム。
- 前記助剤が、前記助剤の総重量に基づいて50重量%〜100重量%未満のリン酸トリアリルを含む、請求項8に記載の封止材フィルム。
- 60℃で2.1×1015Ω.cm以上〜1.0×1016Ω.cmの体積抵抗率を有する、請求項1〜9のいずれかに記載の封止材フィルム。
- 電子デバイスモジュールであって、
電子デバイスと、
組成物の反応生成物である架橋ポリマー組成物から構成される少なくとも1つのフィルムと、を備え、前記組成物が、
(A)0.850g/cc〜0.890g/ccの密度を有する非極性エチレン系ポリマーと、
(B)有機過酸化物と、
(C)シランカップリング剤と、
(D)リン酸トリアリルを含む助剤と、を含む、電子デバイスモジュール。 - 前記少なくとも1つのフィルムが、60℃で2.1×1015Ω.cm以上〜1.0×1016Ω.cmの体積抵抗率を有する、請求項11に記載の電子デバイスモジュール。
- 前記架橋ポリマー組成物が、
(A)前記組成物の総重量に基づいて95重量%〜99重量%の前記非極性エチレン系ポリマーと、
(B)前記組成物の総重量に基づいて0.75重量%〜1.5重量%の有機過酸化物と、
(C)前記組成物の総重量に基づいて0.1重量%〜0.3重量%の前記シランカップリング剤と、
(D)前記組成物の総重量に基づいて0.2重量%〜1.3重量%の前記リン酸トリアリルを含む助剤と、の反応生成物であり、
前記少なくとも1つのフィルムが、60℃で2.2×1015Ω.cm以上〜9.5×1015Ω.cmの体積抵抗率を有する、請求項11〜12のいずれかに記載の電子デバイスモジュール。 - 前記電子デバイスが、光起電性電池である、請求項11〜13のいずれかに記載の電子デバイスモジュール。
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CN103289582B (zh) * | 2013-05-21 | 2014-11-19 | 上海海优威电子技术有限公司 | 交联型的poe太阳能光伏组件用封装胶膜 |
KR20170008811A (ko) * | 2014-06-27 | 2017-01-24 | 미쓰이 가가쿠 토세로 가부시키가이샤 | 태양 전지 밀봉재용 수지 조성물, 태양 전지 밀봉재 및 태양 전지 모듈 |
JP2017529461A (ja) * | 2014-07-23 | 2017-10-05 | ザ プロクター アンド ギャンブル カンパニー | 処理組成物 |
CN104263285A (zh) * | 2014-09-19 | 2015-01-07 | 乐凯胶片股份有限公司 | 一种光伏组件用聚烯烃封装胶膜 |
CN107148678A (zh) * | 2014-11-28 | 2017-09-08 | 三井化学东赛璐株式会社 | 太阳能电池模块 |
CN106684186B (zh) * | 2016-11-22 | 2018-05-29 | 苏州赛伍应用技术股份有限公司 | 一种无翻边粘结良好的封装胶膜 |
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JP2020529481A (ja) | 2020-10-08 |
CN110691833A (zh) | 2020-01-14 |
TW201903113A (zh) | 2019-01-16 |
US20200115517A1 (en) | 2020-04-16 |
CN110691833B (zh) | 2022-07-26 |
KR102396057B1 (ko) | 2022-05-10 |
EP3630905B1 (en) | 2022-01-05 |
KR20200015576A (ko) | 2020-02-12 |
BR112019024888A2 (pt) | 2020-06-16 |
EP3630905A4 (en) | 2020-12-23 |
WO2018218482A1 (en) | 2018-12-06 |
EP3630905A1 (en) | 2020-04-08 |
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