JP6862069B2 - フォーム状皮膚洗浄料 - Google Patents
フォーム状皮膚洗浄料 Download PDFInfo
- Publication number
- JP6862069B2 JP6862069B2 JP2019522199A JP2019522199A JP6862069B2 JP 6862069 B2 JP6862069 B2 JP 6862069B2 JP 2019522199 A JP2019522199 A JP 2019522199A JP 2019522199 A JP2019522199 A JP 2019522199A JP 6862069 B2 JP6862069 B2 JP 6862069B2
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- Prior art keywords
- component
- mass
- foam
- content
- fatty acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000006260 foam Substances 0.000 title description 86
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 86
- 239000000194 fatty acid Substances 0.000 claims description 86
- 229930195729 fatty acid Natural products 0.000 claims description 86
- -1 fatty acid ester Chemical class 0.000 claims description 59
- 150000004665 fatty acids Chemical class 0.000 claims description 44
- 239000000243 solution Substances 0.000 claims description 39
- 239000002202 Polyethylene glycol Substances 0.000 claims description 27
- 229920001223 polyethylene glycol Polymers 0.000 claims description 27
- 239000003380 propellant Substances 0.000 claims description 26
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 24
- 239000011550 stock solution Substances 0.000 claims description 20
- 239000003915 liquefied petroleum gas Substances 0.000 claims description 19
- 239000000443 aerosol Substances 0.000 claims description 18
- 239000003599 detergent Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 229920001285 xanthan gum Polymers 0.000 claims description 14
- 239000000230 xanthan gum Substances 0.000 claims description 14
- 235000010493 xanthan gum Nutrition 0.000 claims description 14
- 229940082509 xanthan gum Drugs 0.000 claims description 14
- 239000001569 carbon dioxide Substances 0.000 claims description 12
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 12
- 239000002253 acid Substances 0.000 claims description 10
- ARIWANIATODDMH-UHFFFAOYSA-N rac-1-monolauroylglycerol Chemical compound CCCCCCCCCCCC(=O)OCC(O)CO ARIWANIATODDMH-UHFFFAOYSA-N 0.000 claims description 10
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 claims description 10
- 239000002562 thickening agent Substances 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 9
- 239000004615 ingredient Substances 0.000 claims description 9
- 150000003839 salts Chemical class 0.000 claims description 9
- 239000012459 cleaning agent Substances 0.000 claims description 8
- 150000005846 sugar alcohols Polymers 0.000 claims description 7
- LKUNXBRZDFMZOK-GFCCVEGCSA-N Capric acid monoglyceride Natural products CCCCCCCCCC(=O)OC[C@H](O)CO LKUNXBRZDFMZOK-GFCCVEGCSA-N 0.000 claims description 5
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- 229940068939 glyceryl monolaurate Drugs 0.000 claims description 5
- LKUNXBRZDFMZOK-UHFFFAOYSA-N rac-1-monodecanoylglycerol Chemical compound CCCCCCCCCC(=O)OCC(O)CO LKUNXBRZDFMZOK-UHFFFAOYSA-N 0.000 claims description 5
- 230000014759 maintenance of location Effects 0.000 description 19
- 238000005187 foaming Methods 0.000 description 18
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- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 description 16
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- 125000004432 carbon atom Chemical group C* 0.000 description 13
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- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 6
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- 239000000693 micelle Substances 0.000 description 5
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- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 4
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 description 4
- CKLJMWTZIZZHCS-REOHCLBHSA-N L-aspartic acid Chemical compound OC(=O)[C@@H](N)CC(O)=O CKLJMWTZIZZHCS-REOHCLBHSA-N 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 235000003704 aspartic acid Nutrition 0.000 description 4
- OQFSQFPPLPISGP-UHFFFAOYSA-N beta-carboxyaspartic acid Natural products OC(=O)C(N)C(C(O)=O)C(O)=O OQFSQFPPLPISGP-UHFFFAOYSA-N 0.000 description 4
- 230000001815 facial effect Effects 0.000 description 4
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- 239000004220 glutamic acid Substances 0.000 description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 239000008213 purified water Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
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- 238000012360 testing method Methods 0.000 description 4
- NOOLISFMXDJSKH-KXUCPTDWSA-N (-)-Menthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1O NOOLISFMXDJSKH-KXUCPTDWSA-N 0.000 description 3
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 3
- RFVNOJDQRGSOEL-UHFFFAOYSA-N 2-hydroxyethyl octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCCO RFVNOJDQRGSOEL-UHFFFAOYSA-N 0.000 description 3
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 3
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 3
- 239000005635 Caprylic acid (CAS 124-07-2) Substances 0.000 description 3
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 3
- 239000005642 Oleic acid Substances 0.000 description 3
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 235000021355 Stearic acid Nutrition 0.000 description 3
- 239000004359 castor oil Substances 0.000 description 3
- 235000019438 castor oil Nutrition 0.000 description 3
- 229960000541 cetyl alcohol Drugs 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 3
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229940043348 myristyl alcohol Drugs 0.000 description 3
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 3
- 229960002446 octanoic acid Drugs 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 3
- 235000021313 oleic acid Nutrition 0.000 description 3
- 239000002540 palm oil Substances 0.000 description 3
- 239000001818 polyoxyethylene sorbitan monostearate Substances 0.000 description 3
- 235000010989 polyoxyethylene sorbitan monostearate Nutrition 0.000 description 3
- IEXXLSKKBWIDAC-ZOWNYOTGSA-M sodium;(3s)-3-(dodecanoylamino)-4-hydroxy-4-oxobutanoate Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CC(O)=O IEXXLSKKBWIDAC-ZOWNYOTGSA-M 0.000 description 3
- 239000008117 stearic acid Substances 0.000 description 3
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 2
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 2
- HOVAGTYPODGVJG-UVSYOFPXSA-N (3s,5r)-2-(hydroxymethyl)-6-methoxyoxane-3,4,5-triol Chemical compound COC1OC(CO)[C@@H](O)C(O)[C@H]1O HOVAGTYPODGVJG-UVSYOFPXSA-N 0.000 description 2
- 229940031723 1,2-octanediol Drugs 0.000 description 2
- WNWHHMBRJJOGFJ-UHFFFAOYSA-N 16-methylheptadecan-1-ol Chemical compound CC(C)CCCCCCCCCCCCCCCO WNWHHMBRJJOGFJ-UHFFFAOYSA-N 0.000 description 2
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- TWJNQYPJQDRXPH-UHFFFAOYSA-N 2-cyanobenzohydrazide Chemical compound NNC(=O)C1=CC=CC=C1C#N TWJNQYPJQDRXPH-UHFFFAOYSA-N 0.000 description 2
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- NCZPCONIKBICGS-UHFFFAOYSA-N 3-(2-ethylhexoxy)propane-1,2-diol Chemical compound CCCCC(CC)COCC(O)CO NCZPCONIKBICGS-UHFFFAOYSA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
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- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 description 2
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- VUYXVWGKCKTUMF-UHFFFAOYSA-N tetratriacontaethylene glycol monomethyl ether Chemical compound COCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO VUYXVWGKCKTUMF-UHFFFAOYSA-N 0.000 description 1
- 235000010384 tocopherol Nutrition 0.000 description 1
- 229960001295 tocopherol Drugs 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- FGMPLJWBKKVCDB-UHFFFAOYSA-N trans-L-hydroxy-proline Natural products ON1CCCC1C(O)=O FGMPLJWBKKVCDB-UHFFFAOYSA-N 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- OUYCCCASQSFEME-UHFFFAOYSA-N tyrosine Natural products OC(=O)C(N)CC1=CC=C(O)C=C1 OUYCCCASQSFEME-UHFFFAOYSA-N 0.000 description 1
- 239000004474 valine Substances 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Classifications
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/34—Alcohols
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C11D1/10—Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/08—Liquid soap, e.g. for dispensers; capsuled
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/22—Gas releasing
- A61K2800/222—Effervescent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- Detergent Compositions (AREA)
Description
成分A:N−アシルアミノ酸塩
成分B:ポリグリセリン脂肪酸エステル
成分C:モノグリセリン脂肪酸エステル
成分D:キサンタンガム及び/又はセルロース系増粘剤
成分E:多価アルコール
成分F:水
成分G:ポリエチレングリコール脂肪酸エステル
上記成分Aは、N−アシルアミノ酸塩である。成分Aは、アニオン界面活性剤であり、洗浄成分として作用しフォーム状皮膚洗浄料の洗浄力を高めるとともに、フォーム状皮膚洗浄料の起泡力を向上させる。成分Aは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Bは、ポリグリセリン脂肪酸エステルである。成分Bは、フォーム状皮膚洗浄料の濃密でクリーミーな泡(すなわち、細かく、高密度に形成した泡)の形成性を高める。また、フォーム状皮膚洗浄料の起泡力を向上させる。成分Bは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Cは、モノグリセリン脂肪酸エステルである。成分Cは、形成した泡をつぶれにくくし、フォーム状皮膚洗浄料の泡もち(泡の持続性)を向上させる。特に、水の存在下でもフォーム状皮膚洗浄料の泡もち(泡の持続性)を向上させることができる。成分Cは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Dは、キサンタンガム及び/又はセルロース系増粘剤、即ち、キサンタンガム及びセルロース系増粘剤のうちの一方又は両方である。成分Dは、形成した泡をつぶれにくくし、フォーム状皮膚洗浄料の泡もち(泡の持続性)を向上させる。特に、エアゾール剤型で用いることにより、上記効果を発揮しやすい。成分Dをポンプ式のフォーマー容器に充填される洗浄料に配合する場合には、泡の形成が不十分となり、濃密でクリーミーな泡を形成しにくくなりやすい。成分Dは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Eは、多価アルコールである。成分Eは、泡質(濃密でクリーミーな泡質)をより一層向上する効果を有する。また、洗い上がりのしっとり感を向上させる効果を有する。上記成分Eは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記成分Fは水であり、特に限定されないが、精製水が好ましい。原液100質量%中の、成分Fの水の含有量は、良好な泡を形成する観点から、18.0〜96.25質量%が好ましく、より好ましくは50.0〜90.0質量%、さらに好ましくは60.0〜80.0質量%である。
上記成分Gは、ポリエチレングリコール脂肪酸エステルである。成分Gは、フォーム状皮膚洗浄料の泡もちと泡質のより一層の向上に効果的である。上記成分Gは、1種のみを用いてもよいし、2種以上を用いてもよい。
上記問題を解決すべく、本発明においては、ポリグリセリン脂肪酸エステル(成分B)とモノグリセリン脂肪酸エステル(成分C)を併用している。成分Bは、比較的嵩高い親水基を有する。これにより、フォーム状皮膚洗浄料の泡形成時に成分Bが気液界面に配向した際、形成するミセルの曲率が大きくなるためと推定されるが、細かな泡を形成しうる。一方、成分Cは、比較的コンパクトな親水基を有するため、成分A及び成分Bが配向したミセルの気液界面において、成分Aや成分Bの隙間に入り込む形で配向することにより界面を安定化させ泡の膜強度を向上させるためと推定されるが、泡の持続性(泡もち)が向上する。
さらに、水溶性の増粘剤であるキサンタンガム及び/又はセルロース系増粘剤(成分D)により、泡の液膜の粘性を高め、泡膜を強固にし、形成した泡をつぶれにくくし、泡もちを向上させている。さらにまた、多価アルコール(成分E)は、ミセル間の水中に存在し、ミセルを形成する成分Bの親水基と相互作用することにより、ミセル同士を安定化させるものと推定されるが、泡質を向上させる。また、保湿効果により、洗い上がりのしっとり感にも寄与する。
加えて、ポリエチレングリコール脂肪酸エステル(成分G)は成分Bと同様に比較的大きな親水基を有し、さらに増粘効果を有するため、これを添加する場合には、泡質及び泡もちをより一層向上させることができる。
表に記した組成からなる原液をエアゾール容器(φ35mm×105mm、アルミ缶、容器満注量:91ml)に充填し、エアゾールバルブを該容器にクリンチした後、噴射剤をステムより充填し、適したスパウトを装着し、フォーム状皮膚洗浄料を得た。なお、エアゾール容器に充填した原液と噴射剤の合計量は40gであった。噴射剤は、LPG(イソブタン100%)と炭酸ガスの混合物であり、LPGと炭酸ガスの質量比は3.0:0.5(LPG:炭酸ガス)であった。原液と噴射剤の質量比は96.5:3.5(原液:噴射剤)であった。
N−ヤシ油脂肪酸アシル−L−グルタミン酸ナトリウム:旭化成ケミカルズ社製、商品名「アミノサーファクトACDS−L」
モノミリスチン酸デカグリセリル:青木油脂工業社製、商品名「グリサーフ 10MM」
モノラウリン酸デカグリセリル:日本サーファクタント工業社製、商品名「DECAGLYN1−L」
モノラウリン酸グリセリル:太陽化学社製、商品名「サンソフトNo.750−C」
モノカプリル酸グリセリル:太陽化学社製、商品名「サンソフトNo.700P−2−C」
モノカプリン酸グリセリル:太陽化学社製、商品名「サンソフトNo.760−C」
キサンタンガム:DSP五協フード&ケミカル社製、商品名「エコーガムT」
ヒドロキシエチルセルロース:ダイセル社製、商品名「HECダイセルSE400」
グリセリン:阪本薬品工業社製、商品名「化粧用濃グリセリン」
ジプロピレングリコール:シェルケミカルズジャパン社製、商品名「ジプロピレングリコールS」
ポリエチレングリコール:三洋化成工業社製、商品名「PEG−1500」、数平均分子量1500
モノステアリン酸ポリエチレングリコール:花王社製、商品名「エマノーン3199VB」、酸化エチレンの付加モル数150
ミリスチルアルコール:花王社製、商品名「カルコール4098」
ヤシ油脂肪酸ソルビタン:花王社製、商品名「レオドールスーパーSP−L10」
モノステアリン酸ポリオキシエチレンソルビタン:花王社製、商品名「レオドールTW−S120V」
キムタオル(4つ折りタイプ:日本製紙クレシア社製)の上に、各実施例及び各比較例のフォーム状皮膚洗浄料を1秒間吐出した。
吐出後10秒後に、泡の形成性及び形成した泡を目視にて確認し、下記の基準で評価した。評価結果を表に記載した。
○(良好):ドーム状に泡が形成していた。
×(不良):発泡が不十分でありドーム状に泡が形成しなかった。
○(良好):細かな泡が均一かつ高密度に形成しており、全体的にクリーミーな外観であった。
×(不良):泡の表面に比較的大きな気泡が認められ、泡の密度が低く、泡の大きさが不均一であった。
試験例1の評価直後に、ドーム状に形成した泡の上端から約20cm離れた距離から、ポンプ容器(噴霧吐出量:0.5mL/1プッシュ)に充填した精製水を2プッシュ、泡全体に噴霧し、30秒後に泡を目視にて確認し、下記の基準で評価した。評価結果を表に記載した。
○(良好):吐出直後の泡形状が維持されていた。
○(良好):吐出直後の泡形状が明らかに崩れていた。
さらに、実施例1〜30で調製したフォーム状皮膚洗浄料について、以下の方法により、「使用感」を評価した。なお、評価は、3名の専門評価員が行った。
各実施例及び各比較例のフォーム状皮膚洗浄料を掌に2秒間吐出し、吐出した泡により洗顔を行った。洗顔後の肌の感触より使用感を評価した。
その結果、実施例1〜30の全てのフォーム状皮膚洗浄料を用いた場合において、目刺激は感じられなかった。また、実施例1〜5、7〜11、13〜17、19〜23、25〜27、29〜30のフォーム状皮膚洗浄料を用いた場合には、汚れの洗い落ち感とつっぱりのなさの両立した良好な洗い上がりであった。一方、実施例6、18のフォーム状皮膚洗浄料は脱脂力が強く、洗顔後の肌のさっぱり感が少し強すぎ、つっぱり感がやや感じられた。また、一方、実施例12、24、28のフォーム状皮膚洗浄料を用いた場合には、洗顔後の肌にぬるつき又はべたつきがやや感じられた。
(原液)
L−メントール 0.1質量%
イソプロピルメチルフェノール 0.1質量%
グリチルリチン酸ジカリウム 0.1質量%
キサンタンガム 0.3質量%
N−ラウロイル−L−アスパラギン酸ナトリウム 3.0質量%
グリセリン 15.0質量%
ソルビトール 5.0質量%
ポリエチレングリコール(PEG1500) 5.0質量%
ポリオキシエチレン硬化ヒマシ油 0.5質量%
ヤシ油脂肪酸ソルビタン 0.2質量%
セタノール 0.2質量%
モノラウリン酸デカグリセリル 4.0質量%
モノラウリン酸グリセリル 1.5質量%
ヒアルロン酸ナトリウム 0.1質量%
グリセリンモノ2−エチルヘキシルエーテル 0.1質量%
香料 0.1質量%
精製水 残部
合計 100質量%
(噴射剤)
LPG(イソブタン100%) 86.0質量%
炭酸ガス 14.0質量%
合計 100質量%
原液/噴射剤(質量比)=97/3
(原液)
L−メントール 0.1質量%
N−ヤシ油脂肪酸アシル−L−グルタミン酸ナトリウム 5.0質量%
ミリスチン酸 0.1質量%
モノステアリン酸ポリエチレングリコール 0.5質量%
ヤシ油脂肪酸ソルビタン 0.5質量%
モノステアリン酸ポリオキシエチレンソルビタン 1.0質量%
ヒドロキシエチルセルロース 0.3質量%
チャエキス 3.0質量%
ジプロピレングリコール 5.0質量%
グリセリン 5.0質量%
1,3−ブチレングリコール 5.0質量%
フェノキシエタノール 0.1質量%
モノミリスチン酸デカグリセリル 5.0質量%
モノカプリル酸グリセリル 0.5質量%
ラベンダー油 0.1質量%
精製水 残部
合計 100質量%
(噴射剤)
LPG(プロパン1質量%/ブタン99質量%、20℃における蒸気圧0.39MPa)
100質量%
原液/噴射剤(質量比)=95/5
(原液)
N−ヤシ油脂肪酸アシル−L−グルタミン酸ナトリウム 5.0質量%
モノラウリン酸ポリエチレングリコール 1.0質量%
ヤシ油脂肪酸ソルビタン 0.5質量%
ポリオキシエチレンセチルエーテル(セテス−20) 1.0質量%
キサンタンガム 0.3質量%
アロエエキス 0.1質量%
カンゾウ抽出末 0.1質量%
グリセリン 20.0質量%
ジプロピレングリコール 5.0質量%
マルチトール 5.0質量%
1,2−オクタンジオール 0.1質量%
モノラウリン酸デカグリセリル 4.0質量%
モノカプリン酸グリセリル 2.0質量%
オレンジ油 0.1質量%
精製水 残部
合計 100質量%
(噴射剤)
LPG(イソブタン100%) 86.0質量%
炭酸ガス 14.0質量%
合計 100質量%
原液/噴射剤(質量比)=96/4
Claims (6)
- 原液と噴射剤とがエアゾール容器に充填されたフォーム状皮膚洗浄料であって、前記原液が、下記成分A、下記成分B、下記成分C、下記成分D、下記成分E、及び下記成分Fを含有し、
前記成分Dがキサンタンガムを含み、
前記原液中の、前記成分Aの含有量が0.5〜15.0質量%、前記成分Bの含有量が1.0〜7.0質量%、前記成分Cの含有量が0.1〜10.0質量%、前記成分Dの含有量が0.05〜2.0質量%、前記成分Eの含有量が3.0〜40.0質量%、前記成分Fの含有量が18.0〜90.0質量%であることを特徴とするフォーム状皮膚洗浄料。
成分A:N−アシルアミノ酸塩
成分B:モノラウリン酸ポリグリセリル及び/又はモノミリスチン酸ポリグリセリル
成分C:モノラウリン酸グリセリル、モノカプリル酸グリセリル、及びモノカプリン酸グリセリルからなる群より選択される1種以上
成分D:キサンタンガム及び/ 又はセルロース系増粘剤
成分E:多価アルコール
成分F:水 - 前記原液が、さらに、下記成分Gを含有する、請求項1に記載のフォーム状皮膚洗浄料。
成分G:ポリエチレングリコール脂肪酸エステル - 前記原液中の、前記成分Gの含有量が0.05〜3.0質量%である請求項2に記載のフォーム状皮膚洗浄料。
- 前記原液が高級脂肪酸及び高級脂肪酸塩を含まないか、または、前記原液中の高級脂肪酸の含有量と高級脂肪酸塩の含有量の合計量が0.1質量%以下である請求項1〜3のいずれか一項に記載のフォーム状皮膚洗浄料。
- 前記噴射剤が、液化石油ガスを含有する、請求項1〜4のいずれか一項に記載のフォーム状皮膚洗浄料。
- 前記噴射剤が、さらに、炭酸ガスを含有する、請求項1〜5のいずれか一項に記載のフォーム状皮膚洗浄料。
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