JP6804568B2 - 加圧接着型粘着テープ - Google Patents
加圧接着型粘着テープ Download PDFInfo
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- JP6804568B2 JP6804568B2 JP2018568030A JP2018568030A JP6804568B2 JP 6804568 B2 JP6804568 B2 JP 6804568B2 JP 2018568030 A JP2018568030 A JP 2018568030A JP 2018568030 A JP2018568030 A JP 2018568030A JP 6804568 B2 JP6804568 B2 JP 6804568B2
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- adhesive tape
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- VEYCPJGKKJULEP-UHFFFAOYSA-N prop-2-enoic acid sulfuric acid Chemical compound OC(=O)C=C.OS(O)(=O)=O VEYCPJGKKJULEP-UHFFFAOYSA-N 0.000 description 1
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 description 1
- BOQSSGDQNWEFSX-UHFFFAOYSA-N propan-2-yl 2-methylprop-2-enoate Chemical compound CC(C)OC(=O)C(C)=C BOQSSGDQNWEFSX-UHFFFAOYSA-N 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 229920005604 random copolymer Polymers 0.000 description 1
- 239000002964 rayon Substances 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920005573 silicon-containing polymer Polymers 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000010378 sodium ascorbate Nutrition 0.000 description 1
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 description 1
- 229960005055 sodium ascorbate Drugs 0.000 description 1
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 1
- 229940079827 sodium hydrogen sulfite Drugs 0.000 description 1
- 229940001584 sodium metabisulfite Drugs 0.000 description 1
- 235000010262 sodium metabisulphite Nutrition 0.000 description 1
- 235000010265 sodium sulphite Nutrition 0.000 description 1
- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical compound [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 description 1
- OGRPJZFGZFQRHZ-UHFFFAOYSA-M sodium;4-octoxy-4-oxo-3-sulfobutanoate Chemical compound [Na+].CCCCCCCCOC(=O)C(S(O)(=O)=O)CC([O-])=O OGRPJZFGZFQRHZ-UHFFFAOYSA-M 0.000 description 1
- IRZFQKXEKAODTJ-UHFFFAOYSA-M sodium;propan-2-yloxymethanedithioate Chemical compound [Na+].CC(C)OC([S-])=S IRZFQKXEKAODTJ-UHFFFAOYSA-M 0.000 description 1
- 229940035044 sorbitan monolaurate Drugs 0.000 description 1
- 239000001587 sorbitan monostearate Substances 0.000 description 1
- 235000011076 sorbitan monostearate Nutrition 0.000 description 1
- 229940035048 sorbitan monostearate Drugs 0.000 description 1
- 235000019337 sorbitan trioleate Nutrition 0.000 description 1
- 229960000391 sorbitan trioleate Drugs 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229920003048 styrene butadiene rubber Polymers 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- 229940095064 tartrate Drugs 0.000 description 1
- OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 description 1
- SJMYWORNLPSJQO-UHFFFAOYSA-N tert-butyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC(C)(C)C SJMYWORNLPSJQO-UHFFFAOYSA-N 0.000 description 1
- NMOALOSNPWTWRH-UHFFFAOYSA-N tert-butyl 7,7-dimethyloctaneperoxoate Chemical compound CC(C)(C)CCCCCC(=O)OOC(C)(C)C NMOALOSNPWTWRH-UHFFFAOYSA-N 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 150000003557 thiazoles Chemical class 0.000 description 1
- 150000003585 thioureas Chemical class 0.000 description 1
- RUELTTOHQODFPA-UHFFFAOYSA-N toluene 2,6-diisocyanate Chemical compound CC1=C(N=C=O)C=CC=C1N=C=O RUELTTOHQODFPA-UHFFFAOYSA-N 0.000 description 1
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 238000007740 vapor deposition Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000007883 water-soluble azo polymerization initiator Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 239000004246 zinc acetate Substances 0.000 description 1
- RKQOSDAEEGPRER-UHFFFAOYSA-L zinc diethyldithiocarbamate Chemical compound [Zn+2].CCN(CC)C([S-])=S.CCN(CC)C([S-])=S RKQOSDAEEGPRER-UHFFFAOYSA-L 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- DUBNHZYBDBBJHD-UHFFFAOYSA-L ziram Chemical compound [Zn+2].CN(C)C([S-])=S.CN(C)C([S-])=S DUBNHZYBDBBJHD-UHFFFAOYSA-L 0.000 description 1
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- C09J7/00—Adhesives in the form of films or foils
- C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
- C09J7/38—Pressure-sensitive adhesives [PSA]
- C09J7/381—Pressure-sensitive adhesives [PSA] based on macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C09J7/385—Acrylic polymers
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- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/10—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet
- C09J2301/12—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers
- C09J2301/124—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present on both sides of the carrier, e.g. double-sided adhesive tape
- C09J2301/1242—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive tape or sheet by the arrangement of layers the adhesive layer being present on both sides of the carrier, e.g. double-sided adhesive tape the opposite adhesive layers being different
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- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/20—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive itself
- C09J2301/21—Additional features of adhesives in the form of films or foils characterized by the structural features of the adhesive itself the adhesive layer being formed by alternating adhesive areas of different nature
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- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
- C09J2301/408—Additional features of adhesives in the form of films or foils characterized by the presence of essential components additives as essential feature of the adhesive layer
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- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
- C09J2301/412—Additional features of adhesives in the form of films or foils characterized by the presence of essential components presence of microspheres
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Description
支持体と、該支持体の一方の側に備えられた第一粘着剤層と、該支持体のもう一方の側に備えられた第二粘着剤層と、を有する加圧接着型粘着テープであって、
幅20mmの該加圧接着型粘着テープの該第一粘着剤層をポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合せた直後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙表面から剥離して測定した180°ピール粘着力をA1、
幅20mmの該加圧接着型粘着テープの該第二粘着剤層をポリ塩化ビニル壁紙裏面に0.5kgのローラーで1往復圧着して貼り合せた直後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙裏面から剥離して測定した180°ピール粘着力をA2、
幅20mmの前記加圧接着型粘着テープの前記第一粘着剤層をポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合せてから温度60℃で1週間保存後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙表面から剥離して測定した180°ピール粘着力をB1、
幅20mmの前記加圧接着型粘着テープの前記第二粘着剤層をポリ塩化ビニル壁紙裏面に2kgのローラーで1往復圧着して貼り合せてから温度60℃で1週間保存後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙裏面から剥離して測定した180°ピール粘着力をB2、としたときに、
A1<A2であり、且つ、B1<B2である。
本発明の加圧接着型粘着テープは、支持体と、該支持体の一方の側に備えられた第一粘着剤層と、該支持体のもう一方の側に備えられた第二粘着剤層と、を有する加圧接着型粘着テープである。支持体と第一粘着剤層との間には、本発明の効果を損なわない範囲で任意の適切な他の層を備えていてもよい。支持体と第二粘着剤層との間には、本発明の効果を損なわない範囲で任意の適切な他の層を備えていてもよい。
(1)幅20mmの該加圧接着型粘着テープの該第一粘着剤層をポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合せた直後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙表面から剥離して測定した180°ピール粘着力をA1、
(2)幅20mmの該加圧接着型粘着テープの該第二粘着剤層をポリ塩化ビニル壁紙裏面に0.5kgのローラーで1往復圧着して貼り合せた直後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙裏面から剥離して測定した180°ピール粘着力をA2、
(3)幅20mmの前記加圧接着型粘着テープの前記第一粘着剤層をポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合せてから温度60℃で1週間保存後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙表面から剥離して測定した180°ピール粘着力をB1、
(4)幅20mmの前記加圧接着型粘着テープの前記第二粘着剤層をポリ塩化ビニル壁紙裏面に2kgのローラーで1往復圧着して貼り合せてから温度60℃で1週間保存後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙裏面から剥離して測定した180°ピール粘着力をB2、としたときに、A1<A2であり、且つ、B1<B2である。
支持体は、本発明の効果を損なわない範囲で任意の適切な材料からなる支持体を採用し得る。このような支持体の材料としては、例えば、樹脂フィルム、紙、布、ゴムシート、発泡体シート、金属箔、これらの複合体などが挙げられる。
第一粘着剤層を構成する粘着剤としては、本発明の効果を損なわない範囲で任意の適切な粘着剤を採用し得る。第一粘着剤層を構成する粘着剤は、1種のみであってもよいし、2種以上であってもよい。このような粘着剤としては、例えば、アクリル系粘着剤、シリコーン系粘着剤、ゴム系粘着剤、ポリアミド系粘着剤、ポリエステル系粘着剤、エチレン−酢酸ビニル共重合体系粘着剤、ポリウレタン系粘着剤などが挙げられ、好ましくは、アクリル系粘着剤、シリコーン系粘着剤、ゴム系粘着剤である。
アクリル系粘着剤は、好ましくは、(メタ)アクリル酸アルキルエステル由来の構成単位を主たるモノマー単位とするアクリル系重合体をベースポリマーとして含有する。アクリル系重合体は、ランダム共重合体、ブロック共重合体、グラフト共重合体など、任意の適切な構造を採り得る。アクリル系粘着剤は、1種のみであってもよいし、2種以上であってもよい。
シリコーン系粘着剤としては、本発明の効果を損なわない範囲で任意の適切なシリコーン系粘着剤を採用し得る。このようなシリコーン系粘着剤としては、例えば、付加型シリコーン系粘着剤、過酸化物硬化型シリコーン系粘着剤、縮合型シリコーン系粘着剤などが挙げられる。シリコーン系粘着剤としては、1液型シリコーン系粘着剤、2液型シリコーン系粘着剤が挙げられる。シリコーン系粘着剤は、1種のみであってもよいし、2種以上であってもよい。
ゲル分率(重量%)=(A−B)/(C−B)×100
ゴム系粘着剤は、ゴム系ポリマーをベースポリマーとし、ベースポリマーが天然ゴム(NR)であるもの、ベースポリマーが変性天然ゴムであるもの、ベースポリマーが合成ゴムであるものが包含される。
第二粘着剤層は、好ましくは、本体層と、本体層の表面に設けられた複数の凸部とを含む。
本体層としては、≪第一粘着剤層≫の項目で説明した第一粘着剤層を構成する粘着層をそのまま援用し得る。
本体層の表面に設けられる複数の凸部は、例えば、壁紙等を十分な圧力で加圧するまでは、壁紙等が本体層と接触しない状態を保つために設けられており、自身は壁紙等に接触するだけでは高い粘着力を発現しない低粘着性の粘着剤により形成される。このため、第二粘着剤層上において壁紙等を移動させることができ、壁紙等の位置調整が可能になる。
本発明の加圧接着型粘着テープを使用するまでは、図2に示すように、第二粘着剤層20の表面は剥離ライナー40で保護されていることが好ましい。剥離ライナー40は、好ましくは、本発明の加圧接着型粘着テープを用いて壁紙等の貼付施工を行う際に剥離される。
(1)紙、織布、不織布(例えば、ポリエステル(例えば、ポリエチレンテレフタレート(PET)等)不織布等)、
(2)ポリエステル(例えば、ポリエチレンテレフタレート(PET)等)、ナイロン、サラン(商品名)、ポリ塩化ビニル、ポリエチレン、ポリプロピレン、エチレン−酢酸ビニル共重合体、ポリテトラフルオロエチレン、アイオノマーから選ばれる少なくとも1種の樹脂を成分とする中実のフィルムに機械的に穿孔処理を施したフィルム、
(3)ポリオレフィン発泡体(例えば、非架橋ポリエチレン発泡体、架橋ポリエチレン発泡体、ポリプロピレン発泡体、ポリエチレン(PE)を成分とする発泡体、ポリプロピレン(PP)を成分とする発泡体、ポリエチレン(PE)とポリプロピレン(PP)を成分とする発泡体等)、ポリエステル発泡体(例えば、ポリエチレンテレフタレート発泡体等)、ウレタン発泡体(例えば、軟質ウレタンフォーム、硬質ウレタンフォーム、ウレタン変性ポリイソシアヌレートフォーム、ポリイソシアヌレートフォーム等)、ゴム系発泡体などの発泡体フィルム、
などが挙げられる。これらの中でも、十分なクッション性が得られやすい点から、発泡体フィルムが好ましく、ポリオレフィン発泡体フィルムがより好ましい。
PP板(厚さ:2mm)に両面テープ(日東電工株式会社製、品番:No.5000NS)によってポリ塩化ビニル壁紙(サンゲツ社製、品番:SP9919)を、柄面が表面になるように貼り合せ、被着体(1)とした。
加圧接着型粘着テープの第二粘着剤層側の剥離ライナーを剥離し、露出させた第二粘着剤層を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラーS10」、東レ社製)に貼り合わせ、試験片を得た。得られた試験片を幅20mmにカットし、もう一方の剥離ライナーを剥離し、露出させた第一粘着剤層を被着体(1)のポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合わせ、直後に、引張圧縮試験機(装置名「TG−1kN」、ミネベア社製)によって、温度23℃、湿度50%RH、引張速度300mm/分で、加圧接着型粘着テープをポリ塩化ビニル壁紙表面から剥離して、180°ピール粘着力A1を測定した。
PP板(厚さ:2mm)に両面テープ(日東電工株式会社製、品番:No,5000NS)によってポリ塩化ビニル壁紙(ルノン社製、品番:RH9392)を、無地面が表面になるように貼り合せ、被着体(2)とした。
加圧接着型粘着テープの第一粘着剤層側の剥離ライナーを剥離し、露出させた第一粘着剤層を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラーS10」、東レ社製)に貼り合わせ、試験片を得た。得られた試験片を幅20mmにカットし、もう一方の剥離ライナーを剥離し、露出させた第二粘着剤層を被着体(2)のポリ塩化ビニル壁紙裏面に0.5kgのローラーで1往復圧着して貼り合わせ、直後に、引張圧縮試験機(装置名「TG−1kN」、ミネベア社製)によって、温度23℃、湿度50%RH、引張速度300mm/分で、加圧接着型粘着テープをポリ塩化ビニル壁紙裏面から剥離して、180°ピール粘着力A2を測定した。
PP板(厚さ:2mm)に両面テープ(日東電工株式会社製、品番:No.5000NS)によってポリ塩化ビニル壁紙(サンゲツ社製、品番:SP9919)を、柄面が表面になるように貼り合せ、被着体(1)とした。
加圧接着型粘着テープの第二粘着剤層側の剥離ライナーを剥離し、露出させた第二粘着剤層を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラーS10」、東レ社製)に貼り合わせ、試験片を得た。得られた試験片を幅20mmにカットし、もう一方の剥離ライナーを剥離し、露出させた第一粘着剤層を被着体(1)のポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合わせ、温度60℃で1週間保存後に、引張圧縮試験機(装置名「TG−1kN」、ミネベア社製)によって、温度23℃、湿度50%RH、引張速度300mm/分で、加圧接着型粘着テープをポリ塩化ビニル壁紙表面から剥離して、180°ピール粘着力B1を測定した。
PP板(厚さ:2mm)に両面テープ(日東電工株式会社製、品番:No.5000NS)によってポリ塩化ビニル壁紙(ルノン社製、品番:RH9392)を、無地面が表面になるように貼り合せ、被着体(2)とした。
加圧接着型粘着テープの第一粘着剤層側の剥離ライナーを剥離し、露出させた第一粘着剤層を厚さが25μmのポリエチレンテレフタレート(PET)フィルム(商品名「ルミラーS10」、東レ社製)に貼り合わせ、試験片を得た。得られた試験片を幅20mmにカットし、もう一方の剥離ライナーを剥離し、露出させた第二粘着剤層を被着体(2)のポリ塩化ビニル壁紙裏面に2kgのローラーで1往復圧着して貼り合わせ、温度60℃で1週間保存後に、引張圧縮試験機(装置名「TG−1kN」、ミネベア社製)によって、温度23℃、湿度50%RH、引張速度300mm/分で、加圧接着型粘着テープをポリ塩化ビニル壁紙裏面から剥離して、180°ピール粘着力B2を測定した。
(モノマーエマルションA)
容器に原料として、2−エチルヘキシルアクリレート(2−EHA)100部、反応性界面活性剤であるアクアロンHS−1025(第一工業製薬(株)製)1.5部、イオン交換水82部の混合物を作製し、ホモミキサーを用い窒素雰囲気下で5分間、6000rpmで撹拌し、モノマーエマルションAを調製した。
(モノマーエマルションB)
容器に原料として、メチルメタクリレート(MMA)80部、ブチルアクリレート(BA)10部、アクリル酸(AA)5部、メタクリル酸(MAA)5部、反応性界面活性剤であるアクアロンHS−1025(第一工業製薬(株)製)1.5部、イオン交換水82部の混合物を作製し、ホモミキサーを用い窒素雰囲気下で5分間、6000rpmで撹拌し、モノマーエマルションBを調製した。
(水分散型のアクリル系粘着剤)
冷却管、窒素導入管、温度計、滴下設備、及び撹拌羽根を備えた反応容器に、反応性界面活性剤であるアクアロンHS−1025(第一工業製薬(株)製)0.5部、イオン交換水76.8部を入れ、撹拌しながら十分に窒素置換した後、反応液を60℃まで昇温した。60℃で一定になったことを確認した後、水溶性アゾ重合開始剤であるVA−57(和光純薬(株)製)0.05部を添加し、10分後モノマーエマルション(A)150.6部を、2時間半かけて滴下し、コア層となる共重合体を得た。次いで、VA−57を0.05部更に添加し、10分後、モノマーエマルション(B)37.6部を45分かけて滴下し、シェル層となる共重合体を形成して、分散質としてコアシェル型アクリル系共重合体粒子を含む、水分散型のアクリル系粘着剤を製造した。コアシェル型アクリル系共重合体粒子のゾル重量平均分子量は200000であった。コアシェル型アクリル系共重合体粒子のレーザー回折・散乱法により測定される体積基準のメディアン径(D50)は160nmであった。このようにして得た水分散型のアクリル系粘着剤のコアシェル型アクリル系共重合体粒子(固形分)100部当たり、濃度10%のアンモニア水を0.18重量部、重合ロジンエステル系粘着付与剤(荒川化学工業(株)製の「スーパーエステルE−865−NT」)10部(固形分)を添加して、最終の、水分散型のアクリル系粘着剤(1)とした。
(加圧接着型粘着テープの作製)
ゴム系両面粘着テープ(No.513(Nitto製))の粘着剤表面に、塗工機を用いて、水分散型のアクリル系粘着剤(1)(コアシェル比率が80対20)を塗工し、ストライプ状の凸部を形成した。粘着剤面積率が90%(凸部の線幅0.5mm、線のピッチ4.50mm)、凸部の狙い高さが25μmとなるように塗工した。塗工時におけるテープの搬送速度は10m/minとし、110℃で1分程度乾燥した。凸部を保護するためクッション性を有する剥離ライナーと貼り合わせ巻き取り、加圧接着型粘着テープ(1)を得た。
粘着剤面積率は以下の式から求めた。
粘着剤面積率(%)=(1−凸部の線幅/(凸部の線幅+隣接する凸部間のピッチ))×100
結果を表1に示した。
凸部の形成において、粘着剤面積率が66%(凸部の線幅0.5mm、線のピッチ1mm)、凸部の狙い高さが25μmとなるように塗工した以外は、実施例1と同様に行い、加圧接着型粘着テープ(C1)を得た。
結果を表1に示した。
20 第二粘着剤層
20a 本体層
20b 凸部
21 コアシェル型アクリル系共重合体粒子
22 コア
23 シェル
30 支持体
40 剥離ライナー
50 壁
50A 壁の表面
60 壁紙
100 加圧接着型粘着テープ
Claims (7)
- 支持体と、該支持体の一方の側に備えられた第一粘着剤層と、該支持体のもう一方の側に備えられた第二粘着剤層と、を有する加圧接着型粘着テープであって、
該第二粘着剤層は、本体層と、該本体層の表面に設けられた複数の凸部とを含み、
該凸部は、アクリル系共重合体粒子の凝集体で構成され、
該アクリル系共重合体粒子のゾル重量平均分子量(Mw)が、1.0×10 4 より大きく、1.0×10 7 以下であり、
幅20mmの該加圧接着型粘着テープの該第一粘着剤層をポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合せた直後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙表面から剥離して測定した180°ピール粘着力をA1、
幅20mmの該加圧接着型粘着テープの該第二粘着剤層をポリ塩化ビニル壁紙裏面に0.5kgのローラーで1往復圧着して貼り合せた直後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙裏面から剥離して測定した180°ピール粘着力をA2、
幅20mmの前記加圧接着型粘着テープの前記第一粘着剤層をポリ塩化ビニル壁紙表面に2kgのローラーで1往復圧着して貼り合せてから温度60℃で1週間保存後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙表面から剥離して測定した180°ピール粘着力をB1、
幅20mmの前記加圧接着型粘着テープの前記第二粘着剤層をポリ塩化ビニル壁紙裏面に2kgのローラーで1往復圧着して貼り合せてから温度60℃で1週間保存後に、引張圧縮試験機によって、温度23℃、湿度50%RH、引張速度300mm/分で該加圧接着型粘着テープを該ポリ塩化ビニル壁紙裏面から剥離して測定した180°ピール粘着力をB2、としたときに、
A1<A2であり、且つ、B1<B2である、
加圧接着型粘着テープ。 - 前記B1が1N/20mm以上である、請求項1に記載の加圧接着型粘着テープ。
- 前記B2が1N/20mm以上である、請求項1または2に記載の加圧接着型粘着テープ。
- 前記A1が1N/20mm以上である、請求項1から3までのいずれかに記載の加圧接着型粘着テープ。
- 前記A2が1N/20mm以上である、請求項1から4までのいずれかに記載の加圧接着型粘着テープ。
- 前記B1が4N/20mm以下である、請求項1から5までのいずれかに記載の加圧接着型粘着テープ。
- 前記A2が5N/20mm以下である、請求項1から6までのいずれかに記載の加圧接着型粘着テープ。
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