JP6577462B2 - 粗メタノールから硫黄を除去する方法 - Google Patents
粗メタノールから硫黄を除去する方法 Download PDFInfo
- Publication number
- JP6577462B2 JP6577462B2 JP2016521949A JP2016521949A JP6577462B2 JP 6577462 B2 JP6577462 B2 JP 6577462B2 JP 2016521949 A JP2016521949 A JP 2016521949A JP 2016521949 A JP2016521949 A JP 2016521949A JP 6577462 B2 JP6577462 B2 JP 6577462B2
- Authority
- JP
- Japan
- Prior art keywords
- methanol
- organic solvent
- nonpolar organic
- washing
- crude
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
- C07C29/84—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0488—Flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C11/00—Regeneration of pulp liquors or effluent waste waters
- D21C11/0007—Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C27/00—Processes involving the simultaneous production of more than one class of oxygen-containing compounds
- C07C27/26—Purification; Separation; Stabilisation
- C07C27/34—Purification; Separation; Stabilisation by extraction
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/02—Monohydroxylic acyclic alcohols
- C07C31/04—Methanol
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
- Paper (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE1351209-0 | 2013-10-11 | ||
| SE1351209 | 2013-10-11 | ||
| PCT/SE2014/051205 WO2015053704A1 (en) | 2013-10-11 | 2014-10-13 | Process for removal of sulphur from raw methanol |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016536290A JP2016536290A (ja) | 2016-11-24 |
| JP2016536290A5 JP2016536290A5 (https=) | 2017-11-09 |
| JP6577462B2 true JP6577462B2 (ja) | 2019-09-18 |
Family
ID=52813419
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016521949A Active JP6577462B2 (ja) | 2013-10-11 | 2014-10-13 | 粗メタノールから硫黄を除去する方法 |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US10160706B2 (https=) |
| EP (1) | EP3055280B1 (https=) |
| JP (1) | JP6577462B2 (https=) |
| CN (1) | CN105793220B (https=) |
| AU (1) | AU2014332576B2 (https=) |
| CA (1) | CA2926589C (https=) |
| CL (1) | CL2016000786A1 (https=) |
| ES (1) | ES2732048T3 (https=) |
| NZ (1) | NZ718740A (https=) |
| PT (1) | PT3055280T (https=) |
| RU (1) | RU2672732C2 (https=) |
| SE (1) | SE539579C2 (https=) |
| WO (1) | WO2015053704A1 (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE1850706A1 (en) * | 2018-06-11 | 2019-12-12 | Valmet Oy | A method and a system for obtaining methanol from foul condensate of a pulping process |
| SE542659C2 (en) | 2018-07-10 | 2020-06-23 | Stora Enso Oyj | Method for desulfurization of methanol |
| SE542491C2 (en) * | 2018-07-10 | 2020-05-19 | Stora Enso Oyj | Method for desulfurization of crude sulfate turpentine |
| SE2050074A1 (en) * | 2020-01-28 | 2021-01-29 | Soedra Skogsaegarna Ekonomisk Foerening | Process for producing one, or more, compounds |
| FI130591B (en) | 2020-06-30 | 2023-11-28 | Andritz Oy | Crude methanol purification method |
| CN116194429A (zh) * | 2020-08-06 | 2023-05-30 | 艾尔控股公司 | 用于增强蒸馏过程中的杂质去除的合金和方法 |
| SE544418C2 (en) * | 2020-09-22 | 2022-05-17 | Mill Solution And Tech Ab | Method for separation of reduced nitrogen and reduced sulphur from a feed of foul methanol vapor |
| FI20246130A1 (en) * | 2024-09-17 | 2026-03-18 | Andritz Oy | Method for processing crude methanol |
| FI20246131A1 (en) * | 2024-09-17 | 2026-03-18 | Andritz Oy | Process for removing sulfur from crude methanol |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI52710C (fi) | 1976-04-22 | 1977-11-10 | Kemi Oy | Menetelmä sulfaattiprosessin lauhteista erotetun metanolin puhdistamis eksi. |
| JPS63135342A (ja) * | 1986-11-28 | 1988-06-07 | Jgc Corp | エタノ−ル又はメタノ−ル液の精製方法 |
| SE463670B (sv) * | 1988-10-11 | 1991-01-07 | Eka Nobel Ab | Foerfarande foer framstaellning av klordioxid |
| GB8927266D0 (en) | 1989-12-01 | 1990-01-31 | Csir | Production of methanol |
| US5138101A (en) * | 1991-07-19 | 1992-08-11 | Eastman Kodak Company | Recovery of high-boiling aldehydes from rhodium-catalyzed hydroformylation processes |
| US5450892A (en) | 1993-03-29 | 1995-09-19 | Alliedsignal Inc. | Alkaline scrubber for condensate stripper off-gases |
| US5718810A (en) * | 1996-03-19 | 1998-02-17 | The Dow Chemical Company | Methanol recovery using extractive distillation |
| JP2001181265A (ja) * | 1999-12-22 | 2001-07-03 | Wako Pure Chem Ind Ltd | メルカプトテトラゾール化合物の製造方法 |
| JP3720713B2 (ja) * | 2000-02-22 | 2005-11-30 | 三菱レイヨン株式会社 | ２−（メタ）アクリロイルオキシメチル−２−メチルビシクロ［２．２．１］ヘプタン、その製造方法、その原料アルコールの精製方法、その原料アルデヒドの製造方法、および、その（共）重合体 |
| EP1490457B1 (en) * | 2002-04-01 | 2007-06-13 | E.I. du Pont de Nemours and Company | Preparation of levulinic acid esters and formic acid esters from biomass and olefins |
| JP2005089347A (ja) * | 2003-09-16 | 2005-04-07 | Mitsubishi Heavy Ind Ltd | アルコールと水の分離方法及びその装置 |
| FI20085400A0 (fi) | 2007-11-09 | 2008-04-30 | Upm Kymmene Oyj | Menetelmä jäteveden integroidulle käsittelylle |
| SE531478C2 (sv) | 2007-11-26 | 2009-04-21 | Processum Biorefinery Initiative Ab | Förfarande för utvinning av ammoniumsalt och metanol ur vätska emanerande från orent kondensat, som uppstår vid cellulosamassaframställning |
| MX2011008516A (es) | 2009-02-12 | 2011-10-11 | A H Lundberg Systems Ltd | Metodo y aparato para purificacion de metanol. |
| FI127304B (fi) * | 2011-02-03 | 2018-03-15 | Stora Enso Oyj | Menetelmä puhdistetun metanolin valmistamiseksi sulfaattisellukeiton lauhteesta |
| US8721995B2 (en) | 2011-11-03 | 2014-05-13 | Fluor Technologies Corporation | Conversion of organosulfur compounds to hydrogen sulfide in mixed alcohol synthesis reactor effluent |
| CN202398144U (zh) * | 2011-12-28 | 2012-08-29 | 惠生（南京）清洁能源股份有限公司 | 一种甲醇预精馏塔二级水冷产物的分离装置 |
| US20130172633A1 (en) * | 2011-12-29 | 2013-07-04 | Celanese International Corporation | Process For Producing Ethanol From Impure Methanol |
| EP3010877B1 (en) | 2013-06-19 | 2019-12-18 | FPInnovations | Method for producing bio-methanol at pulp mills |
-
2014
- 2014-10-13 PT PT14852668T patent/PT3055280T/pt unknown
- 2014-10-13 AU AU2014332576A patent/AU2014332576B2/en active Active
- 2014-10-13 SE SE1650632A patent/SE539579C2/en unknown
- 2014-10-13 US US15/027,967 patent/US10160706B2/en active Active
- 2014-10-13 ES ES14852668T patent/ES2732048T3/es active Active
- 2014-10-13 CA CA2926589A patent/CA2926589C/en active Active
- 2014-10-13 JP JP2016521949A patent/JP6577462B2/ja active Active
- 2014-10-13 NZ NZ718740A patent/NZ718740A/en unknown
- 2014-10-13 RU RU2016112932A patent/RU2672732C2/ru active
- 2014-10-13 EP EP14852668.4A patent/EP3055280B1/en active Active
- 2014-10-13 WO PCT/SE2014/051205 patent/WO2015053704A1/en not_active Ceased
- 2014-10-13 CN CN201480066761.5A patent/CN105793220B/zh active Active
-
2016
- 2016-04-05 CL CL2016000786A patent/CL2016000786A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US10160706B2 (en) | 2018-12-25 |
| RU2016112932A (ru) | 2017-11-16 |
| EP3055280A1 (en) | 2016-08-17 |
| CA2926589A1 (en) | 2015-04-16 |
| CN105793220B (zh) | 2018-10-09 |
| WO2015053704A1 (en) | 2015-04-16 |
| RU2016112932A3 (https=) | 2018-06-07 |
| RU2672732C2 (ru) | 2018-11-19 |
| US20160237011A1 (en) | 2016-08-18 |
| EP3055280A4 (en) | 2017-06-14 |
| ES2732048T3 (es) | 2019-11-20 |
| AU2014332576A1 (en) | 2016-04-28 |
| JP2016536290A (ja) | 2016-11-24 |
| CL2016000786A1 (es) | 2016-10-21 |
| PT3055280T (pt) | 2019-06-28 |
| CA2926589C (en) | 2022-08-02 |
| SE1650632A1 (en) | 2016-05-11 |
| NZ718740A (en) | 2019-02-22 |
| SE539579C2 (en) | 2017-10-17 |
| EP3055280B1 (en) | 2019-04-17 |
| CN105793220A (zh) | 2016-07-20 |
| AU2014332576B2 (en) | 2018-02-22 |
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