JP6547088B1 - 前処理剤、前処理方法、化成皮膜を有する金属材料及びその製造方法、並びに塗装金属材料及びその製造方法 - Google Patents
前処理剤、前処理方法、化成皮膜を有する金属材料及びその製造方法、並びに塗装金属材料及びその製造方法 Download PDFInfo
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- JP6547088B1 JP6547088B1 JP2019512841A JP2019512841A JP6547088B1 JP 6547088 B1 JP6547088 B1 JP 6547088B1 JP 2019512841 A JP2019512841 A JP 2019512841A JP 2019512841 A JP2019512841 A JP 2019512841A JP 6547088 B1 JP6547088 B1 JP 6547088B1
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- metal material
- chemical conversion
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- coating
- conversion film
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 119
- 239000000126 substance Substances 0.000 title claims abstract description 106
- 239000007769 metal material Substances 0.000 title claims abstract description 104
- 238000000576 coating method Methods 0.000 title claims abstract description 82
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 80
- 239000011248 coating agent Substances 0.000 title claims abstract description 67
- 238000002203 pretreatment Methods 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 14
- -1 PRETREATMENT METHOD Substances 0.000 title description 3
- 238000011282 treatment Methods 0.000 claims abstract description 73
- 229920000642 polymer Polymers 0.000 claims abstract description 51
- 238000000034 method Methods 0.000 claims abstract description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- 239000000203 mixture Substances 0.000 claims abstract description 6
- 239000003973 paint Substances 0.000 claims description 43
- 150000007524 organic acids Chemical class 0.000 claims description 18
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 6
- 125000004170 methylsulfonyl group Chemical group [H]C([H])([H])S(*)(=O)=O 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 3
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- 238000004070 electrodeposition Methods 0.000 description 27
- 238000001035 drying Methods 0.000 description 19
- 238000012360 testing method Methods 0.000 description 18
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 15
- 238000005238 degreasing Methods 0.000 description 13
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 11
- 125000002091 cationic group Chemical group 0.000 description 11
- 238000011156 evaluation Methods 0.000 description 11
- 229910052735 hafnium Inorganic materials 0.000 description 11
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 description 11
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- 239000002184 metal Substances 0.000 description 11
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- 239000010936 titanium Substances 0.000 description 11
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- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 description 10
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 229910000398 iron phosphate Inorganic materials 0.000 description 8
- WBJZTOZJJYAKHQ-UHFFFAOYSA-K iron(3+) phosphate Chemical compound [Fe+3].[O-]P([O-])([O-])=O WBJZTOZJJYAKHQ-UHFFFAOYSA-K 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 7
- VVJKKWFAADXIJK-UHFFFAOYSA-N Allylamine Chemical compound NCC=C VVJKKWFAADXIJK-UHFFFAOYSA-N 0.000 description 6
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- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
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- UYMKPFRHYYNDTL-UHFFFAOYSA-N ethenamine Chemical compound NC=C UYMKPFRHYYNDTL-UHFFFAOYSA-N 0.000 description 3
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- DYUWTXWIYMHBQS-UHFFFAOYSA-N n-prop-2-enylprop-2-en-1-amine Chemical compound C=CCNCC=C DYUWTXWIYMHBQS-UHFFFAOYSA-N 0.000 description 3
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- 229910001209 Low-carbon steel Inorganic materials 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
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- XIOUDVJTOYVRTB-UHFFFAOYSA-N 1-(1-adamantyl)-3-aminothiourea Chemical compound C1C(C2)CC3CC2CC1(NC(=S)NN)C3 XIOUDVJTOYVRTB-UHFFFAOYSA-N 0.000 description 1
- XNDZQQSKSQTQQD-UHFFFAOYSA-N 3-methylcyclohex-2-en-1-ol Chemical compound CC1=CC(O)CCC1 XNDZQQSKSQTQQD-UHFFFAOYSA-N 0.000 description 1
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
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- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
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- 239000004793 Polystyrene Substances 0.000 description 1
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
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- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 239000010960 cold rolled steel Substances 0.000 description 1
- 238000004440 column chromatography Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 239000013527 degreasing agent Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
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- 239000012153 distilled water Substances 0.000 description 1
- 238000001227 electron beam curing Methods 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 1
- 229920000578 graft copolymer Polymers 0.000 description 1
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- 239000004615 ingredient Substances 0.000 description 1
- JSUQJUFJRAKSKG-UHFFFAOYSA-N iron(3+);nonahydrate Chemical compound O.O.O.O.O.O.O.O.O.[Fe+3] JSUQJUFJRAKSKG-UHFFFAOYSA-N 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- ALTWGIIQPLQAAM-UHFFFAOYSA-N metavanadate Chemical compound [O-][V](=O)=O ALTWGIIQPLQAAM-UHFFFAOYSA-N 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 229940074355 nitric acid Drugs 0.000 description 1
- YOYLLRBMGQRFTN-SMCOLXIQSA-N norbuprenorphine Chemical compound C([C@@H](NCC1)[C@]23CC[C@]4([C@H](C3)C(C)(O)C(C)(C)C)OC)C3=CC=C(O)C5=C3[C@@]21[C@H]4O5 YOYLLRBMGQRFTN-SMCOLXIQSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
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- 239000005011 phenolic resin Substances 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 238000007746 phosphate conversion coating Methods 0.000 description 1
- 229940085991 phosphate ion Drugs 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229920001228 polyisocyanate Polymers 0.000 description 1
- 239000005056 polyisocyanate Substances 0.000 description 1
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- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
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- 235000019260 propionic acid Nutrition 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
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- 239000010935 stainless steel Substances 0.000 description 1
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- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 229920002554 vinyl polymer Polymers 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/78—Pretreatment of the material to be coated
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Treatment Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2017/039461 WO2019087320A1 (fr) | 2017-10-31 | 2017-10-31 | Agent de prétraitement, procédé de prétraitement, matériau métallique ayant un film de conversion chimique et son procédé de fabrication, et matériau métallique peint et son procédé de fabrication |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP6547088B1 true JP6547088B1 (ja) | 2019-07-17 |
| JPWO2019087320A1 JPWO2019087320A1 (ja) | 2019-11-14 |
Family
ID=66331571
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2019512841A Active JP6547088B1 (ja) | 2017-10-31 | 2017-10-31 | 前処理剤、前処理方法、化成皮膜を有する金属材料及びその製造方法、並びに塗装金属材料及びその製造方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP6547088B1 (fr) |
| TW (1) | TWI776980B (fr) |
| WO (1) | WO2019087320A1 (fr) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004218075A (ja) * | 2002-12-24 | 2004-08-05 | Nippon Paint Co Ltd | 化成処理剤及び表面処理金属 |
| WO2007013626A1 (fr) * | 2005-07-29 | 2007-02-01 | Nippon Paint Co., Ltd. | Produits de traitement de surface et procédé de traitement de surface |
| JP2008063612A (ja) * | 2006-09-06 | 2008-03-21 | Nippon Paint Co Ltd | 表面調整用組成物、表面調整方法及び表面調整処理物 |
| US20140272405A1 (en) * | 2013-03-15 | 2014-09-18 | Ppg Industries Ohio, Inc. | Method for preparing and treating a steel substrate |
| JP2016003347A (ja) * | 2014-06-16 | 2016-01-12 | 関西ペイント株式会社 | 金属表面改質液、金属表面改質方法、塗装方法及び塗装物品 |
-
2017
- 2017-10-31 JP JP2019512841A patent/JP6547088B1/ja active Active
- 2017-10-31 WO PCT/JP2017/039461 patent/WO2019087320A1/fr active Application Filing
-
2018
- 2018-10-25 TW TW107137724A patent/TWI776980B/zh active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004218075A (ja) * | 2002-12-24 | 2004-08-05 | Nippon Paint Co Ltd | 化成処理剤及び表面処理金属 |
| WO2007013626A1 (fr) * | 2005-07-29 | 2007-02-01 | Nippon Paint Co., Ltd. | Produits de traitement de surface et procédé de traitement de surface |
| JP2008063612A (ja) * | 2006-09-06 | 2008-03-21 | Nippon Paint Co Ltd | 表面調整用組成物、表面調整方法及び表面調整処理物 |
| US20140272405A1 (en) * | 2013-03-15 | 2014-09-18 | Ppg Industries Ohio, Inc. | Method for preparing and treating a steel substrate |
| JP2016003347A (ja) * | 2014-06-16 | 2016-01-12 | 関西ペイント株式会社 | 金属表面改質液、金属表面改質方法、塗装方法及び塗装物品 |
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| Publication number | Publication date |
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| JPWO2019087320A1 (ja) | 2019-11-14 |
| TW201922973A (zh) | 2019-06-16 |
| WO2019087320A1 (fr) | 2019-05-09 |
| TWI776980B (zh) | 2022-09-11 |
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