JP6180378B2 - Method for producing tea beverage - Google Patents
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本発明は茶飲料の製造方法に関する。より詳細には、本発明は茶葉の浸出液の加工方法および殺菌方法ならびにこれらの方法による茶飲料の製造方法に関する。 The present invention relates to a method for producing a tea beverage. More particularly, the present invention relates to a processing method and a sterilizing method for tea leaf leachate and a method for producing a tea beverage by these methods.
現在、茶飲料を加工する際の殺菌方法としては、通常加熱殺菌方法が使用されており、今までの茶飲料の製造方法は、通常、高温による殺菌過程が含まれる。 At present, a heat sterilization method is usually used as a sterilization method for processing tea beverages, and conventional tea beverage production methods usually include a high temperature sterilization process.
一方で高温を用いないクチナシグサの殺菌方法として、特許文献1は、クチナシグサを超高圧抽出そして超高圧滅菌し、飲料にする方法を開示している。特許文献1によれば、超高圧抽出は、粉砕機で1mm〜3mmの細粒にし、飲用水と1〜5:100の重量比で15分間浸し、100〜250MPaの圧力で5〜20分間保持した、としている。さらに、濾過して得られた抽出液をアルミ箔、プラスチック複合素材に封入し、水を介して250〜450MPaの圧力で、5〜15分間保持して滅菌した、としている。 On the other hand, as a method for sterilizing gardenia rush without using high temperature, Patent Document 1 discloses a method of extracting gardenia rush by ultra-high pressure extraction and ultra-high pressure sterilization to obtain a beverage. According to Patent Document 1, ultra-high pressure extraction is performed by crushing into 1 to 3 mm fine granules, immersed in drinking water at a weight ratio of 1 to 5: 100 for 15 minutes, and held at a pressure of 100 to 250 MPa for 5 to 20 minutes. It has been done. Furthermore, the extract obtained by filtration is sealed in an aluminum foil and a plastic composite material, and sterilized by being held at a pressure of 250 to 450 MPa through water for 5 to 15 minutes.
従来の茶飲料の製造過程に含まれる高温殺菌過程はお茶の甘味成分を破壊し、その風味に不利な影響を与える。したがって、高温を用いない殺菌方法が切望されている。 The high-temperature sterilization process included in the conventional tea beverage manufacturing process destroys the sweetness component of tea and adversely affects its flavor. Therefore, a sterilization method that does not use high temperature is desired.
そこで本発明は高温を用いることなく、長時間保存した場合であっても良好な風味を保持できる茶飲料の製造方法を提供することを目的とする。 Then, this invention aims at providing the manufacturing method of the tea drink which can hold | maintain favorable flavor, even when it preserve | saves for a long time, without using high temperature.
本発明者らは上記課題を解決すべく鋭意検討を重ねた。その結果、茶浸出液を高圧で処理することにより、上記課題が解決されうることを見出し、本発明を完成するに至った。 The present inventors have intensively studied to solve the above problems. As a result, it has been found that the above problems can be solved by treating the tea infusion liquid at a high pressure, and the present invention has been completed.
すなわち、本発明の一形態によれば、a)茶浸出液を軟性容器に密封する工程;及びb)100〜600MPaの圧力で前記密封した容器を0.1〜10分間加圧する工程;を含む、茶飲料の製造方法が提供される。 That is, according to one aspect of the present invention, the method includes: a) a step of sealing the tea infusion in a soft container; and b) a step of pressurizing the sealed container at a pressure of 100 to 600 MPa for 0.1 to 10 minutes. A method for producing a tea beverage is provided.
得られた製品は、冷蔵や常温で保存でき、そして茶葉固有の風味をよく保存できる利点を有する。 The obtained product has the advantage that it can be stored refrigerated or at room temperature, and the flavor unique to tea leaves can be well preserved.
本発明の一実施形態に係る茶飲料の製造方法は、a)茶浸出液を軟性容器に密封(封入)する工程;およびb)100〜600MPaの圧力で前記密封した容器を0.1〜10分間加圧処理する工程;を含む。 The method for producing a tea beverage according to an embodiment of the present invention includes: a) a step of sealing (sealing) a tea infusion in a soft container; and b) the sealed container at a pressure of 100 to 600 MPa for 0.1 to 10 minutes. Applying a pressure treatment.
本発明は、ある茶葉の浸出液の加工方法、および、殺菌方法を提供する。得られた茶飲料は、冷蔵や常温で長期間保存でき、長期間保存しても良好な風味を保持できる。 The present invention provides a method for processing a tea leaf leachate and a method for sterilization. The obtained tea beverage can be stored for a long time at refrigeration or at room temperature, and can retain a good flavor even if stored for a long time.
また、本発明の一実施形態に係る殺菌方法は、100〜600MPaの圧力で、1〜10分間加圧処理することである。 Moreover, the sterilization method which concerns on one Embodiment of this invention is pressurizing at a pressure of 100-600 MPa for 1-10 minutes.
従来の茶葉の製造方法は、生葉摘採、日干萎凋、室内萎凋、回転発酵、釜炒り、静置、揉捻、玉解き、そして乾燥の工程を含む。他の方法には、乾燥せずに、冷凍による保存を行う場合もある。 A conventional method for producing tea leaves includes the steps of fresh leaf picking, sun-dried wilting, indoor wilting, rotary fermentation, roasting in a pot, standing, twisting, thawing, and drying. In other methods, storage by freezing may be performed without drying.
本発明の一実施形態では、従来の製造工程における未乾燥の半製品茶葉(水分含量30〜50重量%)や乾燥された製品茶葉に水を添加し茶浸出液を得、これを、好ましくは常温で、高圧(>100MPa)処理することにより殺菌する。かかる殺菌方法により得られた製品は、冷蔵や常温で保存でき、そして茶葉固有の風味をよく保存できるメリットを有する。 In one embodiment of the present invention, water is added to undried semi-finished tea leaves (moisture content 30-50% by weight) and dried product tea leaves in a conventional manufacturing process to obtain a tea infusion, preferably at room temperature. Then, it is sterilized by high pressure (> 100 MPa) treatment. The product obtained by such a sterilization method can be stored at refrigeration or at room temperature, and has the merit of preserving the flavor unique to tea leaves.
なお、本明細書において、未乾燥の半製品茶葉とは水分含量30〜50重量%であるものをいう。 In the present specification, undried semi-finished tea leaves are those having a water content of 30 to 50% by weight.
本明細書において、茶葉としては、市販されている茶葉であれば特に制限されないが、例えば、緑茶(煎茶、玉露、茎茶、かぶせ茶、碾茶、抹茶、番茶、ほうじ茶、釜炒り茶等)、龍井茶、鉄観音茶、包種茶、烏龍茶、紅茶、アールグレイ茶、または茉莉花茶を使用することができる。 In the present specification, the tea leaf is not particularly limited as long as it is a commercially available tea leaf. Longjing tea, iron kannon tea, baling tea, oolong tea, black tea, Earl Gray tea, or Yuka tea can be used.
上述のように、茶浸出液は、乾燥した茶葉または未乾燥の半製品茶葉を所定の重量比で抽出溶媒としての水に浸漬させ、抽出されることにより得られる。水は飲用水であれば特に制限されない。 As described above, the tea infusion is obtained by immersing dried tea leaves or undried semi-finished tea leaves in water as an extraction solvent at a predetermined weight ratio and extracting the tea leaves. If water is drinking water, it will not be restrict | limited in particular.
茶葉と水との比率は茶葉の種類や消費者に要求される味感に応じて設定すればよく、特に制限されないが、一例を挙げると、茶浸出液は、乾燥した茶葉または未乾燥の半製品茶葉を重量比(茶葉:水)1:5〜1:200の割合で水に浸漬することにより得られる。より好ましくは、茶葉の浸出液は、乾燥した茶葉または未乾燥の半製品茶葉を重量比(茶葉:水)が1:5〜1:20の割合で水に浸漬することにより得られる。 The ratio of tea leaves to water may be set according to the type of tea leaves and the taste required by consumers, and is not particularly limited, but for example, tea exudates are dried tea leaves or undried semi-finished products It is obtained by immersing tea leaves in water at a weight ratio (tea leaves: water) of 1: 5 to 1: 200. More preferably, the tea leaf leachate is obtained by immersing dried tea leaves or undried semi-finished tea leaves in water at a weight ratio (tea leaves: water) of 1: 5 to 1:20.
一実施形態において、乾燥した茶葉または未乾燥の半製品茶葉を浸漬する水、すなわち、抽出用水の温度は、エネルギーを削減する面から0℃〜50℃が好ましい。抽出用水はエネルギーを削減する面から加熱しないことが好ましい。ただし、浸漬時間を短縮できるために室温(25〜35℃、例えば、25℃)以上の温度を用いてもよく、室温以上50℃以下の温度もまた好ましい。なお、この場合には茶葉を茶飲料から除去する必要がある。 In one embodiment, the temperature of water in which dried tea leaves or undried semi-finished tea leaves are immersed, that is, the temperature of extraction water is preferably 0 ° C. to 50 ° C. from the viewpoint of reducing energy. The extraction water is preferably not heated from the viewpoint of reducing energy. However, since the immersion time can be shortened, a temperature of room temperature (25 to 35 ° C., for example, 25 ° C.) or higher may be used, and a temperature of room temperature or higher and 50 ° C. or lower is also preferable. In this case, it is necessary to remove the tea leaves from the tea beverage.
前記茶葉の浸漬時間、すなわち、抽出時間は、茶葉の種類や消費者に要求される味感に応じて設定すればよく、特に制限されないが、一例を挙げると、0.5〜24時間であることが好ましい。また、上記茶葉の浸漬工程において圧力は特に制限されず、例えば、常圧である。 The immersion time of the tea leaves, that is, the extraction time may be set according to the type of tea leaves and the taste required by the consumer, and is not particularly limited, but an example is 0.5 to 24 hours. It is preferable. Further, the pressure is not particularly limited in the tea leaf dipping step, and is, for example, normal pressure.
また、好ましくは、茶浸出液は、前記茶葉を水に浸漬した後に前記茶葉を固液分離により除去することにより得られる。固液分離の方法は特に制限されないが、例えば、常法にて濾過する方法が挙げられる。 Preferably, the tea infusion is obtained by immersing the tea leaves in water and then removing the tea leaves by solid-liquid separation. The method of solid-liquid separation is not particularly limited, and examples thereof include a method of filtering by a conventional method.
なお、上記固液分離処理をしない場合には、茶浸出液は茶葉を含む。かかる形態もまた好ましい。すなわち、好ましい一実施形態において、茶浸出液は、茶葉を含む。かかる場合には茶葉を軟性容器から除去する必要がなく、浸漬時間が短縮され、比較的小さな工場における製造速度の増大を意味する。 In addition, when not performing the said solid-liquid separation process, tea infusion liquid contains tea leaves. Such a form is also preferred. That is, in one preferred embodiment, the tea infusion contains tea leaves. In such a case, it is not necessary to remove the tea leaves from the flexible container, so that the immersion time is shortened, which means an increase in production speed in a relatively small factory.
ついで、このようにして得た茶浸出液を軟性容器に密封(封入)する(工程a)。 Next, the tea infusion obtained in this way is sealed (enclosed) in a soft container (step a).
本発明の好ましい実施形態において、その軟性容器は、プラスチック複合フィルム、プラスチック袋、およびプラスチック瓶からなる群から選択される。容易に市場で入手できるためである。 In a preferred embodiment of the invention, the flexible container is selected from the group consisting of a plastic composite film, a plastic bag, and a plastic bottle. This is because it can be easily obtained in the market.
その後、前記密封した容器を100〜600MPaの圧力で0.1〜10分間加圧処理する(工程b)。かかる処理により、お茶の甘味成分を保持しつつ殺菌処理がなされ、長時間保存が可能な茶飲料が得られる。圧力が600MPaを超える場合にはエネルギーのコストおよび圧力設備のコストの面から好ましくない。圧力が100MPa未満であると殺菌処理に必要な時間が長くなりすぎて実用的ではない。圧力処理の時間が10分を超えると同圧力で維持した場合エネルギーコストが増大するため好ましくない。圧力処理の時間が0.1分未満である場合、圧力の値が600MPa以下であると細菌の殺菌効果が不十分である。より好ましくは、工程b)において加圧処理を300〜600MPaで0.1〜5分間行うことである。 Thereafter, the sealed container is pressurized at a pressure of 100 to 600 MPa for 0.1 to 10 minutes (step b). By this treatment, a tea beverage that is sterilized while retaining the sweetening component of tea and can be stored for a long time is obtained. When the pressure exceeds 600 MPa, it is not preferable from the viewpoint of the cost of energy and the cost of pressure equipment. Pressure is not practical time becomes too long required sterilization process is less than 100 M Pa. If the pressure treatment time exceeds 10 minutes, the energy cost increases when the pressure is maintained at the same pressure, which is not preferable. When the pressure treatment time is less than 0.1 minutes, the sterilizing effect of bacteria is insufficient when the pressure value is 600 MPa or less. More preferably, in step b), the pressure treatment is performed at 300 to 600 MPa for 0.1 to 5 minutes.
また、工程b)において加圧処理を0〜50℃の温度で行うことが好ましい。 Moreover, it is preferable to perform a pressurizing process in the temperature of 0-50 degreeC in process b).
以下、本発明による効果を、実施例および比較例を用いて説明するが、本発明の技術的範囲はこれらの実施例に限定されない。なお、本明細書において、常温とは冷却や加熱を行わない状態の温度であって、室温(25〜35℃)を意味する。 Hereinafter, although the effect by this invention is demonstrated using an Example and a comparative example, the technical scope of this invention is not limited to these Examples. In addition, in this specification, normal temperature is the temperature in the state which does not perform cooling and heating, Comprising: Room temperature (25-35 degreeC) is meant.
以下の実施例は、下記の材料と方法を採用する:
1.1実験材料
1.1.1乾燥された茶葉(種類:烏龍茶)または未乾燥の半製品茶葉(種類:烏龍茶;水分含量約40重量%);及び
1.1.2常温飲料水。
The following examples employ the following materials and methods:
1.1 Experimental Materials 1.1.1 Dried tea leaves (type: oolong tea) or undried semi-finished tea leaves (type: oolong tea; moisture content about 40% by weight); and 1.1.2 cold drinking water.
1.2実験方法
1.2.1高圧設備
高圧設備(QFP2L−700、Avure Technologies社製、スウェーデン)を用い、媒質の水に圧力をかける。包装は、ポリエチレンテレフタレート(PET)で作られたプラスチック袋である。すなわち、茶浸出液を封入した密封プラスチック袋を加圧処理する。
1.2 Experimental Method 1.2.1 High Pressure Equipment Using a high pressure equipment (QFP2L-700, manufactured by Avure Technologies, Sweden), pressure is applied to the medium water. The package is a plastic bag made of polyethylene terephthalate (PET). That is, the sealed plastic bag in which the tea infusion liquid is sealed is pressurized.
1.2.2生菌数測定
1mlのよく混合した標品を取り、異なった割合に希釈した。希釈液1mlを好気性生菌数測定プレート(aerobic plate count,3M Petrifilm plate,St.Paul,Minnesota,USA)に移し、35℃で48時間培養した後、紅色のコロニーを計数した。希釈液ごとに二回測定をした。
1.2.2 Viable count 1 ml of well mixed preparation was taken and diluted to different proportions. 1 ml of the diluted solution was transferred to an aerobic plate count plate (aerobic plate count, 3M Petrifilm plate, St. Paul, Minnesota, USA) and cultured at 35 ° C. for 48 hours, and then red colonies were counted. Two measurements were taken for each dilution.
1.2.3カビ酵母菌数
1mlのよく混合した標品を取り、異なった割合で標品を希釈した。希釈液1mlを酵母およびカビ測定プレート(yeast and mold count plate,3M Petrifilm plate,St.Paul,Minnesota,USA)に移し、25℃で3〜5日培養した後、コロニーを計数した。希釈液ごとに二回測定をした。
1.2.3 Number of mold yeast 1 ml of a well mixed sample was taken and diluted in different proportions. 1 ml of the diluted solution was transferred to a yeast and mold measurement plate (yeast and mold count plate, 3M Petrifilm plate, St. Paul, Minnesota, USA) and cultured at 25 ° C. for 3 to 5 days, and colonies were counted. Two measurements were taken for each dilution.
[実施例1:茶葉含有の浸出液に対する高圧殺菌の有効性]
未乾燥の半製品茶葉1gを取り、常圧下、10g、20gまたは200gの水(室温)を添加した後、さらに、リステリア イノキュア(Listeria innocua;L.innocua)またはアスペルギルス ニガー(Aspergillus niger;A.niger)菌液を追加した。一部の試験は、菌液を添加しなかった。こうして得た茶浸出液を軟性容器としてのプラスチック袋に密封し、室温において100MPa〜600MPaの圧力を掛け、0.1〜10分間保持した。生菌数とカビ酵母菌数を測定した結果を、表1のように対数で表す。100〜600MPaで0.1〜5分間の加圧処理は、細菌、カビ酵母菌の数の対数値を2.5から5.8まで減らすことができた。
[Example 1: Effectiveness of high-pressure sterilization for tea leaf-containing leachate]
After taking 1 g of undried semi-finished tea leaves and adding 10 g, 20 g or 200 g of water (room temperature) under normal pressure, further, Listeria innocua or L. innocua or Aspergillus niger; A. niger ) Added bacterial solution. Some tests did not add bacterial solution. The tea infusion thus obtained was sealed in a plastic bag as a flexible container, and a pressure of 100 MPa to 600 MPa was applied at room temperature and held for 0.1 to 10 minutes. The results of measuring the number of viable cells and the number of mold yeasts are represented by logarithms as shown in Table 1. The pressure treatment at 100 to 600 MPa for 0.1 to 5 minutes was able to reduce the logarithmic value of the number of bacteria and mold yeast from 2.5 to 5.8.
[実施例2:茶葉抜きの浸出液に対する高圧殺菌の有効性]
未乾燥の半製品茶葉1gに10gまたは30gの水(室温)を添加し、1時間後、茶葉を濾過で除き、浸出液にL.innocuaやA.niger菌液を添加し(常圧)、プラスチック袋中に封入し密封して室温で300MPaで3分間または5分間加圧した。生菌数とカビ酵母菌数を分析した結果を表2に示す。これらは本発明は有効的に細菌、カビそして酵母菌を殺菌したことを示す。
[Example 2: Effectiveness of high-pressure sterilization for tea leaves exudate]
10 g or 30 g of water (room temperature) was added to 1 g of undried semi-finished tea leaves, and after 1 hour, the tea leaves were removed by filtration. innocua and A.I. Niger bacteria solution was added (normal pressure), sealed in a plastic bag, sealed, and pressurized at 300 MPa at room temperature for 3 or 5 minutes. Table 2 shows the results of analyzing the viable cell count and the mold yeast cell count. These show that the present invention effectively killed bacteria, mold and yeast.
[実施例3:高圧殺菌した茶葉浸出液の長期間保存性]
乾燥された茶葉または未乾燥の半製品茶葉1gに5〜20gの水(室温)を常圧下で添加し、0.1mlの枯草菌(Bacillus subtilis)胞子やL.innocua菌液を接種した。それをプラスチック袋中に密封してから室温で600MPaで3分間または10分間加圧した。得られたものは、4〜10℃の冷蔵や室温で30日間保存でき、最高70日間も保存できた。結果は、表3に示した通り、冷蔵や室温で30日間保存できた。
[Example 3: Long-term preservation of tea leaf exudate sterilized under high pressure]
5 to 20 g of water (room temperature) is added to 1 g of dried tea leaves or undried semi-finished tea leaves under normal pressure, and 0.1 ml of Bacillus subtilis spores or L. innocua solution was inoculated. It was sealed in a plastic bag and then pressurized at 600 MPa for 3 minutes or 10 minutes at room temperature. The obtained product could be stored at 4-10 ° C. refrigeration or at room temperature for 30 days, and could be stored for up to 70 days. As shown in Table 3, the results were refrigerated or stored at room temperature for 30 days.
[実施例4:高圧殺菌後の茶浸出液の風味評価]
未乾燥の半製品茶葉1重量部に7.5重量部の水を添加した(室温)。また、未乾燥の半製品茶葉1重量部に20重量部の水を別途添加した(室温)。これらをそれぞれプラスチック袋中に密封し(常圧)、当該プラスチック袋を600MPa、室温(25〜35℃)で3分間加圧した。4〜10℃で100日間保存した後に、浸出液を取りだし、適量の水で0.6〜0.7のブリックス度まで希釈した。希釈した浸出液は、強烈な香りと後口の甘味を有し、渋みが弱くて、茶色が薄かった。それと比べ、茶葉に添加した水の温度を85℃とした以外は上記と同様に加圧処理した浸出液を適量の水で0.7のブリックス度まで希釈したら、渋みと茶色はかなり強くて濃い色であった。
[Example 4: Evaluation of flavor of tea infusion after autoclaving]
7.5 parts by weight of water was added to 1 part by weight of undried semi-finished tea leaves (room temperature). Further, 20 parts by weight of water was separately added to 1 part by weight of undried semi-finished tea leaves (room temperature). These were each sealed in a plastic bag (normal pressure), and the plastic bag was pressurized at 600 MPa and room temperature (25 to 35 ° C.) for 3 minutes. After storage at 4-10 ° C. for 100 days, the leachate was taken out and diluted with a suitable amount of water to a Brix degree of 0.6-0.7. The diluted leachate had a strong aroma and sweetness in the back, astringency was weak, and the brown color was light. In contrast, when the leachate that was pressure-treated in the same way as above except that the temperature of the water added to the tea leaves was 85 ° C. was diluted with a suitable amount of water to a Brix degree of 0.7, the astringency and brown were fairly strong and dark colors Met.
乾燥した茶葉1重量部に10重量部の水(室温)を添加し、プラスチック袋中に密封し(常圧)、当該プラスチック袋を450MPa、室温(25〜35℃)で1分間加圧した。4〜10℃で32日間保存した後に、浸出液を取り出し、適量の水で0.6〜0.7のブリックス度まで希釈した。希釈した浸出液は、渋みが弱くて、香りと後口の甘味を有し、茶色がわりと薄かった。それと比べ、茶葉に添加した水の温度を95℃とした以外は上記と同様に加圧処理した浸出液を適量の水で0.7のブリックス度まで希釈したら、渋みと茶色はかなり強くて濃い色であった。 10 parts by weight of water (room temperature) was added to 1 part by weight of the dried tea leaves, sealed in a plastic bag (normal pressure), and the plastic bag was pressurized at 450 MPa at room temperature (25-35 ° C.) for 1 minute. After storage at 4-10 ° C. for 32 days, the leachate was removed and diluted with an appropriate amount of water to a Brix degree of 0.6-0.7. The diluted leachate had a mild astringency, had a fragrance and a sweetness on the back, and was rather light brown. Compared with that, except that the temperature of the water added to the tea leaves was 95 ° C, the exudate that had been pressure-treated in the same manner as above was diluted with an appropriate amount of water to a Brix degree of 0.7. Met.
Claims (9)
b)100〜600MPaの圧力で前記密封した容器を0〜35℃の温度で0.1〜10分間加圧処理する工程;
を含む、茶飲料の製造方法。 a) sealing a tea infusion obtained by immersing dried tea leaves or undried semi-finished tea leaves in water in a weight ratio (tea leaves: water) of 1: 5 to 1:30 in a soft container; and b) Pressurizing the sealed container at a temperature of 0 to 35 ° C. for 0.1 to 10 minutes at a pressure of 100 to 600 MPa;
A method for producing a tea beverage, comprising:
b)100〜600MPaの圧力で前記密封した容器を0〜35℃の温度で0.1〜10分間加圧処理する工程;
を含む、茶飲料の製造方法。 a) A tea infusion containing tea leaves obtained by immersing dried tea leaves or undried semi-finished tea leaves in water at a weight ratio (tea leaves: water) of 1: 5 to 1:30 is sealed in a soft container. And b) pressure-treating the sealed container at a temperature of 0 to 35 ° C. for 0.1 to 10 minutes at a pressure of 100 to 600 MPa;
A method for producing a tea beverage, comprising:
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