JP6144174B2 - Cleaning composition - Google Patents
Cleaning composition Download PDFInfo
- Publication number
- JP6144174B2 JP6144174B2 JP2013210838A JP2013210838A JP6144174B2 JP 6144174 B2 JP6144174 B2 JP 6144174B2 JP 2013210838 A JP2013210838 A JP 2013210838A JP 2013210838 A JP2013210838 A JP 2013210838A JP 6144174 B2 JP6144174 B2 JP 6144174B2
- Authority
- JP
- Japan
- Prior art keywords
- extract
- fatty acid
- cleaning composition
- sodium
- oil fatty
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000203 mixture Substances 0.000 title claims description 54
- 238000004140 cleaning Methods 0.000 title claims description 36
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 69
- 239000000194 fatty acid Substances 0.000 claims description 69
- 229930195729 fatty acid Natural products 0.000 claims description 69
- 150000004665 fatty acids Chemical group 0.000 claims description 57
- -1 fatty acid salt Chemical class 0.000 claims description 31
- 150000003839 salts Chemical class 0.000 claims description 15
- 125000004432 carbon atom Chemical group C* 0.000 claims description 7
- 229920006317 cationic polymer Polymers 0.000 claims description 7
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- 150000001413 amino acids Chemical class 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 125000000217 alkyl group Chemical group 0.000 claims description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 3
- 229930195712 glutamate Natural products 0.000 claims description 2
- 239000001103 potassium chloride Substances 0.000 claims description 2
- 235000011164 potassium chloride Nutrition 0.000 claims description 2
- 239000000284 extract Substances 0.000 description 79
- 239000006260 foam Substances 0.000 description 19
- 239000003240 coconut oil Substances 0.000 description 18
- 235000019864 coconut oil Nutrition 0.000 description 18
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 13
- 238000005187 foaming Methods 0.000 description 13
- 239000011734 sodium Substances 0.000 description 13
- 229910052708 sodium Inorganic materials 0.000 description 13
- 238000005406 washing Methods 0.000 description 13
- 235000019482 Palm oil Nutrition 0.000 description 11
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 11
- 239000002540 palm oil Substances 0.000 description 11
- 229910052700 potassium Inorganic materials 0.000 description 11
- 239000011591 potassium Substances 0.000 description 11
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 10
- 229940024606 amino acid Drugs 0.000 description 10
- 235000001014 amino acid Nutrition 0.000 description 10
- KWIUHFFTVRNATP-UHFFFAOYSA-N glycine betaine Chemical compound C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 10
- 239000000843 powder Substances 0.000 description 10
- 229960004418 trolamine Drugs 0.000 description 10
- 239000002253 acid Substances 0.000 description 7
- 239000003795 chemical substances by application Substances 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 239000003599 detergent Substances 0.000 description 7
- 239000003346 palm kernel oil Substances 0.000 description 7
- 235000019865 palm kernel oil Nutrition 0.000 description 7
- 239000000049 pigment Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- AYFVYJQAPQTCCC-UHFFFAOYSA-N Threonine Natural products CC(O)C(N)C(O)=O AYFVYJQAPQTCCC-UHFFFAOYSA-N 0.000 description 6
- 239000004473 Threonine Substances 0.000 description 6
- 239000004359 castor oil Substances 0.000 description 6
- 235000019438 castor oil Nutrition 0.000 description 6
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 6
- 235000013399 edible fruits Nutrition 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 6
- 239000003760 tallow Substances 0.000 description 6
- 241001474374 Blennius Species 0.000 description 5
- AYFVYJQAPQTCCC-GBXIJSLDSA-N L-threonine Chemical compound C[C@@H](O)[C@H](N)C(O)=O AYFVYJQAPQTCCC-GBXIJSLDSA-N 0.000 description 5
- 229960003237 betaine Drugs 0.000 description 5
- GQOKIYDTHHZSCJ-UHFFFAOYSA-M dimethyl-bis(prop-2-enyl)azanium;chloride Chemical compound [Cl-].C=CC[N+](C)(C)CC=C GQOKIYDTHHZSCJ-UHFFFAOYSA-M 0.000 description 5
- 239000004006 olive oil Substances 0.000 description 5
- 235000008390 olive oil Nutrition 0.000 description 5
- 230000008719 thickening Effects 0.000 description 5
- MTCFGRXMJLQNBG-REOHCLBHSA-N (2S)-2-Amino-3-hydroxypropansäure Chemical compound OC[C@H](N)C(O)=O MTCFGRXMJLQNBG-REOHCLBHSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 4
- 239000002202 Polyethylene glycol Substances 0.000 description 4
- 241000220317 Rosa Species 0.000 description 4
- MTCFGRXMJLQNBG-UHFFFAOYSA-N Serine Natural products OCC(N)C(O)=O MTCFGRXMJLQNBG-UHFFFAOYSA-N 0.000 description 4
- 235000015278 beef Nutrition 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 229920001577 copolymer Polymers 0.000 description 4
- 241000411851 herbal medicine Species 0.000 description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- 230000000704 physical effect Effects 0.000 description 4
- 239000000419 plant extract Substances 0.000 description 4
- 229920001223 polyethylene glycol Polymers 0.000 description 4
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 4
- 235000004400 serine Nutrition 0.000 description 4
- 239000000344 soap Substances 0.000 description 4
- 159000000000 sodium salts Chemical class 0.000 description 4
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 4
- 239000002562 thickening agent Substances 0.000 description 4
- JDRSMPFHFNXQRB-CMTNHCDUSA-N Decyl beta-D-threo-hexopyranoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)C(O)[C@H](O)C1O JDRSMPFHFNXQRB-CMTNHCDUSA-N 0.000 description 3
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 3
- 239000005639 Lauric acid Substances 0.000 description 3
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 3
- 235000006040 Prunus persica var persica Nutrition 0.000 description 3
- 244000288377 Saxifraga stolonifera Species 0.000 description 3
- 240000003768 Solanum lycopersicum Species 0.000 description 3
- 235000001484 Trigonella foenum graecum Nutrition 0.000 description 3
- 244000250129 Trigonella foenum graecum Species 0.000 description 3
- 229920006322 acrylamide copolymer Polymers 0.000 description 3
- 239000004480 active ingredient Substances 0.000 description 3
- 125000002252 acyl group Chemical group 0.000 description 3
- 239000002280 amphoteric surfactant Substances 0.000 description 3
- 239000003945 anionic surfactant Substances 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 3
- 235000006708 antioxidants Nutrition 0.000 description 3
- 230000005587 bubbling Effects 0.000 description 3
- 238000007796 conventional method Methods 0.000 description 3
- 229940073499 decyl glucoside Drugs 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- PYIDGJJWBIBVIA-UYTYNIKBSA-N lauryl glucoside Chemical compound CCCCCCCCCCCCO[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O PYIDGJJWBIBVIA-UYTYNIKBSA-N 0.000 description 3
- 229940048848 lauryl glucoside Drugs 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- 229940114930 potassium stearate Drugs 0.000 description 3
- MQOCIYICOGDBSG-UHFFFAOYSA-M potassium;hexadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCC([O-])=O MQOCIYICOGDBSG-UHFFFAOYSA-M 0.000 description 3
- ANBFRLKBEIFNQU-UHFFFAOYSA-M potassium;octadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCCCC([O-])=O ANBFRLKBEIFNQU-UHFFFAOYSA-M 0.000 description 3
- PYJBVGYZXWPIKK-UHFFFAOYSA-M potassium;tetradecanoate Chemical compound [K+].CCCCCCCCCCCCCC([O-])=O PYJBVGYZXWPIKK-UHFFFAOYSA-M 0.000 description 3
- 235000020712 soy bean extract Nutrition 0.000 description 3
- 235000001019 trigonella foenum-graecum Nutrition 0.000 description 3
- 229930003231 vitamin Natural products 0.000 description 3
- 235000013343 vitamin Nutrition 0.000 description 3
- 239000011782 vitamin Substances 0.000 description 3
- 229940088594 vitamin Drugs 0.000 description 3
- YBJHBAHKTGYVGT-ZKWXMUAHSA-N (+)-Biotin Chemical compound N1C(=O)N[C@@H]2[C@H](CCCCC(=O)O)SC[C@@H]21 YBJHBAHKTGYVGT-ZKWXMUAHSA-N 0.000 description 2
- JXQLSFGNCSECAG-WNQIDUERSA-N (2s)-2-aminobutanedioic acid;2-[bis(2-hydroxyethyl)amino]ethanol Chemical compound OC(=O)[C@@H](N)CC(O)=O.OCCN(CCO)CCO JXQLSFGNCSECAG-WNQIDUERSA-N 0.000 description 2
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 description 2
- KAKVFSYQVNHFBS-UHFFFAOYSA-N (5-hydroxycyclopenten-1-yl)-phenylmethanone Chemical compound OC1CCC=C1C(=O)C1=CC=CC=C1 KAKVFSYQVNHFBS-UHFFFAOYSA-N 0.000 description 2
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
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- 235000003261 Artemisia vulgaris Nutrition 0.000 description 2
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
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- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 2
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- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- GKQPCPXONLDCMU-CCEZHUSRSA-N lacidipine Chemical compound CCOC(=O)C1=C(C)NC(C)=C(C(=O)OCC)C1C1=CC=CC=C1\C=C\C(=O)OC(C)(C)C GKQPCPXONLDCMU-CCEZHUSRSA-N 0.000 description 1
- VMPHSYLJUKZBJJ-UHFFFAOYSA-N lauric acid triglyceride Natural products CCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCC)COC(=O)CCCCCCCCCCC VMPHSYLJUKZBJJ-UHFFFAOYSA-N 0.000 description 1
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- 229930013686 lignan Natural products 0.000 description 1
- 235000009408 lignans Nutrition 0.000 description 1
- 150000005692 lignans Chemical class 0.000 description 1
- 239000000711 locust bean gum Substances 0.000 description 1
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- 235000010335 lysozyme Nutrition 0.000 description 1
- 239000004325 lysozyme Substances 0.000 description 1
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- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000001333 moisturizer Effects 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 235000013917 monoammonium glutamate Nutrition 0.000 description 1
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- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 235000010460 mustard Nutrition 0.000 description 1
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- VVGIYYKRAMHVLU-UHFFFAOYSA-N newbouldiamide Natural products CCCCCCCCCCCCCCCCCCCC(O)C(O)C(O)C(CO)NC(=O)CCCCCCCCCCCCCCCCC VVGIYYKRAMHVLU-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- ZHALDANPYXAMJF-UHFFFAOYSA-N octadecanoate;tris(2-hydroxyethyl)azanium Chemical compound OCC[NH+](CCO)CCO.CCCCCCCCCCCCCCCCCC([O-])=O ZHALDANPYXAMJF-UHFFFAOYSA-N 0.000 description 1
- 239000008041 oiling agent Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000020333 oolong tea Nutrition 0.000 description 1
- 229940116257 pepper extract Drugs 0.000 description 1
- 235000020737 peppermint extract Nutrition 0.000 description 1
- 229940067631 phospholipid Drugs 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002643 polyglutamic acid Polymers 0.000 description 1
- 229920002503 polyoxyethylene-polyoxypropylene Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 229940068988 potassium aspartate Drugs 0.000 description 1
- 229940096992 potassium oleate Drugs 0.000 description 1
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- MLICVSDCCDDWMD-KVVVOXFISA-M potassium;(z)-octadec-9-enoate Chemical compound [K+].CCCCCCCC\C=C/CCCCCCCC([O-])=O MLICVSDCCDDWMD-KVVVOXFISA-M 0.000 description 1
- NGNZTXNWCGRXKL-UHFFFAOYSA-M potassium;16-methylheptadecanoate Chemical compound [K+].CC(C)CCCCCCCCCCCCCCC([O-])=O NGNZTXNWCGRXKL-UHFFFAOYSA-M 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 229940069949 propolis Drugs 0.000 description 1
- 239000011814 protection agent Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229960003471 retinol Drugs 0.000 description 1
- 235000020944 retinol Nutrition 0.000 description 1
- 239000011607 retinol Substances 0.000 description 1
- 150000004609 retinol derivatives Chemical class 0.000 description 1
- 229940092258 rosemary extract Drugs 0.000 description 1
- 235000020748 rosemary extract Nutrition 0.000 description 1
- 239000001233 rosmarinus officinalis l. extract Substances 0.000 description 1
- 229940109850 royal jelly Drugs 0.000 description 1
- 229940112950 sage extract Drugs 0.000 description 1
- 235000020752 sage extract Nutrition 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 235000017709 saponins Nutrition 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 125000005471 saturated fatty acid group Chemical group 0.000 description 1
- 239000013535 sea water Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000003352 sequestering agent Substances 0.000 description 1
- UQDJGEHQDNVPGU-UHFFFAOYSA-N serine phosphoethanolamine Chemical compound [NH3+]CCOP([O-])(=O)OCC([NH3+])C([O-])=O UQDJGEHQDNVPGU-UHFFFAOYSA-N 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- 229910021647 smectite Inorganic materials 0.000 description 1
- BTURAGWYSMTVOW-UHFFFAOYSA-M sodium dodecanoate Chemical compound [Na+].CCCCCCCCCCCC([O-])=O BTURAGWYSMTVOW-UHFFFAOYSA-M 0.000 description 1
- 229940073490 sodium glutamate Drugs 0.000 description 1
- 239000001540 sodium lactate Substances 0.000 description 1
- 229940005581 sodium lactate Drugs 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
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- 229940045845 sodium myristate Drugs 0.000 description 1
- RYYKJJJTJZKILX-UHFFFAOYSA-M sodium octadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCCCC([O-])=O RYYKJJJTJZKILX-UHFFFAOYSA-M 0.000 description 1
- 229940045870 sodium palmitate Drugs 0.000 description 1
- 229940045920 sodium pyrrolidone carboxylate Drugs 0.000 description 1
- 229940080350 sodium stearate Drugs 0.000 description 1
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 description 1
- WTWSHHITWMVLBX-DKWTVANSSA-M sodium;(2s)-2-aminobutanedioate;hydron Chemical compound [Na+].[O-]C(=O)[C@@H](N)CC(O)=O WTWSHHITWMVLBX-DKWTVANSSA-M 0.000 description 1
- FRHNXUKHAUWMOQ-UHFFFAOYSA-M sodium;16-methylheptadecanoate Chemical compound [Na+].CC(C)CCCCCCCCCCCCCCC([O-])=O FRHNXUKHAUWMOQ-UHFFFAOYSA-M 0.000 description 1
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- QKJPFZCCZMBRFB-UHFFFAOYSA-M sodium;3-aminopropanoate Chemical compound [Na+].NCCC([O-])=O QKJPFZCCZMBRFB-UHFFFAOYSA-M 0.000 description 1
- GGXKEBACDBNFAF-UHFFFAOYSA-M sodium;hexadecanoate Chemical compound [Na+].CCCCCCCCCCCCCCCC([O-])=O GGXKEBACDBNFAF-UHFFFAOYSA-M 0.000 description 1
- JUQGWKYSEXPRGL-UHFFFAOYSA-M sodium;tetradecanoate Chemical compound [Na+].CCCCCCCCCCCCCC([O-])=O JUQGWKYSEXPRGL-UHFFFAOYSA-M 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000001587 sorbitan monostearate Substances 0.000 description 1
- 235000011076 sorbitan monostearate Nutrition 0.000 description 1
- 229940035048 sorbitan monostearate Drugs 0.000 description 1
- 150000003408 sphingolipids Chemical class 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 210000004233 talus Anatomy 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000000213 tara gum Substances 0.000 description 1
- 235000010491 tara gum Nutrition 0.000 description 1
- 235000013616 tea Nutrition 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 125000000341 threoninyl group Chemical group [H]OC([H])(C([H])([H])[H])C([H])(N([H])[H])C(*)=O 0.000 description 1
- 239000001585 thymus vulgaris Substances 0.000 description 1
- 239000001430 tilia cordata extract Substances 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 229930003799 tocopherol Natural products 0.000 description 1
- 239000011732 tocopherol Substances 0.000 description 1
- 235000019149 tocopherols Nutrition 0.000 description 1
- 108010021724 tonin Proteins 0.000 description 1
- 229960003500 triclosan Drugs 0.000 description 1
- 229940029614 triethanolamine stearate Drugs 0.000 description 1
- 229940045136 urea Drugs 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 150000003712 vitamin E derivatives Chemical class 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
- 239000003357 wound healing promoting agent Substances 0.000 description 1
- 239000012138 yeast extract Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229930007845 β-thujaplicin Natural products 0.000 description 1
- QUEDXNHFTDJVIY-UHFFFAOYSA-N γ-tocopherol Chemical class OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 QUEDXNHFTDJVIY-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Cosmetics (AREA)
Description
本発明は洗浄剤組成物に関し、詳しくは、使用時の泡立ちや泡質(クリーミィ性)、洗い流し時のきしみ感やべたつきない使用感、及び低温安定性に優れ、増粘剤を使用しなくても粘度を有する洗浄剤組成物に関する。 The present invention relates to a detergent composition, and in particular, it is excellent in foaming and foam quality (creamy property) at the time of use, squeaky feeling and non-sticky feeling at the time of washing, and low-temperature stability without using a thickener. Also relates to a detergent composition having a viscosity.
従来、ボディソープや洗顔料といった洗浄剤において、増泡や泡質(クリーミィ性)調整、使用性や安定性に優れた粘度を出すために、アニオン性界面活性剤、両性界面活性剤等の洗浄基剤と組み合わせる物質として、ラウリン酸モノエタノールアミドやヤシ油脂肪酸ジエタノールアミド等の高級脂肪酸アルカノールアミドが広く用いられている(例えば、非特許文献1参照。)。しかしながら、高級脂肪酸ジエタノールアミドを多量に配合した場合には、すすぎ性や仕上がり感に悪影響を及ぼす等の問題があった。また、高級脂肪酸モノエタノールアミド等を用いた場合、低温で結晶が析出する場合があった。 In the past, detergents such as body soaps and facial cleansers used to wash anionic surfactants and amphoteric surfactants in order to produce foam with increased foam, foam quality (creaminess) adjustment, and excellent usability and stability. Higher fatty acid alkanolamides such as lauric acid monoethanolamide and coconut oil fatty acid diethanolamide are widely used as substances to be combined with the base (for example, see Non-Patent Document 1). However, when a higher fatty acid diethanolamide is blended in a large amount, there are problems such as adverse effects on rinsing properties and finished feeling. Further, when higher fatty acid monoethanolamide or the like was used, crystals sometimes precipitated at a low temperature.
このような問題を解決する手段として、高級脂肪酸塩とカチオン化フェヌグリークガムとを組み合わせ、実質的に脂肪酸ジエタノールアミドを含まない皮膚洗浄剤組成物の発明がなされている(例えば、特許文献1参照。)。しかしながら、アルカリ性である高級脂肪酸塩主体の洗浄剤において、カチオン化フェヌグリークガム等のカチオン化高分子のみで増粘効果を期待できるほど配合した場合、経時変化によって異臭を放つようになり、製品として満足できるものではなかった。 As a means for solving such a problem, an invention of a skin cleansing composition which is a combination of a higher fatty acid salt and cationized fenugreek gum and substantially does not contain fatty acid diethanolamide has been made (see, for example, Patent Document 1). ). However, in alkaline detergents mainly composed of higher fatty acid salts, when blended to such an extent that a thickening effect can be expected only with a cationized polymer such as cationized fenugreek gum, a strange odor will be emitted over time, which is satisfactory as a product. It wasn't possible.
上記従来技術を背景とした本発明の目的は、使用時の泡立ちや泡質(クリーミィ性)、洗い流し時のきしみ感やべたつきのない使用感、及び低温安定性に優れ、増粘剤を使用しなくても粘度を有する洗浄剤組成物を提供することにある。 The object of the present invention against the background of the above prior art is excellent in foaming and foam quality (creaminess) at the time of use, squeaky feeling and non-stickiness at the time of washing, and low temperature stability, and using a thickener. An object of the present invention is to provide a cleaning composition having a viscosity even without it.
本発明者等は、本発明の目的を達成するために鋭意研究した結果、高級脂肪酸塩と、特定のN−アシルアミノ酸塩と、陽イオン性高分子と、アルキルポリグルコシドを組み合わせることにより、使用時の泡立ちや泡質(クリーミィ性)、洗い流し時のきしみ感やべたつきのない使用感、及び低温安定性に優れ、増粘剤を使用しなくても粘度を有する洗浄剤組成物が得られることを見出し、本発明を完成した。 As a result of intensive studies to achieve the object of the present invention, the present inventors have used a combination of a higher fatty acid salt, a specific N-acyl amino acid salt, a cationic polymer, and an alkyl polyglucoside. Excellent foaming and foam quality (creaminess), squeaky and non-sticky feel during washing, and low-temperature stability, and a detergent composition with viscosity can be obtained without using a thickener. The present invention has been completed.
すなわち、本発明は、下記成分(A)〜(E)を含有し、且つ配合比(B)/(D)が1〜5.5であり、配合量(B)+(D)が全組成物中の20〜45質量%であることを特徴とする洗浄剤組成物。
(A)アシル基が炭素原子数8〜22の脂肪酸残基と、IOB値が3以上、又はカルボキシル基を2つ有するアミノ酸からなるN−アシルアミノ酸塩から選ばれる一種または二種以上
(B)炭素数8〜22の高級脂肪酸塩 10〜42質量%
(C)陽イオン性高分子
(D)アルキルポリグルコシド 3〜22.5質量%
(E)塩化ナトリウム 0.1〜1.5質量%
That is, the present invention contains the following components (A) to (E), the blending ratio (B) / (D) is 1 to 5.5, and the blending amount (B) + (D) is the total composition. A cleaning composition, characterized in that it is 20 to 45% by mass in the product.
(A) One type or two or more types (B) selected from N-acyl amino acid salts consisting of fatty acid residues having 8 to 22 carbon atoms and an IOB value of 3 or more, or an amino acid having two carboxyl groups 10 to 42% by mass of higher fatty acid salt having 8 to 22 carbon atoms
(C) Cationic polymer (D) Alkyl polyglucoside 3 to 22.5% by mass
(E) Sodium chloride 0.1-1.5 mass%
本発明におけるIOB値とは、Inorganic/Organic Balance(無機性/有機性 比)の略であって、化合物の有機値に対する化合物の無機値の比に対応する値であり、有機化合物の極性の度合いを示す指標である。具体的には、IOB値=無機性値/有機性値として表される。 The IOB value in the present invention is an abbreviation of Inorganic / Organic Balance (inorganic / organic ratio), and corresponds to the ratio of the inorganic value of the compound to the organic value of the compound, and the degree of polarity of the organic compound It is an index showing. Specifically, it is expressed as IOB value = inorganic value / organic value.
ここで、「無機性値」、「有機性値」のそれぞれについては、例えば、分子中の炭素原子1個について「有機性値」が20、同水酸基1個について「無機性値」が100といったように、各種原子又は官能基に応じた「無機性値」、「有機性値」が設定されており、有機化合物中の全ての原子及び官能基の「無機性値」、「有機性値」を積算することによって、当該有機化合物のIOB値が算出される(例えば、甲田善生 著、「有機概念図―基礎と応用―」11頁〜17頁、三共出版 1984年発行 参照)。 Here, for each of the “inorganic value” and “organic value”, for example, “organic value” is 20 for one carbon atom in the molecule, and “inorganic value” is 100 for one hydroxyl group. As described above, “inorganic value” and “organic value” corresponding to various atoms or functional groups are set, and “inorganic value” and “organic value” of all atoms and functional groups in the organic compound. Is integrated to calculate the IOB value of the organic compound (see, for example, Yoshio Koda, “Organic Conceptual Diagram—Basics and Applications”, pages 11-17, published by Sankyo Publishing, 1984).
本発明によれば、使用時の泡立ちや泡質(クリーミィ性)、洗い流し時のきしみ感やべたつきのない使用感、及び低温安定性に優れ、増粘剤を使用しなくても粘度を有する洗浄剤組成物を提供することができる。 According to the present invention, it is excellent in foaming and foam quality (creamy property) at the time of use, squeaky feeling and non-stickiness at the time of washing, and low temperature stability, and has a viscosity without using a thickener. An agent composition can be provided.
以下、本発明の洗浄剤組成物について詳細に説明する。 Hereinafter, the cleaning composition of the present invention will be described in detail.
本発明の洗浄剤組成物で用いられる成分(A)はアシル基が炭素原子数8〜22の脂肪酸残基と、IOB値が3以上、又はカルボキシル基を2つ有するアミノ酸からなるN−アシルアミノ酸塩である。炭素原子数8〜22の脂肪酸残基としては、例えばラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸、イソステアリン酸、オレイン酸などの単一のアシル基や、ヤシ油脂肪酸、牛脂脂肪酸、ヒマシ油脂肪酸、オリーブ油脂肪酸、パーム油脂肪酸などから誘導されるアシル基、又はそれらの混合物が挙げられる。IOB値が3以上、又はカルボキシル基を2つ有するアミノ酸としては、例えばトレオニン、グリシン、セリン、グルタミン酸、アスパラギン酸などが挙げられ、またD−体、L−体及びDL−体の別を問わず使用できる。好ましくは、トレオニン、グルタミン酸、グリシンである。N−アシルアミノ酸塩を構成する塩としては、例えばナトリウム塩、カリウム塩等のアルカリ金属塩、低級アルカノールアミン塩などが挙げられるが、好ましくは、ナトリウム塩、カリウム塩である。 The component (A) used in the cleaning composition of the present invention is an N-acyl amino acid consisting of a fatty acid residue having an acyl group of 8 to 22 carbon atoms and an IOB value of 3 or more, or an amino acid having two carboxyl groups. It is salt. Examples of the fatty acid residue having 8 to 22 carbon atoms include a single acyl group such as lauric acid, myristic acid, palmitic acid, stearic acid, isostearic acid, oleic acid, coconut oil fatty acid, beef tallow fatty acid, castor oil fatty acid. , Acyl groups derived from olive oil fatty acids, palm oil fatty acids and the like, or mixtures thereof. Examples of amino acids having an IOB value of 3 or more or having two carboxyl groups include threonine, glycine, serine, glutamic acid, aspartic acid, and the like, regardless of the D-form, L-form, and DL-form. Can be used. Threonine, glutamic acid, and glycine are preferable. Examples of the salt constituting the N-acylamino acid salt include alkali metal salts such as sodium salt and potassium salt, and lower alkanolamine salts, and sodium salt and potassium salt are preferable.
本発明の洗浄剤組成物で用いられる成分(A)N−アシルアミノ酸塩を具体的に例示すれば、ヤシ油脂肪酸グルタミン酸カリウム、ヤシ油脂肪酸グルタミン酸ナトリウム、ヤシ油脂肪酸グルタミン酸トリエタノールアミン、パーム核油脂肪酸グルタミン酸アンモニウム、ラウロイルグルタミン酸ナトリウム、ラウロイルグルタミン酸トリエタノールアミン、ヤシ油脂肪酸トレオニンカリウム、ヤシ油脂肪酸トレオニントリエタノールアミン、パーム核油脂肪酸トレオニンアンモニウム、ヤシ油脂肪酸トレオニンナトリウム、ラウロイルトレオニンナトリウム、ラウロイルトレオニントリエタノールアミン、ヤシ油脂肪酸グリシンカリウム、ヤシ油脂肪酸グリシンナトリウム、パーム核油脂肪酸グリシンアンモニウム、ラウロイルグリシンナトリウム、ラウロイルグリシントリエタノールアミン、ヤシ油脂肪酸セリンカリウム、ヤシ油脂肪酸セリントリエタノールアミン、ラウロイルセリンナ
トリウム、ラウロイルセリントリエタノールアミン、パーム核油脂肪酸セリンアンモニウム、ヤシ油脂肪酸アスパラギン酸カリウム、ヤシ油脂肪酸アスパラギン酸ナトリウム、ヤシ油脂肪酸アスパラギン酸トリエタノールアミン、パーム核油脂肪酸アスパラギン酸アンモニウム、ラウロイルアスパラギン酸ナトリウム、ラウロイルアスパラギン酸トリエタノールアミンなどが挙げられる。これらN−アシルアミノ酸塩は市販品を使用することができ、具体的に例示すれば、アミライトGCK−12K、アミライトGCS−12K、アミライトET−CS−12等のアミライトシリーズ、アミソフトLS−11、アミソフトLT−12、アミソフトCK−11等のアミソフトシリーズ(いずれも味の素社製)等が挙げられる。本発明の洗浄剤組成物には、これらN−アシルアミノ酸塩を1種単独又は2種以上を組み合わせて用いることができる。
Specific examples of the component (A) N-acyl amino acid salt used in the cleaning composition of the present invention include coconut oil fatty acid potassium glutamate, coconut oil fatty acid sodium glutamate, coconut oil fatty acid glutamate triethanolamine, and palm kernel oil. Fatty Acid Ammonium Glutamate, Lauroyl Glutamate, Lauroyl Glutamate Triethanolamine, Palm Oil Fatty Acid Threonine Potassium, Palm Oil Fatty Acid Threonine Triethanolamine, Palm Kernel Oil Fatty Acid Threonine Ammonium, Palm Oil Fatty Acid Threonine Sodium, Lauroyl Lethreonine Sodium, Lauroyl Lethreonine Triethanolamine , Palm oil fatty acid glycine potassium, coconut oil fatty acid glycine sodium, palm kernel oil fatty acid glycine ammonium, lauroyl glycine nato Um, lauroylglycine triethanolamine, coconut oil fatty acid serine potassium, coconut oil fatty acid serine triethanolamine, lauroylserine sodium, lauroylserine triethanolamine, palm kernel oil fatty acid serine ammonium, coconut oil fatty acid potassium aspartate, coconut oil fatty acid asparagine Examples thereof include sodium acid, coconut oil fatty acid aspartate triethanolamine, palm kernel oil fatty acid ammonium aspartate, lauroyl aspartate sodium, lauroyl aspartate triethanolamine, and the like. Commercially available products of these N-acyl amino acid salts can be used. Specifically, amylite series such as amylite GCK-12K, amylite GCS-12K, amylite ET-CS-12, amisoft LS-11, Amisoft series (all manufactured by Ajinomoto Co., Inc.) such as Amisoft LT-12 and Amisoft CK-11. These N-acylamino acid salts can be used alone or in combination of two or more in the cleaning composition of the present invention.
本発明の洗浄剤組成物において、成分(A)N−アシルアミノ酸塩の配合量は、好ましくは0.6〜15%である。より好ましくは1%〜5%である。0.6%以上であれば、洗い流し中にきしみが生じることなく、つっぱり感も生じないため好ましい。一方15%以下であれば、洗浄剤組成物の粘度が低下することなく、使用性に優れた粘度が得られて好ましい。 In the cleaning composition of the present invention, the amount of component (A) N-acylamino acid salt is preferably 0.6 to 15%. More preferably, it is 1% to 5%. If it is 0.6% or more, a squeak does not occur during washing and a feeling of tension does not occur, which is preferable. On the other hand, if it is 15% or less, the viscosity which was excellent in usability will be obtained, without the viscosity of a cleaning composition falling, and it is preferable.
本発明の洗浄剤組成物で用いられる成分(B)は高級脂肪酸塩である。高級脂肪酸塩を構成する脂肪酸としては、好ましくは炭素数8〜22の飽和の脂肪酸である。例えばラウリン酸、ミリスチン酸、パルミチン酸、ステアリン酸などの単一の脂肪酸や、ヤシ油脂肪酸、牛脂脂肪酸、ヒマシ油脂肪酸、オリーブ油脂肪酸、パーム油脂肪酸などから誘導される脂肪酸、又はそれらの混合物が挙げられる。高級脂肪酸塩を構成する塩としては、例えばナトリウム塩、カリウム塩等のアルカリ金属塩、低級アルカノールアミン塩などが挙げられるが、好ましくは、ナトリウム塩、カリウム塩である。 The component (B) used in the cleaning composition of the present invention is a higher fatty acid salt. The fatty acid constituting the higher fatty acid salt is preferably a saturated fatty acid having 8 to 22 carbon atoms. For example, single fatty acids such as lauric acid, myristic acid, palmitic acid, stearic acid, fatty acids derived from coconut oil fatty acid, beef tallow fatty acid, castor oil fatty acid, olive oil fatty acid, palm oil fatty acid, etc., or a mixture thereof It is done. Examples of the salt constituting the higher fatty acid salt include alkali metal salts such as sodium salt and potassium salt, lower alkanolamine salts and the like, and sodium salt and potassium salt are preferable.
本発明の洗浄剤組成物で用いられる成分(B)高級脂肪酸塩を具体的に例示すれば、ラウリン酸ナトリウム、ミリスチン酸ナトリウム、パルミチン酸ナトリウム、ステアリン酸ナトリウム、イソステアリン酸ナトリウム、オレイン酸ナトリウム、ラウリン酸カリウム、ミリスチン酸カリウム、パルミチン酸カリウム、ステアリン酸カリウム、イソステアリン酸カリウム、オレイン酸カリウム、ラウリン酸トリエタノールアミン、ミリスチン酸トリエタノールアミン、パルミチン酸トリエタノールアミン、ステアリン酸トリエタノールアミン、イソステアリン酸トリエタノールアミン、オレイン酸トリエタノールアミン、ヤシ油脂肪酸ナトリウム、牛脂脂肪酸ナトリウム、ヒマシ油脂肪酸ナトリウム、オリーブ油脂肪酸ナトリウム、パーム油脂肪酸ナトリウム、パーム核油脂肪酸ナトリウム、ヤシ油脂肪酸カリウム、牛脂脂肪酸カリウム、ヒマシ油脂肪酸カリウム、オリーブ油脂肪酸カリウム、パーム油脂肪酸カリウム、パーム核油脂肪酸カリウム、ヤシ油脂肪酸トリエタノールアミン、牛脂脂肪酸トリエタノールアミン、ヒマシ油脂肪酸トリエタノールアミン、オリーブ油脂肪酸トリエタノールアミン、パーム油脂肪酸トリエタノールアミン、パーム核油脂肪酸トリエタノールアミン等が挙げられる。本発明の洗浄剤組成物には、これら高級脂肪酸塩を1種単独又は2種以上を組み合わせて用いることができる。 Specific examples of the component (B) higher fatty acid salt used in the cleaning composition of the present invention include sodium laurate, sodium myristate, sodium palmitate, sodium stearate, sodium isostearate, sodium oleate, laurin. Potassium acid, potassium myristate, potassium palmitate, potassium stearate, potassium isostearate, potassium oleate, triethanolamine laurate, triethanolamine myristate, triethanolamine palmitate, triethanolamine stearate, triisostearate Ethanolamine, oleic acid triethanolamine, palm oil fatty acid sodium, beef tallow fatty acid sodium, castor oil fatty acid sodium, olive oil fatty acid sodium, palm oil Sodium acid, palm kernel fatty acid sodium, palm oil fatty acid potassium, beef tallow fatty acid potassium, castor oil fatty acid potassium, olive oil fatty acid potassium, palm oil fatty acid potassium, palm kernel oil fatty acid potassium, coconut oil fatty acid triethanolamine, tallow fatty acid triethanolamine Castor oil fatty acid triethanolamine, olive oil fatty acid triethanolamine, palm oil fatty acid triethanolamine, palm kernel oil fatty acid triethanolamine, and the like. These higher fatty acid salts can be used alone or in combination of two or more in the cleaning composition of the present invention.
本発明の洗浄剤組成物において、成分(B)高級脂肪酸塩の配合量は、10〜42%であり、好ましくは10〜35%である。より好ましくは15〜30%である。10%未満では、良好な泡立ち、泡質(クリーミィ性)に加え、成分(D)との相互作用で得られる粘性が得られない。一方42%を超えると、低温での安定性が得られない。 In the cleaning composition of the present invention, the blending amount of the component (B) higher fatty acid salt is 10 to 42%, preferably 10 to 35%. More preferably, it is 15 to 30%. If it is less than 10%, in addition to good foaming and foam quality (creaminess), viscosity obtained by interaction with component (D) cannot be obtained. On the other hand, if it exceeds 42%, stability at low temperatures cannot be obtained.
本発明の洗浄剤組成物で使用される成分(C)陽イオン性高分子は、例えば塩化ジメチルジアリルアンモニウム・アルリルアミド共重合体、アクリルアミド・アクリル酸・塩化ジメチルジアリルアンモニウム共重合体液、塩化ジメチルジアリルアンモニウム・アクリル酸共重合体液、ポリ塩化ジメチルメチレンピペリジニウム液、カチオン化セルロース、カ
チオン化グァーガム、カチオン化フェヌグリークガム、カチオン化タラガム、カチオン化グルコマンナン、カチオン化ローカストビーンガム、アジピン酸ジメチルアミノヒドロキシプロピルジエチルトリアリアミン共重合体、ポリエチレンイミン、ポリエチレングリコール・エピクロルヒドリン・牛脂アルキルアミン・ジプロピレントリアミン縮合物などが挙げられる。これらのうち、塩化ジメチルジアリルアンモニウム・アクリルアミド共重合体、カチオン化グァーガム、カチオン化グルコマンナンが好ましい。これら陽イオン性高分子は、市販品を用いることが可能であり、例えば、マーコート550、マーコート295等のマーコートシリーズ(いずれもナルコ社製)、カチナールCG−100S、カチナールCLB−100等のカチナールシリーズ(いずれも東邦化学社製)が挙げられる。本発明の洗浄剤組成物には、これら陽イオン性高分子を1種単独又は2種以上を組み合わせて用いることができる。
The component (C) cationic polymer used in the cleaning composition of the present invention includes, for example, a dimethyldiallylammonium chloride / arrylamide copolymer, an acrylamide / acrylic acid / dimethyldiallylammonium chloride copolymer solution, and dimethyldiallylammonium chloride.・ Acrylic acid copolymer liquid, polydimethylmethylenepiperidinium chloride liquid, cationized cellulose, cationized guar gum, cationized fenugreek gum, cationized tara gum, cationized glucomannan, cationized locust bean gum, dimethylaminohydroxypropyl adipate Examples include diethyltrialiamine copolymer, polyethyleneimine, polyethylene glycol / epichlorohydrin / tallow alkylamine / dipropylenetriamine condensate. Of these, dimethyldiallylammonium chloride / acrylamide copolymer, cationized guar gum, and cationized glucomannan are preferable. Commercially available products can be used as these cationic polymers. For example, marcoat series such as Marcoat 550 and Marcoat 295 (both manufactured by Nalco), kachinal CG-100S, kachinal CLB-100, etc. Series (all manufactured by Toho Chemical Co., Ltd.). These cationic polymers can be used alone or in combination of two or more in the cleaning composition of the present invention.
本発明の洗浄剤組成物において、成分(C)陽イオン性高分子の配合量は、好ましくは0.01%〜1%である。より好ましくは0.1〜0.5%である。0.01%以上であれば、洗い流し中にきしみが生じることなく、つっぱり感も生じないため好ましい。一方、1%以下であれば、泡立ちが遅くならず製品の使用性上好ましい。 In the cleaning composition of the present invention, the amount of the component (C) cationic polymer is preferably 0.01% to 1%. More preferably, it is 0.1 to 0.5%. If it is 0.01% or more, squeaking does not occur during washing, and a feeling of tension does not occur, which is preferable. On the other hand, if it is 1% or less, foaming is not slow, which is preferable in terms of usability of the product.
本発明の洗浄剤組成物で使用される成分(D)アルキルポリグルコシドを具体的に例示すれば、デシルグルコシド、ラウリルグルコシド、ミリスチルグルコシド、ココイルグルコシド等が挙げられる。これらアルキルポリグルコシドは市販品を使用することができ、具体的に例示すれば、マイドール10、マイドール12(いずれも花王社製)、プランタケア2000UP、プランタケア1200UP、プランタケア818UP、プランタケア800UP等のプランタケアシリーズ(いずれもBASF社製)等が挙げられる。本発明の洗浄剤組成物には、これらアルキルポリグルコシドを1種単独又は2種以上を組み合わせて用いることができる。 Specific examples of the component (D) alkyl polyglucoside used in the cleaning composition of the present invention include decyl glucoside, lauryl glucoside, myristyl glucoside, cocoyl glucoside and the like. Commercially available products of these alkylpolyglucosides can be used. For example, Mydol 10, Mydol 12 (both manufactured by Kao Corporation), Planta Care 2000UP, Planta Care 1200UP, Planta Care 818UP, Planta Care A planter care series such as 800 UP (all manufactured by BASF) and the like. These alkyl polyglucosides can be used alone or in combination of two or more in the cleaning composition of the present invention.
本発明の洗浄剤組成物において、成分(D)アルキルポリグルコシドの配合量は、3〜22.5%であり、好ましくは5%〜20%である。より好ましくは5〜10%である。5%未満では、十分な粘度を得られず、22.5%を超えるとアルキルポリグルコシド特有のべたつき感が残り、感触上好ましくない。 In the cleaning composition of the present invention, the blending amount of component (D) alkylpolyglucoside is 3 to 22.5%, preferably 5% to 20%. More preferably, it is 5 to 10%. If it is less than 5%, sufficient viscosity cannot be obtained, and if it exceeds 22.5%, a sticky feeling peculiar to alkylpolyglucoside remains, which is not preferable in terms of touch.
本発明の洗浄剤組成物で使用される成分(E)塩化ナトリウムの配合量は、0%〜1.5%であり、好ましくは0.1〜1%である。1.5%を超えると低温での安定性が得られない。 The amount of component (E) sodium chloride used in the cleaning composition of the present invention is 0% to 1.5%, preferably 0.1 to 1%. If it exceeds 1.5%, stability at low temperatures cannot be obtained.
本発明の洗浄剤組成物で使用される成分(F)塩化カリウムの配合量は、0%〜2%であり、好ましくは0.3〜1.5%である。2.0%を超えると低温での安定性が得られない。 The amount of component (F) potassium chloride used in the cleaning composition of the present invention is 0% to 2%, preferably 0.3 to 1.5%. If it exceeds 2.0%, stability at low temperatures cannot be obtained.
本発明の洗浄剤組成物は、上述した成分の他に、本発明の目的を損なわない範囲で他の成分、例えば、アニオン界面活性剤、カチオン界面活性剤、両性界面活性剤、ノニオン界面活性剤、水溶性高分子化合物(ノニオン性、アニオン性等を含む)、粉体(顔料、色素、樹脂等)、生理活性成分、酸化防止剤、金属イオン封鎖剤、防腐剤、紫外線吸収剤、香料、保湿剤、塩類、溶媒、パール化剤、中和剤、昆虫忌避剤、酵素等の成分を適宜配合することができる。 In addition to the above-described components, the cleaning composition of the present invention includes other components as long as the object of the present invention is not impaired, for example, anionic surfactants, cationic surfactants, amphoteric surfactants, nonionic surfactants. , Water-soluble polymer compounds (including nonionic, anionic, etc.), powders (pigments, dyes, resins, etc.), physiologically active ingredients, antioxidants, sequestering agents, antiseptics, ultraviolet absorbers, fragrances, Components such as humectants, salts, solvents, pearling agents, neutralizing agents, insect repellents, enzymes and the like can be appropriately blended.
上記アニオン界面活性剤としては、特に限定されるものではなく、例えばラウリル硫酸トリエタノールアミン、ラウリル硫酸アンモニウム、ラウリルエーテル硫酸ナトリウム、ポリオキシエチレンラウリルエーテル硫酸ナトリウム、ポリオキシエチレンヤシ油脂肪酸アミドエーテル硫酸カリウム、ラウリルリン酸ナトリウム、ポリオキシエチレンラウリルエ
ーテル酢酸ナトリウム等が挙げられ、適宜一種又は二種以上選択して用いればよい。
The anionic surfactant is not particularly limited. For example, lauryl sulfate triethanolamine, ammonium lauryl sulfate, sodium lauryl ether sulfate, polyoxyethylene lauryl ether sodium sulfate, polyoxyethylene coconut oil fatty acid amide ether potassium sulfate, Examples thereof include sodium lauryl phosphate, sodium polyoxyethylene lauryl ether acetate and the like, and one or two or more may be appropriately selected and used.
上記両性界面活性剤としては、特に限定されるものではないが、例えばラウリン酸アミドプロピルベタイン、ヤシ油脂肪酸アミドプロピルベタイン、ラウリルジメチルアミノ酢酸ベタイン、2−アルキル−N−カルボキシメチル−N−ヒドロキシエチルイミダゾリニウムベタイン、ラウリルアミノジ酢酸ナトリウム、β−アミノプロピオン酸ナトリウム、N−ラウロイル−N’−カルボキシメチル−N’−ヒドロキシエチルエチレンジアミンナトリウム等が挙げられ、適宜一種又は二種以上選択して用いればよい。 The amphoteric surfactant is not particularly limited, and examples thereof include lauric acid amidopropyl betaine, coconut oil fatty acid amidopropyl betaine, lauryldimethylaminoacetic acid betaine, 2-alkyl-N-carboxymethyl-N-hydroxyethyl. Examples include imidazolinium betaine, sodium laurylaminodiacetate, sodium β-aminopropionate, N-lauroyl-N′-carboxymethyl-N′-hydroxyethylethylenediamine sodium, etc. That's fine.
上記ノニオン界面活性剤としては、特に限定されるものではないが、例えばポリオキシエチレンセチルエーテル、モノステアリン酸ソルビタン、トリイソステアリン酸ポリオキシエチレンソルビタン、ポリオキシエチレン硬化ヒマシ油、ポリオキシエチレンモノイソステアレート、ポリオキシエチレンジオレイン酸グリセリル、ヤシ油脂肪酸ジエタノールアミド、ヤシ油脂肪酸モノエタノールアミド、ヤシ油脂肪酸N−メチルエタノールアミド、ポリオキシエチレンポリオキシプロピレングリコール、モノラウリン酸ポリエチレングリコール等が挙げられ、適宜一種又は二種以上選択して用いればよい。 The nonionic surfactant is not particularly limited. For example, polyoxyethylene cetyl ether, sorbitan monostearate, polyoxyethylene sorbitan triisostearate, polyoxyethylene hydrogenated castor oil, polyoxyethylene monoisostearate Glyceryl polyoxyethylene dioleate, coconut oil fatty acid diethanolamide, coconut oil fatty acid monoethanolamide, coconut oil fatty acid N-methylethanolamide, polyoxyethylene polyoxypropylene glycol, polyethylene glycol monolaurate, etc. One type or two or more types may be selected and used.
上記水溶性高分子としては、特に限定されるものではないが、例えばヒドロキシエチルセルロース、ヒドロキシプロピルセルロース、ヒドロキシプロピルメチルセルロース、ポリエチレングリコール、高重合ポリエチレングリコール、ポリビニルアルコール、ポリグルタミン酸、カルボキシビニルポリマー、アクリル酸・メタクリル酸アルキル共重合体、アクリル酸アルキル共重合体等が挙げられ、適宜一種又は二種以上選択して用いればよい。 The water-soluble polymer is not particularly limited. For example, hydroxyethyl cellulose, hydroxypropyl cellulose, hydroxypropyl methylcellulose, polyethylene glycol, highly polymerized polyethylene glycol, polyvinyl alcohol, polyglutamic acid, carboxyvinyl polymer, acrylic acid / Examples thereof include an alkyl methacrylate copolymer and an alkyl acrylate copolymer, and one or two or more types may be appropriately selected and used.
また、上記粉体としては、例えば赤色201号、黄色4号、青色1号、黒色401号等の色素、黄色4号Alレーキ、黄色203号Baレーキ等のレーキ色素、ナイロンパウダー、シルクパウダー、シリコーンパウダー、セルロースパウダー、シリコーンエラストマー球状粉体、ポリエチレン末等の高分子、黄酸化鉄、赤色酸化鉄、酸化クロム、カーボンブラック、群青、紺青等の有色顔料、酸化亜鉛、酸化チタン等の白色顔料、タルク、マイカ、セリサイト、カオリン等の体質顔料、雲母チタン等のパール顔料、硫酸バリウム、炭酸カルシウム、炭酸マグネシウム、珪酸マグネシウム等の金属塩、シリカ、アルミナ等の無機粉体、ベントナイト、スメクタイト、窒化ホウ素等が挙げられる。これらの粉体の形状(球状、棒状、針状、板状、不定形状、燐片状、紡錘状など)に特に制限はない。 Examples of the powder include pigments such as red No. 201, yellow No. 4, blue No. 1, black No. 401, lake pigments such as yellow No. 4 Al lake, yellow No. 203 Ba lake, nylon powder, silk powder, Silicone powder, cellulose powder, silicone elastomer spherical powder, polymers such as polyethylene powder, yellow iron oxide, red iron oxide, chromium oxide, carbon black, colored pigments such as ultramarine and bitumen, white pigments such as zinc oxide and titanium oxide , Body pigments such as talc, mica, sericite, kaolin, pearl pigments such as titanium mica, metal salts such as barium sulfate, calcium carbonate, magnesium carbonate, magnesium silicate, inorganic powders such as silica and alumina, bentonite, smectite, Examples thereof include boron nitride. There are no particular restrictions on the shape of these powders (spherical, rod-like, needle-like, plate-like, indeterminate, flake-like, spindle-like, etc.).
上記生理活性成分としては、皮膚に塗布した場合に皮膚に何らかの生理活性を与える物質が挙げられる。例えば、抗炎症剤、老化防止剤、紫外線防御剤、ひきしめ剤、抗酸化剤、保湿剤、血行促進剤、抗菌剤、殺菌剤、乾燥剤、冷感剤、温感剤、ビタミン類、アミノ酸、創傷治癒促進剤、刺激緩和剤、鎮痛剤、細胞賦活剤、酵素成分等が挙げられる。上記生理活性成分は、天然系の植物抽出成分、海藻抽出成分、生薬成分や、化合物等が挙げられるが、これらの中でも、特に天然系の植物抽出成分、海藻抽出成分、生薬成分が安全性の点で好ましい。 Examples of the physiologically active ingredient include substances that impart some physiological activity to the skin when applied to the skin. For example, anti-inflammatory agents, anti-aging agents, UV protection agents, tanning agents, antioxidants, moisturizers, blood circulation promoters, antibacterial agents, bactericides, desiccants, cooling agents, warming agents, vitamins, amino acids, Examples include wound healing promoters, stimulus-relieving agents, analgesics, cell activators, enzyme components, and the like. Examples of the physiologically active component include natural plant extract components, seaweed extract components, herbal medicine components, and compounds. Among these, natural plant extract components, seaweed extract components, herbal medicine components are particularly safe. This is preferable.
上記天然系の植物抽出成分、海藻抽出成分、生薬成分の例としては、例えばアシタバエキス、アマチャエキス、アルテアエキス、アロエエキス、アンズエキス、イチョウエキス、ウイキョウエキス、ウーロン茶エキス、エイジツエキス、オウゴンエキス、オウバクエキス、オトギリソウエキス、オランダカラシエキス、オレンジエキス、海水乾燥物、海藻エキス、加水分解コムギ末、加水分解シルク、カモミラエキス、カロットエキス、カワラヨモギエキス、甘草エキス、カキョクエキス、キウイエキス、キューカンバーエキス、クチナシエキス、クマザサエキス、クララエキス、クルミエキス、グレープフルーツエキス、クロレラエキス、クワエキス、紅茶エキス、酵母エキス、コラーゲン、サルビアエキス、サボンソウエキス、サンザシエキス、ジオウエキス、シコンエキス、シソエキス、シナノ
キエキス、シャクヤクエキス、シラカバエキス、スギナエキス、セイヨウキズタエキス、セイヨウサンザシエキス、セイヨウニワトコエキス、セイヨウノコギリソウエキス、セイヨウハッカエキス、セージエキス、センキュウエキス、センブリエキス、ダイズエキス、タイソウエキス、タイムエキス、茶エキス、チョウジエキス、チンピエキス、トウキエキス、トウニンエキス、ドクダミエキス、トマトエキス、納豆エキス、ニンジンエキス、ニンニクエキス、ノバラエキス、蜂蜜、ハマメリスエキス、ヒキオコシエキス、ビサボロール、ビワエキス、ブクリョウエキス、プロポリス、ヘチマエキス、ペパーミントエキス、ボダイジュエキス、ホップエキス、マドンナリリー花エキス、マロニエエキス、ムクロジエキス、メリッサエキス、モモエキス、ユキノシタエキス、ユズエキス、ヨモギエキス、ラベンダーエキス、レモンエキス、レンゲソウエキス、ローズマリーエキス、ローヤルゼリーエキス等を挙げることができる。
Examples of the above-mentioned natural plant extract components, seaweed extract components, herbal medicine components include, for example, Ashitaba extract, Achacha extract, Altea extract, Aloe extract, Apricot extract, Ginkgo biloba extract, Fennel extract, Oolong tea extract, Ages extract, Ogon extract, Oat extract, Hypericum extract, Dutch mustard extract, Orange extract, Seawater dried product, Seaweed extract, Hydrolyzed wheat powder, Hydrolyzed silk, Chamomile extract, Carrot extract, Kawara mugwort extract, Licorice extract, Kiwi extract, Cucumber extract, Gardenia extract, Kumazasa extract, Clara extract, Walnut extract, Grapefruit extract, Chlorella extract, Mulberry extract, Black tea extract, Yeast extract, Collagen, Salvia extract, Soap extract, Hawthorn Kiss, Giant extract, Shikon extract, Perilla extract, Linden extract, Peonies extract, Birch extract, Horsetail extract, Horseshoe extract, Hawthorn extract, Horseshoe extract, Pepper extract, Sage extract, Senkyu extract, Assembly extract, Soybean extract , Tiso extract, thyme extract, tea extract, clove extract, chimpi extract, toki extract, tonin extract, dokudami extract, tomato extract, natto extract, carrot extract, garlic extract, wild rose extract, honey, hamamelis extract, cassava extract, bisabolol, loquat extract, bukuryu Extract, Propolis, Loofah extract, Peppermint extract, Bodaige extract, Hop extract, Madonna lily flower Ex , Mention may be made of horse chestnut extract, Sapindus extract, Melissa extract, peach, strawberry geranium extract, Yuzuekisu, mugwort extract, lavender extract, lemon extract, Astragalus Saw extract, rosemary extract, royal jelly extract, and the like.
また、上記天然系の植物抽出成分、海藻抽出成分、生薬成分以外の成分としては、例えばデオキシリボ核酸、コラーゲン、エラスチン、キチン、キトサン、加水分解卵殻膜などの生体高分子、アミノ酸、乳酸ナトリウム、尿素、ピロリドンカルボン酸ナトリウム、ベタイン、ホエイなどの保湿成分、スフィンゴ脂質、セラミド、コレステロール、コレステロール誘導体、リン脂質などの油性成分、ε−アミノカプロン酸、グリチルリチン酸、β−グリチルレチン酸、塩化リゾチーム、グアイアズレン、ヒドロコルチゾン等の抗炎症剤、ビタミン類(A、B2、B6、C、D、E)、パントテン酸カルシウム、ビオチン、ニコチン酸アミド、ビタミンCエステル等のビタミン類、アラントイン、ジイソプロピルアミンジクロロアセテート、4−アミノメチルシクロヘキサンカルボン酸等の活性成分、トコフェロール、カロチノイド、フラボノイド、タンニン、リグナン、サポニン等の抗酸化剤、α−ヒドロキシ酸、β−ヒドロキシ酸などの細胞賦活剤、γ−オリザノール、ビタミンE誘導体などの血行促進剤、イソプロピルメチルフェノール、トリクロサン、ヒノキチオール、塩化ベンザルコニウム等の殺菌剤、l−メントール、ハッカ油等の冷感剤、レチノール、レチノール誘導体等の創傷治癒剤等が挙げられる。 Examples of components other than the above natural plant extract components, seaweed extract components, and herbal medicine components include biopolymers such as deoxyribonucleic acid, collagen, elastin, chitin, chitosan, and hydrolyzed eggshell membranes, amino acids, sodium lactate, and urea. , Moisturizing ingredients such as sodium pyrrolidone carboxylate, betaine, whey, oily ingredients such as sphingolipid, ceramide, cholesterol, cholesterol derivatives, phospholipids, ε-aminocaproic acid, glycyrrhizic acid, β-glycyrrhetinic acid, lysozyme chloride, guaiazulene, hydrocortisone Anti-inflammatory agents such as vitamins (A, B2, B6, C, D, E), vitamins such as calcium pantothenate, biotin, nicotinamide, vitamin C ester, allantoin, diisopropylamine dichloroacetate, 4-a Active ingredients such as minomethylcyclohexanecarboxylic acid, antioxidants such as tocopherols, carotenoids, flavonoids, tannins, lignans, saponins, cell activators such as α-hydroxy acids, β-hydroxy acids, γ-oryzanol, vitamin E derivatives, etc. Blood circulation promoters, bactericides such as isopropylmethylphenol, triclosan, hinokitiol and benzalkonium chloride, cooling agents such as l-menthol and mint oil, and wound healing agents such as retinol and retinol derivatives.
本発明の洗浄剤組成物は、洗顔、クレンジング、ボディシャンプー、ハンドソープ、シェービング料、マッサージ料等の皮膚用洗浄剤として好適に使用できる。またそれぞれ、粘性液体、クリーム状等の形態として用いることができ、特に洗顔フォーム、液状ボディシャンプーとして好適に用いられる。 The cleaning composition of the present invention can be suitably used as a cleaning agent for skin such as face washing, cleansing, body shampoo, hand soap, shaving fee, massage fee and the like. Each can be used in the form of a viscous liquid, cream or the like, and is particularly suitably used as a facial cleansing foam or liquid body shampoo.
次に本発明の洗浄剤組成物について、実施例をもって詳細に説明するが、本発明はこれにより限定されるものではない。 Next, although the cleaning composition of this invention is demonstrated in detail with an Example, this invention is not limited by this.
実施例1〜44及び比較例1〜16
表1〜6に示す組成の洗浄剤組成物を常法により調製した。実施例及び比較例の洗浄剤組成物に対し、下記の試験法、評価法の評価を行った。評価結果を表1〜6に併せて示す。なお、以下の全ての実施例及び比較例における配合量は質量%である。
Examples 1-44 and Comparative Examples 1-16
Cleaning compositions having the compositions shown in Tables 1 to 6 were prepared by a conventional method. The following test methods and evaluation methods were evaluated for the cleaning compositions of Examples and Comparative Examples. An evaluation result is combined with Tables 1-6, and is shown. In addition, the compounding quantity in all the following examples and comparative examples is the mass%.
(1)洗い流し時の使用感、泡立ち、泡質(クリーミィ性)評価法
10名の専門パネルにより、実施例及び比較例の洗浄剤組成物を使用し、洗い流し時の使用感、使用時の泡立ち、使用時の泡質(クリーミィ性)の各項目について官能評価により評価を行った。尚、評価基準は以下の通りである。
[洗い流し時の使用感]
<きしみ感のなさ>
◎:極めて良好 きしみ感がないと答えた被験者の数が8人以上
○:良好 きしみ感がないと答えた被験者の数が6人以上、8人未満
△:やや悪い きしみ感がないと答えた被験者の数が4人以上、6人未満
×:悪い きしみ感がないと答えた被験者の数が4人未満
<べたつきのなさ>
◎:極めて良好 べたつきがないと答えた被験者の数が8人以上
○:良好 べたつきがないと答えた被験者の数が6人以上、8人未満
△:やや悪い べたつきがないと答えた被験者の数が4人以上、6人未満
×:悪い べたつきがないと答えた被験者の数が4人未満
[使用時の泡立ち]
◎:極めて良好 泡立ちが良いと答えた被験者の数が8人以上
○:良好 泡立ちが良いと答えた被験者の数が6人以上、8人未満
△:やや悪い 泡立ちが良いと答えた被験者の数が4人以上、6人未満
×:悪い 泡立ちが良いと答えた被験者の数が4人未満
[使用時の泡質(クリーミィ性)]
◎:極めて良好 泡質(クリーミィ性)が良いと答えた被験者の数が8人以上
○:良好 泡質(クリーミィ性)が良いと答えた被験者の数が6人以上、8人未満△:やや悪い 泡質(クリーミィ性)が良いと答えた被験者の数が4人以上、6人未満×:悪い 泡質(クリーミィ性)が良いと答えた被験者の数が4人未満
(1) Usability, foaming and foaming (creamy property) evaluation method at the time of washing Using the detergent compositions of Examples and Comparative Examples by a panel of 10 experts, the feeling of use at the time of washing and foaming at the time of use Each item of foam quality (creamy property) at the time of use was evaluated by sensory evaluation. The evaluation criteria are as follows.
[Usage feeling when washing off]
<No squeaky feeling>
◎: The number of subjects who answered that there was no very squeaking feeling was 8 or more. ○: The number of subjects who answered that there was no squeaking feeling was 6 or more, less than 8. △: There was no feeling of squeaking slightly. Number of subjects is 4 or more and less than 6 ×: The number of subjects who answered that there is no squeaky feeling is less than 4 <no stickiness>
◎: The number of subjects who answered that there was no very good stickiness was 8 or more ○: The number of subjects who answered that there was no good stickiness was 6 or more and less than 8 △: The number of subjects who answered that there was no bad stickiness 4 or more and less than 6 ×: The number of subjects who answered that there was no bad stickiness was less than 4 [bubbles during use]
◎: Very good The number of subjects who answered that bubbling was good was 8 or more. ○: Good The number of subjects who answered that bubbling was good was 6 or more and less than 8. △: Slightly bad Number of subjects who answered that bubbling was good. 4 or more, less than 6 ×: Poor The number of subjects who answered that foaming was good was less than 4 [foam quality during use (creamy)]
◎: Very good The number of subjects who answered that the foam quality (creamy property) is good is 8 or more ○: The number of subjects who answered that the foam quality (creamy property) is good is 6 or more, less than 8 △: Somewhat The number of subjects who answered that the foam quality (creamy) was good was 4 or more and less than 6 x: The number of subjects who answered that the foam quality (creamy) was good was less than 4
(2)低温安定性試験(外観評価)
実施例及び比較例の洗浄剤組成物をガラス瓶に充填し、0℃で静置したときの経時安定性について、下記判断基準により評価を行った。
◎:2ヶ月間析出物なし
○:1ヶ月間析出物なし(2ヶ月後析出物有り)
△:2週間析出物なし(1ヶ月後析出物有り)
×:1週間析出物なし(2週間後析出物有り)
(2) Low temperature stability test (appearance evaluation)
The cleaning compositions of Examples and Comparative Examples were filled in glass bottles and evaluated with respect to stability over time when allowed to stand at 0 ° C. according to the following criteria.
◎: No deposit for 2 months ○: No deposit for 1 month (with deposit after 2 months)
Δ: No deposit for 2 weeks (with deposit after 1 month)
×: No precipitate for 1 week (with deposit after 2 weeks)
(3)物性試験(粘度)
[粘度測定条件]
測定温度:30℃、測定時間:30sec
粘度計:芝浦システム株式会社製 ビスメトロン粘度計VSA型
測定結果:単位(mPa・s)
(3) Physical property test (viscosity)
[Viscosity measurement conditions]
Measurement temperature: 30 ° C., measurement time: 30 sec
Viscometer: Bismetron viscometer VSA type manufactured by Shibaura System Co., Ltd. Measurement result: Unit (mPa · s)
実施例及び比較例の洗浄剤組成物をガラス瓶に充填し、30℃で静置したときの粘度について、増粘剤未配合処方と比較して、下記判断基準により評価を行った。
◎:大きな増粘効果が見られる(2000mPa・s以上)。
○:増粘効果が見られる(1000mPa・s程度)。
△:若干、増粘効果が見られる(500mPa・s程度。)
×:ほとんど増粘効果が見られない。
The viscosity when the detergent compositions of Examples and Comparative Examples were filled in glass bottles and allowed to stand at 30 ° C. was evaluated according to the following criteria, as compared with a thickener-unblended formulation.
A: A large thickening effect is observed (2000 mPa · s or more).
○: A thickening effect is observed (about 1000 mPa · s).
Δ: Slightly thickening effect is observed (about 500 mPa · s)
X: Almost no thickening effect is observed.
表1〜表6より明らかなように、本発明の成分を用いた実施例1〜44の洗浄剤組成物は比較例1〜16の組成物に比べていずれも優れた性能を見出した。 As is clear from Tables 1 to 6, the cleaning compositions of Examples 1 to 44 using the components of the present invention all found superior performance as compared to the compositions of Comparative Examples 1 to 16.
以下、本発明の洗浄剤組成物のその他の処方例を実施例45、46として挙げる。なお、これらの実施例の洗浄剤組成物についても、上記の洗い流し時の使用感、使用時の泡立ち、使用時の泡質(クリーミィ性)、低温安定性、物性の各項目を評価した。 Hereinafter, other formulation examples of the cleaning composition of the present invention are given as Examples 45 and 46. The cleaning compositions of these examples were also evaluated for the items of use feeling during washing, foaming during use, foam quality (creaminess) during use, low-temperature stability, and physical properties.
実施例45 洗顔フォーム
(1)ラウリン酸カリウム 2.0
(2)ミリスチン酸カリウム 16.0
(3)パルミチン酸カリウム 6.0
(4)ステアリン酸カリウム 6.0
(5)ココイルトレオニンナトリウム 2.0
(6)ココイルグルタミン酸ナトリウム 0.3
(7)ココイルグリシンカリウム 2.0
(8)塩化ジメチルジアリルアンモニウム・アクリルアミド共重合体 0.5
(9)トマト果実エキス 0.5
(10)ユズ果実エキス 0.5
(11)スクワラン 0.5
(12)ベリー葉エキス 0.5
(13)ブドウ葉エキス 0.5
(14)プルーン分解物 0.5
(15)シア脂 0.5
(16)アボカド油 0.5
(17)ダイズエキス 0.5
(18)バラエキス 0.5
(19)サピンヅストリホリアツス果実エキス 0.5
(20)ユキノシタエキス 0.5
(21)モモ葉エキス 0.5
(22)アロエベラ葉エキス 0.5
(23)N−アセチルグルコサミン 0.5
(24)カニナバラ果実エキス 0.5
(25)エデト酸二ナトリウム 0.5
(26)フェノキシエタノール 0.5
(27)ジプロピレングリコール 0.5
(28)グリセリン 30.0
(29)デシルグルコシド 4.0
(30)ラウリルグルコシド 4.0
(31)香料 0.2
(32)精製水 残余
Example 45 Face Wash Foam (1) Potassium Laurate 2.0
(2) Potassium myristate 16.0
(3) Potassium palmitate 6.0
(4) Potassium stearate 6.0
(5) Cocoylthreonine sodium 2.0
(6) Sodium cocoyl glutamate 0.3
(7) Potassium cocoylglycine 2.0
(8) Dimethyldiallylammonium chloride / acrylamide copolymer 0.5
(9) Tomato fruit extract 0.5
(10) Yuzu fruit extract 0.5
(11) Squalane 0.5
(12) Berry leaf extract 0.5
(13) Grape leaf extract 0.5
(14) Prune degradation product 0.5
(15) Shea fat 0.5
(16) Avocado oil 0.5
(17) Soybean extract 0.5
(18) Rose extract 0.5
(19) Sapin's Strawberry Fruit Extract 0.5
(20) Yukinoshita extract 0.5
(21) Peach leaf extract 0.5
(22) Aloe vera leaf extract 0.5
(23) N-acetylglucosamine 0.5
(24) Canina rose fruit extract 0.5
(25) Edetate disodium 0.5
(26) Phenoxyethanol 0.5
(27) Dipropylene glycol 0.5
(28) Glycerin 30.0
(29) Decyl glucoside 4.0
(30) Lauryl glucoside 4.0
(31) Fragrance 0.2
(32) Purified water residue
常法により上記組成の洗浄剤組成物を調製し、洗い流し時の使用感、使用時の泡立ち、使用時の泡質(クリーミィ性)、低温安定性、物性を評価したところ、いずれの特性も優れており良好な結果を得た。 A cleaning composition having the above composition was prepared by a conventional method, and when using it, the feeling of use at the time of washing, foaming at the time of use, foam quality (creaminess) at the time of use, low temperature stability, and physical properties were evaluated. Good results were obtained.
実施例29 ボディソープ
(1)ラウリン酸カリウム 6.0
(2)ミリスチン酸カリウム 12.0
(3)パルミチン酸カリウム 3.0
(4)ステアリン酸カリウム 1.0
(5)ココイルトレオニンナトリウム 2.0
(6)ココイルグルタミン酸ナトリウム 0.3
(7)ココイルグリシンカリウム 2.0
(8)塩化ジメチルジアリルアンモニウム・アクリルアミド共重合体 0.5
(9)トマト果実エキス 0.5
(10)ユズ果実エキス 0.5
(11)スクワラン 0.5
(12)ベリー葉エキス 0.5
(13)ブドウ葉エキス 0.5
(14)プルーン分解物 0.5
(15)シア脂 0.5
(16)アボカド油 0.5
(17)ダイズエキス 0.5
(18)バラエキス 0.5
(19)サピンヅストリホリアツス果実エキス 0.5
(20)ユキノシタエキス 0.5
(21)モモ葉エキス 0.5
(22)アロエベラ葉エキス 0.5
(23)N−アセチルグルコサミン 0.5
(24)カニナバラ果実エキス 0.5
(25)エデト酸二ナトリウム 0.5
(26)フェノキシエタノール 0.5
(27)ジプロピレングリコール 0.5
(28)グリセリン 0.5
(29)デシルグルコシド 4.0
(30)ラウリルグルコシド 4.0
(31)香料 0.2
(32)精製水 残余
Example 29 Body Soap (1) Potassium Laurate 6.0
(2) Potassium myristate 12.0
(3) Potassium palmitate 3.0
(4) Potassium stearate 1.0
(5) Cocoylthreonine sodium 2.0
(6) Sodium cocoyl glutamate 0.3
(7) Potassium cocoylglycine 2.0
(8) Dimethyldiallylammonium chloride / acrylamide copolymer 0.5
(9) Tomato fruit extract 0.5
(10) Yuzu fruit extract 0.5
(11) Squalane 0.5
(12) Berry leaf extract 0.5
(13) Grape leaf extract 0.5
(14) Prune degradation product 0.5
(15) Shea fat 0.5
(16) Avocado oil 0.5
(17) Soybean extract 0.5
(18) Rose extract 0.5
(19) Sapin's Strawberry Fruit Extract 0.5
(20) Yukinoshita extract 0.5
(21) Peach leaf extract 0.5
(22) Aloe vera leaf extract 0.5
(23) N-acetylglucosamine 0.5
(24) Canina rose fruit extract 0.5
(25) Edetate disodium 0.5
(26) Phenoxyethanol 0.5
(27) Dipropylene glycol 0.5
(28) Glycerin 0.5
(29) Decyl glucoside 4.0
(30) Lauryl glucoside 4.0
(31) Fragrance 0.2
(32) Purified water residue
常法により上記組成の洗浄剤組成物を調製し、洗い流し時の使用感、使用時の泡立ち、使用時の泡質(クリーミィ性)、低温安定性、物性を評価したところ、いずれの特性も優れており良好な結果を得た。 A cleaning composition having the above composition was prepared by a conventional method, and when using it, the feeling of use at the time of washing, foaming at the time of use, foam quality (creaminess) at the time of use, low temperature stability, and physical properties were evaluated. Good results were obtained.
Claims (3)
(A)アシル基が炭素原子数8〜22の脂肪酸残基と、IOB値が3以上、又はカルボキシル基を2つ有するアミノ酸からなるN−アシルアミノ酸塩から選ばれる一種または二種以上
(B)炭素数8〜22の高級脂肪酸塩 10〜42質量%
(C)陽イオン性高分子
(D)アルキルポリグルコシド 3〜22.5質量%
(E)塩化ナトリウム 0.1〜1.5質量% The following components (A) to (E) are contained, the blending ratio (B) / (D) is 1 to 5.5, and the blending amount (B) + (D) is 20 to 45 in the entire composition. A cleaning composition, wherein the cleaning composition is mass%.
(A) One type or two or more types (B) selected from N-acyl amino acid salts consisting of fatty acid residues having 8 to 22 carbon atoms and an IOB value of 3 or more, or an amino acid having two carboxyl groups 10 to 42% by mass of higher fatty acid salt having 8 to 22 carbon atoms
(C) Cationic polymer (D) Alkyl polyglucoside 3 to 22.5% by mass
(E) Sodium chloride 0.1-1.5 mass%
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JP6959035B2 (en) * | 2016-05-30 | 2021-11-02 | 花王株式会社 | Skin cleanser composition |
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JP7052221B2 (en) * | 2016-07-01 | 2022-04-12 | 味の素株式会社 | Detergent composition |
US10376452B2 (en) * | 2016-07-01 | 2019-08-13 | Ajinomoto Co., Inc. | Cleansing composition |
JP6903426B2 (en) * | 2016-12-15 | 2021-07-14 | ロレアル | Effervescent composition |
FR3068043A1 (en) * | 2017-06-22 | 2018-12-28 | Societe D'exploitation De Produits Pour Les Industries Chimiques Seppic | NOVEL SURFACE MIXTURE, NOVEL COMPOSITION COMPRISING THE SAME AND ITS USE IN COSMETICS |
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