JP6110439B2 - 走査型透過荷電粒子顕微鏡の校正方法 - Google Patents
走査型透過荷電粒子顕微鏡の校正方法 Download PDFInfo
- Publication number
- JP6110439B2 JP6110439B2 JP2015137413A JP2015137413A JP6110439B2 JP 6110439 B2 JP6110439 B2 JP 6110439B2 JP 2015137413 A JP2015137413 A JP 2015137413A JP 2015137413 A JP2015137413 A JP 2015137413A JP 6110439 B2 JP6110439 B2 JP 6110439B2
- Authority
- JP
- Japan
- Prior art keywords
- sample
- scanning
- detector
- calibration
- scanning mode
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002245 particle Substances 0.000 title claims description 37
- 238000000034 method Methods 0.000 title claims description 30
- 230000005540 biological transmission Effects 0.000 title claims description 8
- 238000003384 imaging method Methods 0.000 claims description 30
- 239000013078 crystal Substances 0.000 claims description 17
- 239000003550 marker Substances 0.000 claims description 4
- 238000012360 testing method Methods 0.000 claims description 3
- 239000000523 sample Substances 0.000 description 62
- 230000006870 function Effects 0.000 description 12
- 230000000694 effects Effects 0.000 description 10
- 238000010894 electron beam technology Methods 0.000 description 10
- 150000002500 ions Chemical class 0.000 description 9
- 239000011295 pitch Substances 0.000 description 9
- 230000005855 radiation Effects 0.000 description 9
- 230000033001 locomotion Effects 0.000 description 8
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 5
- 230000003287 optical effect Effects 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 239000011888 foil Substances 0.000 description 4
- 230000004075 alteration Effects 0.000 description 3
- 230000000295 complement effect Effects 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 239000010931 gold Substances 0.000 description 3
- 238000011835 investigation Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 238000003801 milling Methods 0.000 description 3
- 230000003252 repetitive effect Effects 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 238000005452 bending Methods 0.000 description 2
- 238000001444 catalytic combustion detection Methods 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000001186 cumulative effect Effects 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000002149 energy-dispersive X-ray emission spectroscopy Methods 0.000 description 2
- 238000005530 etching Methods 0.000 description 2
- 238000013213 extrapolation Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000001888 ion beam-induced deposition Methods 0.000 description 2
- 238000010884 ion-beam technique Methods 0.000 description 2
- 230000007246 mechanism Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000005424 photoluminescence Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000001902 propagating effect Effects 0.000 description 2
- 238000011002 quantification Methods 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000004611 spectroscopical analysis Methods 0.000 description 2
- 238000009966 trimming Methods 0.000 description 2
- 229910052727 yttrium Inorganic materials 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 241000226585 Antennaria plantaginifolia Species 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 238000003491 array Methods 0.000 description 1
- 230000006399 behavior Effects 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 150000001721 carbon Chemical class 0.000 description 1
- 238000005136 cathodoluminescence Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- BBKFSSMUWOMYPI-UHFFFAOYSA-N gold palladium Chemical compound [Pd].[Au] BBKFSSMUWOMYPI-UHFFFAOYSA-N 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000000386 microscopy Methods 0.000 description 1
- 230000000116 mitigating effect Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 239000013074 reference sample Substances 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000001350 scanning transmission electron microscopy Methods 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/26—Electron or ion microscopes; Electron or ion diffraction tubes
- H01J37/28—Electron or ion microscopes; Electron or ion diffraction tubes with scanning beams
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/20—Means for supporting or positioning the object or the material; Means for adjusting diaphragms or lenses associated with the support
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/244—Detectors; Associated components or circuits therefor
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2237/00—Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
- H01J2237/26—Electron or ion microscopes
- H01J2237/28—Scanning microscopes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2237/00—Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
- H01J2237/26—Electron or ion microscopes
- H01J2237/28—Scanning microscopes
- H01J2237/2802—Transmission microscopes
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2237/00—Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
- H01J2237/26—Electron or ion microscopes
- H01J2237/28—Scanning microscopes
- H01J2237/2813—Scanning microscopes characterised by the application
- H01J2237/2817—Pattern inspection
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J2237/00—Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
- H01J2237/26—Electron or ion microscopes
- H01J2237/282—Determination of microscope properties
- H01J2237/2826—Calibration
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Length-Measuring Devices Using Wave Or Particle Radiation (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14176529.7 | 2014-07-10 | ||
| EP14176529.7A EP2966668B1 (en) | 2014-07-10 | 2014-07-10 | Method of calibrating a scanning transmission charged-particle microscope |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016017966A JP2016017966A (ja) | 2016-02-01 |
| JP2016017966A5 JP2016017966A5 (enExample) | 2016-12-08 |
| JP6110439B2 true JP6110439B2 (ja) | 2017-04-05 |
Family
ID=51162576
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015137413A Active JP6110439B2 (ja) | 2014-07-10 | 2015-07-09 | 走査型透過荷電粒子顕微鏡の校正方法 |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US9396907B2 (enExample) |
| EP (1) | EP2966668B1 (enExample) |
| JP (1) | JP6110439B2 (enExample) |
| CN (1) | CN105261544B (enExample) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB201715902D0 (en) * | 2017-09-29 | 2017-11-15 | Oxford Instr Plc | Improved system for electron diffraction analysis |
| EP3531439B1 (en) * | 2018-02-22 | 2020-06-24 | FEI Company | Intelligent pre-scan in scanning transmission charged particle microscopy |
| JP7138066B2 (ja) * | 2018-03-20 | 2022-09-15 | テスカン ブルノ エスアールオー | 歳差電子回折データマッピングのために走査型透過電子顕微鏡を自動的にアライメントする方法 |
| US12236603B2 (en) | 2020-02-12 | 2025-02-25 | Samantree Medical Sa | Systems and methods for imaging samples with reduced sample motion artifacts |
| US11263510B2 (en) * | 2020-07-15 | 2022-03-01 | GM Global Technology Operations LLC | Method for performing measurements of dendritic structures for all magnifications and camera resolutions of microscopes |
| JP2024531132A (ja) * | 2021-08-04 | 2024-08-29 | サマンツリー メディカル エスアー | 並列撮像システムでライブ試料モニタリング情報を提供するシステム及び方法 |
| EP4345447A1 (en) | 2022-09-30 | 2024-04-03 | Fei Company | A method of automated data acquisition for a transmission electron microscope |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6807314B1 (en) * | 1999-07-02 | 2004-10-19 | General Phosphorix, Llc | Method of precision calibration of a microscope and the like |
| JP4434446B2 (ja) * | 2000-07-21 | 2010-03-17 | Okiセミコンダクタ株式会社 | 走査型電子顕微鏡の校正方法 |
| US6770867B2 (en) | 2001-06-29 | 2004-08-03 | Fei Company | Method and apparatus for scanned instrument calibration |
| JP2005520281A (ja) | 2001-07-13 | 2005-07-07 | ナノファクトリー インストルメンツ アーベー | 顕微鏡のひずみの影響を低減するためのデバイス |
| US7164128B2 (en) * | 2003-11-25 | 2007-01-16 | Hitachi High-Technologies Corporation | Method and apparatus for observing a specimen |
| JP4587742B2 (ja) * | 2004-08-23 | 2010-11-24 | 株式会社日立ハイテクノロジーズ | 荷電粒子線顕微方法及び荷電粒子線応用装置 |
| CN101461026B (zh) * | 2006-06-07 | 2012-01-18 | Fei公司 | 与包含真空室的装置一起使用的滑动轴承 |
| JP4801518B2 (ja) * | 2006-07-07 | 2011-10-26 | 株式会社日立ハイテクノロジーズ | 荷電粒子線顕微方法および荷電粒子線装置 |
| JP5151277B2 (ja) * | 2007-07-04 | 2013-02-27 | 富士通株式会社 | 試料観察装置とその補正方法 |
| EP2166557A1 (en) | 2008-09-22 | 2010-03-24 | FEI Company | Method for correcting distortions in a particle-optical apparatus |
| EP2197018A1 (en) | 2008-12-12 | 2010-06-16 | FEI Company | Method for determining distortions in a particle-optical apparatus |
| EP2511936B1 (en) | 2011-04-13 | 2013-10-02 | Fei Company | Distortion free stigmation of a TEM |
| EP2584584A1 (en) * | 2011-10-19 | 2013-04-24 | FEI Company | Method for adjusting a STEM equipped with an aberration corrector |
| US8598527B2 (en) * | 2011-11-22 | 2013-12-03 | Mochii, Inc. | Scanning transmission electron microscopy |
| US9188555B2 (en) | 2012-07-30 | 2015-11-17 | Fei Company | Automated EDS standards calibration |
-
2014
- 2014-07-10 EP EP14176529.7A patent/EP2966668B1/en active Active
-
2015
- 2015-07-09 JP JP2015137413A patent/JP6110439B2/ja active Active
- 2015-07-09 US US14/795,704 patent/US9396907B2/en active Active
- 2015-07-10 CN CN201510403896.2A patent/CN105261544B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2966668B1 (en) | 2016-10-12 |
| US20160013016A1 (en) | 2016-01-14 |
| JP2016017966A (ja) | 2016-02-01 |
| CN105261544B (zh) | 2017-08-18 |
| US9396907B2 (en) | 2016-07-19 |
| CN105261544A (zh) | 2016-01-20 |
| EP2966668A1 (en) | 2016-01-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP6110439B2 (ja) | 走査型透過荷電粒子顕微鏡の校正方法 | |
| JP6294280B2 (ja) | 特殊な絞り板を備える荷電粒子顕微鏡 | |
| KR102277028B1 (ko) | 회절 패턴을 이용한 샘플 정렬 시스템 | |
| JP6162187B2 (ja) | 透過型荷電粒子顕微鏡内で分光を実行する方法 | |
| JP5727564B2 (ja) | 荷電粒子レンズ系における収差を調査及び補正する方法 | |
| US9535020B2 (en) | Analyzing an object using a particle beam apparatus | |
| KR102365001B1 (ko) | 프티코그래피를 이용한 시료 이미징 방법 | |
| JP7703817B2 (ja) | 電子エネルギー損失分光検出器を備えた透過型荷電粒子顕微鏡 | |
| US8294096B2 (en) | Charged particle beam device and a method of operating a charged particle beam device | |
| CN106796188A (zh) | 基于自动化决策的能量分散式x射线方法及设备 | |
| WO2015015985A1 (ja) | 荷電粒子線装置及び荷電粒子線装置における収差測定法 | |
| JP6416825B2 (ja) | タイコグラフィックイメージングの方法 | |
| JP2018186076A (ja) | 荷電粒子顕微鏡における収差測定 | |
| TW201833969A (zh) | 用於電子束系統中之像差校正之方法及系統 | |
| JP5560246B2 (ja) | 荷電粒子線装置に用いられる標準試料,及び荷電粒子線装置に用いられる標準試料の製造方法 | |
| JP2023110072A (ja) | 走査型電子顕微鏡および走査型電子顕微鏡の2次電子検出方法 | |
| JP7597287B2 (ja) | 透過型電子顕微鏡のための自動データ取得方法 | |
| JP2005032732A (ja) | 走査電子顕微鏡 | |
| Etheridge et al. | Imaging high-energy electrons propagating in a crystal | |
| JP2023007094A (ja) | 走査電子顕微鏡 | |
| Schroer et al. | Hard X‐Ray Scanning Microscopy with Coherent Diffraction Contrast | |
| CN115547798A (zh) | 具有减少的束诱导样品损伤的用于使用扫描透射带电粒子显微镜研究样品的方法和系统 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20161020 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20161020 |
|
| A871 | Explanation of circumstances concerning accelerated examination |
Free format text: JAPANESE INTERMEDIATE CODE: A871 Effective date: 20161020 |
|
| A975 | Report on accelerated examination |
Free format text: JAPANESE INTERMEDIATE CODE: A971005 Effective date: 20161031 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20161122 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20170209 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20170228 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20170309 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 6110439 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |