JP6062244B2 - リアクターの製造方法およびリアクターの集合体 - Google Patents
リアクターの製造方法およびリアクターの集合体 Download PDFInfo
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- JP6062244B2 JP6062244B2 JP2012510307A JP2012510307A JP6062244B2 JP 6062244 B2 JP6062244 B2 JP 6062244B2 JP 2012510307 A JP2012510307 A JP 2012510307A JP 2012510307 A JP2012510307 A JP 2012510307A JP 6062244 B2 JP6062244 B2 JP 6062244B2
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- 238000004519 manufacturing process Methods 0.000 title claims description 9
- 238000000034 method Methods 0.000 claims description 62
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- 230000008569 process Effects 0.000 description 46
- 238000013341 scale-up Methods 0.000 description 10
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- 238000013461 design Methods 0.000 description 6
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- 230000033228 biological regulation Effects 0.000 description 3
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- 238000005259 measurement Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 238000007239 Wittig reaction Methods 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- WASQWSOJHCZDFK-UHFFFAOYSA-N diketene Chemical compound C=C1CC(=O)O1 WASQWSOJHCZDFK-UHFFFAOYSA-N 0.000 description 1
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- 239000000463 material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00004—Scale aspects
- B01J2219/00015—Scale-up
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00801—Means to assemble
- B01J2219/00804—Plurality of plates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00851—Additional features
- B01J2219/00858—Aspects relating to the size of the reactor
- B01J2219/0086—Dimensions of the flow channels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00889—Mixing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00993—Design aspects
- B01J2219/00995—Mathematical modeling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/0318—Processes
- Y10T137/0402—Cleaning, repairing, or assembling
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
リアクターの一例としてのマイクロリアクターが、欧州特許出願公開第1839739号明細書に開示される。リアクターは、一つ以上の反応物または抽出物(典型的には、二つ以上の反応物の混合を含む)の反応のために設けられ、そして加熱又は冷却を経る前記反応物の反応の制御のため、あるいは混合の前、その間、および/またはその後に前記反応物を熱的にバッファする(buffering)ためのある程度の大きさが設けられた反応装置である。小さな領域で化学反応を起こすための他のマイクロリアクターは、例えば欧州特許出願公開第0688242号明細書、欧州特許出願公開第1031375号明細書、国際公開第2004/045761号パンフレット、および米国特許出願公開第2004/0109798号明細書で既知である。
本発明の目的は、同じ生成物を作るために設計されるが容積流量が目標の容積流量と異なる標準のリアクターから始まり、目標のリアクターの中に流れ込む複数の反応物または抽出物の目標のリアクターの内で進む化学反応によって、所望の生成物の目標の容積流量を達成する目標のリアクター、特にマイクロリアクターの製造方法を提供することである。
Claims (5)
- 試作のリアクターから目標のマイクロリアクターを製造する製造方法であって、
前記目標のマイクロリアクターは、前記目標のマイクロリアクターの外に連続的に流れ出る生成物の流れを第1の容積流量f2とするように、前記目標のマイクロリアクターの流路に連続的に流れ込んだ複数の反応物の流れが、乱流または遷移性の乱流となるように混合部で混合されるとともに、反応物の相互の反応を生じさせる流路系を有しており、
前記試作のリアクターは、最小の水力直径dh1と流路系を有しており、
この試作のリアクターの前記流路系内で、試作のリアクターに連続的に流れ込んだ複数の反応物の流れが、乱流または遷移性の乱流となるように混合部で混合されて、前記目標のマイクロリアクターと同じ反応物の同じ反応を生じさせ、前記試作のリアクターの外に連続的に流れ出る生成物の流れを第2の容積流量f1とし、この第2の容積流量f1は、
前記第1の容積流量f2よりも大きいか小さいかであり、
前記目標のマイクロリアクターの流路の最小の水力直径dh2を、次の関係式により計算して求め、
そして、求めた最小の水力直径dh2に基づいて、目標のマイクロリアクターを製造する製造方法。 - 前記dh2とdh1とは、dh2>dh1 であって、f 2 >f 1 である請求項1に記載の方法。
- 前記混合部は、複数の混合要素を有する少なくとも一つの混合区域を備える、請求項1又は2に記載の方法。
- 試作のリアクターと目標のマイクロリアクターとの集合体であって、
前記試作のリアクターは、乱流または遷移性の乱流で試作のリアクターの流路を流れて試作の容積流量f1となるように複数の反応物が混合部で混合されるとともに、前記反応物の反応を生じさせる流路系を備え、
前記目標のマイクロリアクターは、前記目標のマイクロリアクターの流路を連続的に流れて目標の容積流量f2となるように複数の反応物が混合部で混合されるとともに、前記目標のマイクロリアクターと同様の反応物の同じ反応を生じさせる、流路系を備え、
前記試作の容積流量f1は、前記目標の容積流量f2よりも大きいか小さいかであり、
試作のリアクターの最小の水力直径dh1と目標のマイクロリアクターの対応する最小の水力直径dh2とについて次の関数が適用されるように、試作のリアクターと目標のマイクロリアクターとは設定されており、
- 前記dh2とdh1とは、dh2>dh1 であって、f 2 >f 1 である請求項4に記載の集合体。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EPPCT/EP2009/055740 | 2009-05-12 | ||
EP2009055740 | 2009-05-12 | ||
PCT/EP2010/056597 WO2010130811A2 (en) | 2009-05-12 | 2010-05-12 | Method of manufacturing a reactor and set of reactors |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2012526650A JP2012526650A (ja) | 2012-11-01 |
JP6062244B2 true JP6062244B2 (ja) | 2017-01-18 |
Family
ID=41460969
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012510307A Active JP6062244B2 (ja) | 2009-05-12 | 2010-05-12 | リアクターの製造方法およびリアクターの集合体 |
Country Status (12)
Country | Link |
---|---|
US (1) | US9023296B2 (ja) |
JP (1) | JP6062244B2 (ja) |
CN (1) | CN102421518B (ja) |
BR (1) | BRPI1010558A2 (ja) |
CA (1) | CA2757392A1 (ja) |
DE (1) | DE202009017416U1 (ja) |
EA (2) | EA027758B1 (ja) |
HK (1) | HK1170447A1 (ja) |
IL (1) | IL215572A0 (ja) |
MX (1) | MX2011011317A (ja) |
SG (1) | SG175228A1 (ja) |
WO (1) | WO2010130811A2 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR102670096B1 (ko) | 2021-12-31 | 2024-05-27 | 주식회사 신생에너지연구개발 | 바이오 디젤 제조용 극소 반응기 |
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US9599407B2 (en) * | 2009-07-29 | 2017-03-21 | Tokitae Llc | System and structure for heating or sterilizing a liquid stream |
TW201139337A (en) | 2010-03-31 | 2011-11-16 | Lonza Ag | Process for the production of esters of nitric acid |
EP2535105A1 (en) * | 2011-06-14 | 2012-12-19 | Corning Incorporated | Systems and methods for scale-up of microreactors |
WO2014080408A2 (en) * | 2012-11-25 | 2014-05-30 | Turbulent Technologies Ltd. | A mixing method and device for solvent extraction, especially in hydrometallurgical processes |
CN115178206B (zh) | 2017-07-31 | 2023-09-29 | 康宁股份有限公司 | 改进的工艺强化流反应器 |
EP3727672B1 (de) * | 2017-12-21 | 2023-05-17 | HTE GmbH The High Throughput Experimentation Company | Reaktorsystem und verfahren für durchflussreaktionen |
CN108031426A (zh) * | 2018-02-01 | 2018-05-15 | 贵州道元生物技术有限公司 | 一种板式连续流通道化学反应器 |
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BR9405989A (pt) | 1993-03-19 | 1995-12-26 | Du Pont | Estruturas integrais para manufatura e processamento químico processo de preparação de uma estrutura integral aparelho e método de processamento químico e de manufatura |
US6369893B1 (en) * | 1998-05-19 | 2002-04-09 | Cepheid | Multi-channel optical detection system |
DE29903296U1 (de) | 1999-02-24 | 2000-08-03 | Cpc Cellular Process Chemistry | Mikroreaktor |
DE19959249A1 (de) | 1999-12-08 | 2001-07-19 | Inst Mikrotechnik Mainz Gmbh | Modulares Mikroreaktionssystem |
US7241423B2 (en) | 2000-02-03 | 2007-07-10 | Cellular Process Chemistry, Inc. | Enhancing fluid flow in a stacked plate microreactor |
DE10005549A1 (de) | 2000-02-09 | 2001-09-06 | Cpc Cellular Process Chemistry | Mikroreaktor für Reaktionsmedien in Form einer Suspension |
EP1286761A2 (en) | 2000-05-24 | 2003-03-05 | Cellular Process Chemistry Inc. | Modular chemical production system incorporating a microreactor |
DE10036602A1 (de) | 2000-07-27 | 2002-02-14 | Cpc Cellular Process Chemistry | Mikroreaktor für Reaktionen zwischen Gasen und Flüssigkeiten |
DE10036633B4 (de) | 2000-07-27 | 2005-03-10 | Hte Ag The High Throughput Exp | Anordnung in modularer Bauweise und Verfahren zur paralellen Testung einer Mehrzahl von Bausteinen einer Materialbibliothek |
DE10042746A1 (de) | 2000-08-31 | 2002-03-28 | Degussa | Verfahren und Vorrichtung zum Durchführen von Reaktionen in einem Reaktor mit spaltförmigen Reaktionsräumen |
DE10106996C2 (de) | 2001-02-15 | 2003-04-24 | Merck Patent Gmbh | Einrichtung zur Verbindung von Mikrokomponenten |
FR2823995B1 (fr) | 2001-04-25 | 2008-06-06 | Alfa Laval Vicarb | Dispositif perfectionne d'echange et/ou de reaction entre fluides |
CA2472945A1 (en) | 2002-02-13 | 2003-08-21 | Nanostream, Inc. | Microfluidic separation column devices and fabrication methods |
GB0203653D0 (en) | 2002-02-15 | 2002-04-03 | Syrris Ltd | A microreactor |
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SE524540C2 (sv) | 2002-11-18 | 2004-08-24 | Alfa Laval Corp Ab | Flödesstyrande insats i en reaktorkammare samt reaktor försedd med insatsen |
DE602004009681T2 (de) | 2003-05-16 | 2008-08-14 | Velocys, Inc., Plain City | Verfahren zur erzeugung einer emulsion durch verwendung einer mikrokanalverfahrentechnologie |
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EP1679115A1 (en) * | 2005-01-07 | 2006-07-12 | Corning Incorporated | High performance microreactor |
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EP2223741A1 (en) | 2009-02-13 | 2010-09-01 | Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO | Micro fluidic system, including a stack of process modules and heat exchange modules |
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2009
- 2009-12-23 DE DE202009017416U patent/DE202009017416U1/de not_active Expired - Lifetime
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2010
- 2010-05-12 US US12/743,760 patent/US9023296B2/en active Active
- 2010-05-12 MX MX2011011317A patent/MX2011011317A/es not_active Application Discontinuation
- 2010-05-12 CN CN201080020562.2A patent/CN102421518B/zh active Active
- 2010-05-12 EA EA201171166A patent/EA027758B1/ru not_active IP Right Cessation
- 2010-05-12 WO PCT/EP2010/056597 patent/WO2010130811A2/en active Application Filing
- 2010-05-12 EA EA201790846A patent/EA201790846A1/ru unknown
- 2010-05-12 JP JP2012510307A patent/JP6062244B2/ja active Active
- 2010-05-12 SG SG2011075108A patent/SG175228A1/en unknown
- 2010-05-12 CA CA2757392A patent/CA2757392A1/en not_active Abandoned
- 2010-05-12 BR BRPI1010558A patent/BRPI1010558A2/pt not_active IP Right Cessation
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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KR102670096B1 (ko) | 2021-12-31 | 2024-05-27 | 주식회사 신생에너지연구개발 | 바이오 디젤 제조용 극소 반응기 |
Also Published As
Publication number | Publication date |
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US20120045376A1 (en) | 2012-02-23 |
MX2011011317A (es) | 2011-11-18 |
EA201171166A2 (ru) | 2012-05-30 |
BRPI1010558A2 (pt) | 2019-04-09 |
JP2012526650A (ja) | 2012-11-01 |
IL215572A0 (en) | 2011-12-29 |
CA2757392A1 (en) | 2010-11-18 |
EA201790846A1 (ru) | 2017-11-30 |
CN102421518A (zh) | 2012-04-18 |
DE202009017416U1 (de) | 2010-04-15 |
EA027758B1 (ru) | 2017-08-31 |
WO2010130811A2 (en) | 2010-11-18 |
HK1170447A1 (en) | 2013-03-01 |
US9023296B2 (en) | 2015-05-05 |
SG175228A1 (en) | 2011-11-28 |
CN102421518B (zh) | 2014-09-17 |
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