JP2012526650A - リアクターの製造方法およびリアクターの集合体 - Google Patents
リアクターの製造方法およびリアクターの集合体 Download PDFInfo
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- JP2012526650A JP2012526650A JP2012510307A JP2012510307A JP2012526650A JP 2012526650 A JP2012526650 A JP 2012526650A JP 2012510307 A JP2012510307 A JP 2012510307A JP 2012510307 A JP2012510307 A JP 2012510307A JP 2012526650 A JP2012526650 A JP 2012526650A
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000012530 fluid Substances 0.000 claims abstract description 52
- 239000000376 reactant Substances 0.000 claims abstract description 27
- 238000000034 method Methods 0.000 claims description 62
- 238000006243 chemical reaction Methods 0.000 claims description 52
- 230000008569 process Effects 0.000 description 43
- 238000013341 scale-up Methods 0.000 description 10
- 230000008859 change Effects 0.000 description 6
- 238000013461 design Methods 0.000 description 6
- 238000011161 development Methods 0.000 description 6
- 238000012546 transfer Methods 0.000 description 5
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- 230000033228 biological regulation Effects 0.000 description 3
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- 238000005259 measurement Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 238000007239 Wittig reaction Methods 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- WASQWSOJHCZDFK-UHFFFAOYSA-N diketene Chemical compound C=C1CC(=O)O1 WASQWSOJHCZDFK-UHFFFAOYSA-N 0.000 description 1
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- 239000000463 material Substances 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 238000005381 potential energy Methods 0.000 description 1
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00004—Scale aspects
- B01J2219/00015—Scale-up
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00783—Laminate assemblies, i.e. the reactor comprising a stack of plates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00801—Means to assemble
- B01J2219/00804—Plurality of plates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00851—Additional features
- B01J2219/00858—Aspects relating to the size of the reactor
- B01J2219/0086—Dimensions of the flow channels
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00889—Mixing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00781—Aspects relating to microreactors
- B01J2219/00993—Design aspects
- B01J2219/00995—Mathematical modeling
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
- Y10T137/0318—Processes
- Y10T137/0402—Cleaning, repairing, or assembling
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
リアクターの一例としてのマイクロリアクターが、欧州特許出願公開第1839739号明細書に開示される。リアクターは、一つ以上の反応物または抽出物(典型的には、二つ以上の反応物の混合を含む)の反応のために設けられ、そして加熱又は冷却を経る前記反応物の反応の制御のため、あるいは混合の前、その間、および/またはその後に前記反応物を熱的にバッファする(buffering)ためのある程度の大きさが設けられた反応装置である。小さな領域で化学反応を起こすための他のマイクロリアクターは、例えば欧州特許出願公開第0688242号明細書、欧州特許出願公開第1031375号明細書、国際公開第2004/045761号パンフレット、および米国特許出願公開第2004/0109798号明細書で既知である。
本発明の目的は、同じ生成物を作るために設計されるが容積流量が目標の容積流量と異なる標準のリアクターから始まり、目標のリアクターの中に流れ込む複数の反応物または抽出物の目標のリアクターの内で進む化学反応によって、所望の生成物の目標の容積流量を達成する目標のリアクター、特にマイクロリアクターの製造方法を提供することである。
このため、乱流状態において、「混合のスケールアップの判定基準」は、単位容積あたりのエネルギー入力である。より高い流量において、このエネルギー入力に関する計算された水力直径は、方程式(1)で表される。増加されたエネルギーの消失は、より高い圧力降下によって得られる。圧力降下の支配的な要素は混合区域に起因し、これはマイクロリアクターを高い流量で作動させているときに注意されなければならない主要な区域である。例えば、流量が100ミリリットル/分から200ミリリットル/分になるなら、混合区域の水力直径は1.34倍に増加するべきである。滞留区域では状況が異なる。ここでは、板の同じ形状(幅×高さ)を保つことが可能であるが、長さが増加することは当業者には明らかである。上述のように、滞留区域の主な仕事は混合ではなく、熱交換である。このため、滞留区域のスケールアップの判定基準は、水力直径ではなく、流路形状を一定に(可能な限り長く)保つことである。しかし、高い容積流量での幾つかの状況において、流路の高さを増加させ、同じ流路の幅を保ち、例えば0.5×5平方ミリメートルから0.5×10平方ミリメートルにするに足る。熱交換が重要であるため、流路幅は、その区域において重要なスケールアップの要因であり、小さな板から大きな板まで一定に保たれる。
Claims (7)
- 1/3≧n≧0、好ましくは1/4≧n≧0が適用される請求項1の方法。
- dh2>dh1である請求項1または2に記載の方法。
- 前記目標のリアクターが、複数の混合要素を有する少なくとも一つの混合区域を備えるマイクロリアクターである請求項1ないし3のいずれか一つに記載の方法。
- 1/3≧n≧0、好ましくは1/4≧n≧0が適用される請求項5の集合体。
- dh2>dh1である請求項5または6に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP2009055740 | 2009-05-12 | ||
EPPCT/EP2009/055740 | 2009-05-12 | ||
PCT/EP2010/056597 WO2010130811A2 (en) | 2009-05-12 | 2010-05-12 | Method of manufacturing a reactor and set of reactors |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2012526650A true JP2012526650A (ja) | 2012-11-01 |
JP6062244B2 JP6062244B2 (ja) | 2017-01-18 |
Family
ID=41460969
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012510307A Active JP6062244B2 (ja) | 2009-05-12 | 2010-05-12 | リアクターの製造方法およびリアクターの集合体 |
Country Status (12)
Country | Link |
---|---|
US (1) | US9023296B2 (ja) |
JP (1) | JP6062244B2 (ja) |
CN (1) | CN102421518B (ja) |
BR (1) | BRPI1010558A2 (ja) |
CA (1) | CA2757392A1 (ja) |
DE (1) | DE202009017416U1 (ja) |
EA (2) | EA201790846A1 (ja) |
HK (1) | HK1170447A1 (ja) |
IL (1) | IL215572A0 (ja) |
MX (1) | MX2011011317A (ja) |
SG (1) | SG175228A1 (ja) |
WO (1) | WO2010130811A2 (ja) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9599407B2 (en) * | 2009-07-29 | 2017-03-21 | Tokitae Llc | System and structure for heating or sterilizing a liquid stream |
TW201139337A (en) | 2010-03-31 | 2011-11-16 | Lonza Ag | Process for the production of esters of nitric acid |
EP2535105A1 (en) * | 2011-06-14 | 2012-12-19 | Corning Incorporated | Systems and methods for scale-up of microreactors |
WO2014080408A2 (en) * | 2012-11-25 | 2014-05-30 | Turbulent Technologies Ltd. | A mixing method and device for solvent extraction, especially in hydrometallurgical processes |
WO2019028002A1 (en) | 2017-07-31 | 2019-02-07 | Corning Incorporated | PERFECTED CONTINUOUS REACTOR |
WO2019122101A1 (de) * | 2017-12-21 | 2019-06-27 | Hte Gmbh The High Throughput Experimentation Company | Reaktorsystem für durchflussreaktionen |
CN108031426A (zh) * | 2018-02-01 | 2018-05-15 | 贵州道元生物技术有限公司 | 一种板式连续流通道化学反应器 |
KR102670096B1 (ko) * | 2021-12-31 | 2024-05-27 | 주식회사 신생에너지연구개발 | 바이오 디젤 제조용 극소 반응기 |
Family Cites Families (23)
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US4894709A (en) * | 1988-03-09 | 1990-01-16 | Massachusetts Institute Of Technology | Forced-convection, liquid-cooled, microchannel heat sinks |
JP3512186B2 (ja) | 1993-03-19 | 2004-03-29 | イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー | 化学処理及び製造のための一体構造及び方法、並びにその使用方法及び製造方法 |
US6369893B1 (en) | 1998-05-19 | 2002-04-09 | Cepheid | Multi-channel optical detection system |
DE29903296U1 (de) | 1999-02-24 | 2000-08-03 | CPC Cellular Process Chemistry GmbH, 60386 Frankfurt | Mikroreaktor |
DE19959249A1 (de) | 1999-12-08 | 2001-07-19 | Inst Mikrotechnik Mainz Gmbh | Modulares Mikroreaktionssystem |
US7241423B2 (en) | 2000-02-03 | 2007-07-10 | Cellular Process Chemistry, Inc. | Enhancing fluid flow in a stacked plate microreactor |
DE10005549A1 (de) | 2000-02-09 | 2001-09-06 | Cpc Cellular Process Chemistry | Mikroreaktor für Reaktionsmedien in Form einer Suspension |
EP1286761A2 (en) | 2000-05-24 | 2003-03-05 | Cellular Process Chemistry Inc. | Modular chemical production system incorporating a microreactor |
DE10036602A1 (de) | 2000-07-27 | 2002-02-14 | Cpc Cellular Process Chemistry | Mikroreaktor für Reaktionen zwischen Gasen und Flüssigkeiten |
DE10036633B4 (de) | 2000-07-27 | 2005-03-10 | Hte Ag The High Throughput Exp | Anordnung in modularer Bauweise und Verfahren zur paralellen Testung einer Mehrzahl von Bausteinen einer Materialbibliothek |
DE10042746A1 (de) | 2000-08-31 | 2002-03-28 | Degussa | Verfahren und Vorrichtung zum Durchführen von Reaktionen in einem Reaktor mit spaltförmigen Reaktionsräumen |
DE10106996C2 (de) | 2001-02-15 | 2003-04-24 | Merck Patent Gmbh | Einrichtung zur Verbindung von Mikrokomponenten |
FR2823995B1 (fr) | 2001-04-25 | 2008-06-06 | Alfa Laval Vicarb | Dispositif perfectionne d'echange et/ou de reaction entre fluides |
EP1474236B1 (en) | 2002-02-13 | 2006-01-04 | Nanostream, Inc. | Microfluidic separation column devices and fabrication methods |
GB0203653D0 (en) | 2002-02-15 | 2002-04-03 | Syrris Ltd | A microreactor |
US6872645B2 (en) * | 2002-04-02 | 2005-03-29 | Nanosys, Inc. | Methods of positioning and/or orienting nanostructures |
SE524540C2 (sv) | 2002-11-18 | 2004-08-24 | Alfa Laval Corp Ab | Flödesstyrande insats i en reaktorkammare samt reaktor försedd med insatsen |
EP1633463B1 (en) | 2003-05-16 | 2007-10-24 | Velocys Inc. | Process for forming an emulsion using microchannel process technology |
US20050207953A1 (en) | 2003-07-22 | 2005-09-22 | The Regents Of The University Of California | High aspect ratio chemical microreactor |
EP1679115A1 (en) * | 2005-01-07 | 2006-07-12 | Corning Incorporated | High performance microreactor |
SE529516C2 (sv) | 2005-10-24 | 2007-09-04 | Alfa Laval Corp Ab | Universell flödesmodul |
TW200738328A (en) * | 2006-03-31 | 2007-10-16 | Lonza Ag | Micro-reactor system assembly |
EP2223741A1 (en) | 2009-02-13 | 2010-09-01 | Nederlandse Organisatie voor toegepast -natuurwetenschappelijk onderzoek TNO | Micro fluidic system, including a stack of process modules and heat exchange modules |
-
2009
- 2009-12-23 DE DE202009017416U patent/DE202009017416U1/de not_active Expired - Lifetime
-
2010
- 2010-05-12 US US12/743,760 patent/US9023296B2/en active Active
- 2010-05-12 CA CA2757392A patent/CA2757392A1/en not_active Abandoned
- 2010-05-12 JP JP2012510307A patent/JP6062244B2/ja active Active
- 2010-05-12 EA EA201790846A patent/EA201790846A1/ru unknown
- 2010-05-12 EA EA201171166A patent/EA027758B1/ru not_active IP Right Cessation
- 2010-05-12 BR BRPI1010558A patent/BRPI1010558A2/pt not_active IP Right Cessation
- 2010-05-12 SG SG2011075108A patent/SG175228A1/en unknown
- 2010-05-12 CN CN201080020562.2A patent/CN102421518B/zh active Active
- 2010-05-12 MX MX2011011317A patent/MX2011011317A/es not_active Application Discontinuation
- 2010-05-12 WO PCT/EP2010/056597 patent/WO2010130811A2/en active Application Filing
-
2011
- 2011-10-05 IL IL215572A patent/IL215572A0/en unknown
-
2012
- 2012-10-17 HK HK12110274.2A patent/HK1170447A1/xx unknown
Also Published As
Publication number | Publication date |
---|---|
HK1170447A1 (en) | 2013-03-01 |
BRPI1010558A2 (pt) | 2019-04-09 |
SG175228A1 (en) | 2011-11-28 |
US20120045376A1 (en) | 2012-02-23 |
EA201790846A1 (ru) | 2017-11-30 |
MX2011011317A (es) | 2011-11-18 |
WO2010130811A2 (en) | 2010-11-18 |
CN102421518B (zh) | 2014-09-17 |
DE202009017416U1 (de) | 2010-04-15 |
EA027758B1 (ru) | 2017-08-31 |
JP6062244B2 (ja) | 2017-01-18 |
EA201171166A2 (ru) | 2012-05-30 |
US9023296B2 (en) | 2015-05-05 |
CA2757392A1 (en) | 2010-11-18 |
CN102421518A (zh) | 2012-04-18 |
IL215572A0 (en) | 2011-12-29 |
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