JP6013612B2 - 界面活性剤を有する液体活性化処方物 - Google Patents
界面活性剤を有する液体活性化処方物 Download PDFInfo
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- JP6013612B2 JP6013612B2 JP2015533312A JP2015533312A JP6013612B2 JP 6013612 B2 JP6013612 B2 JP 6013612B2 JP 2015533312 A JP2015533312 A JP 2015533312A JP 2015533312 A JP2015533312 A JP 2015533312A JP 6013612 B2 JP6013612 B2 JP 6013612B2
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- Prior art keywords
- acid
- liquid activated
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- yellow
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- 239000000203 mixture Substances 0.000 title claims description 126
- 239000007788 liquid Substances 0.000 title claims description 109
- 238000009472 formulation Methods 0.000 title claims description 73
- 239000004094 surface-active agent Substances 0.000 title claims description 50
- 239000003086 colorant Substances 0.000 claims description 97
- -1 citric acid ester Chemical class 0.000 claims description 65
- 239000002250 absorbent Substances 0.000 claims description 40
- 230000002745 absorbent Effects 0.000 claims description 40
- 239000002253 acid Substances 0.000 claims description 39
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Natural products OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 23
- 239000011159 matrix material Substances 0.000 claims description 23
- 230000004913 activation Effects 0.000 claims description 20
- 239000003381 stabilizer Substances 0.000 claims description 19
- 230000002378 acidificating effect Effects 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 239000003605 opacifier Substances 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- 229920001577 copolymer Polymers 0.000 claims description 13
- RGCKGOZRHPZPFP-UHFFFAOYSA-N alizarin Chemical compound C1=CC=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1 RGCKGOZRHPZPFP-UHFFFAOYSA-N 0.000 claims description 12
- 150000008040 ionic compounds Chemical class 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 11
- FRPHFZCDPYBUAU-UHFFFAOYSA-N Bromocresolgreen Chemical compound CC1=C(Br)C(O)=C(Br)C=C1C1(C=2C(=C(Br)C(O)=C(Br)C=2)C)C2=CC=CC=C2S(=O)(=O)O1 FRPHFZCDPYBUAU-UHFFFAOYSA-N 0.000 claims description 10
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 9
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical group O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 9
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 9
- 239000000194 fatty acid Substances 0.000 claims description 9
- 229930195729 fatty acid Natural products 0.000 claims description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 8
- 239000002356 single layer Substances 0.000 claims description 8
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Natural products OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims description 6
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 6
- UAOMVDZJSHZZME-UHFFFAOYSA-N diisopropylamine Chemical compound CC(C)NC(C)C UAOMVDZJSHZZME-UHFFFAOYSA-N 0.000 claims description 6
- 230000000694 effects Effects 0.000 claims description 6
- 150000004665 fatty acids Chemical class 0.000 claims description 6
- GNBHRKFJIUUOQI-UHFFFAOYSA-N fluorescein Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC=C(O)C=C1OC1=CC(O)=CC=C21 GNBHRKFJIUUOQI-UHFFFAOYSA-N 0.000 claims description 6
- GVKCHTBDSMQENH-UHFFFAOYSA-L phloxine B Chemical compound [Na+].[Na+].[O-]C(=O)C1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1C1=C2C=C(Br)C(=O)C(Br)=C2OC2=C(Br)C([O-])=C(Br)C=C21 GVKCHTBDSMQENH-UHFFFAOYSA-L 0.000 claims description 6
- CQPFMGBJSMSXLP-UHFFFAOYSA-M acid orange 7 Chemical compound [Na+].OC1=CC=C2C=CC=CC2=C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 CQPFMGBJSMSXLP-UHFFFAOYSA-M 0.000 claims description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 5
- UHGIMQLJWRAPLT-UHFFFAOYSA-N octadecyl dihydrogen phosphate Chemical group CCCCCCCCCCCCCCCCCCOP(O)(O)=O UHGIMQLJWRAPLT-UHFFFAOYSA-N 0.000 claims description 5
- 235000010215 titanium dioxide Nutrition 0.000 claims description 5
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 4
- AXDJCCTWPBKUKL-UHFFFAOYSA-N 4-[(4-aminophenyl)-(4-imino-3-methylcyclohexa-2,5-dien-1-ylidene)methyl]aniline;hydron;chloride Chemical compound Cl.C1=CC(=N)C(C)=CC1=C(C=1C=CC(N)=CC=1)C1=CC=C(N)C=C1 AXDJCCTWPBKUKL-UHFFFAOYSA-N 0.000 claims description 4
- SGHZXLIDFTYFHQ-UHFFFAOYSA-L Brilliant Blue Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 SGHZXLIDFTYFHQ-UHFFFAOYSA-L 0.000 claims description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
- DNEHKUCSURWDGO-UHFFFAOYSA-N aluminum sodium Chemical compound [Na].[Al] DNEHKUCSURWDGO-UHFFFAOYSA-N 0.000 claims description 4
- 235000012745 brilliant blue FCF Nutrition 0.000 claims description 4
- 239000004161 brilliant blue FCF Substances 0.000 claims description 4
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 4
- 239000000920 calcium hydroxide Substances 0.000 claims description 4
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 4
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 4
- SEACYXSIPDVVMV-UHFFFAOYSA-L eosin Y Chemical compound [Na+].[Na+].[O-]C(=O)C1=CC=CC=C1C1=C2C=C(Br)C(=O)C(Br)=C2OC2=C(Br)C([O-])=C(Br)C=C21 SEACYXSIPDVVMV-UHFFFAOYSA-L 0.000 claims description 4
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 4
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 4
- 239000000347 magnesium hydroxide Substances 0.000 claims description 4
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 4
- 239000001630 malic acid Substances 0.000 claims description 4
- 235000011090 malic acid Nutrition 0.000 claims description 4
- KJFMBFZCATUALV-UHFFFAOYSA-N phenolphthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2C(=O)O1 KJFMBFZCATUALV-UHFFFAOYSA-N 0.000 claims description 4
- CPRMKOQKXYSDML-UHFFFAOYSA-M rubidium hydroxide Chemical compound [OH-].[Rb+] CPRMKOQKXYSDML-UHFFFAOYSA-M 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- 239000004408 titanium dioxide Substances 0.000 claims description 4
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 4
- CPBJMKMKNCRKQB-UHFFFAOYSA-N 3,3-bis(4-hydroxy-3-methylphenyl)-2-benzofuran-1-one Chemical compound C1=C(O)C(C)=CC(C2(C3=CC=CC=C3C(=O)O2)C=2C=C(C)C(O)=CC=2)=C1 CPBJMKMKNCRKQB-UHFFFAOYSA-N 0.000 claims description 3
- MPVDXIMFBOLMNW-ISLYRVAYSA-N 7-hydroxy-8-[(E)-phenyldiazenyl]naphthalene-1,3-disulfonic acid Chemical compound OC1=CC=C2C=C(S(O)(=O)=O)C=C(S(O)(=O)=O)C2=C1\N=N\C1=CC=CC=C1 MPVDXIMFBOLMNW-ISLYRVAYSA-N 0.000 claims description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- YKTSYUJCYHOUJP-UHFFFAOYSA-N [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] Chemical compound [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] YKTSYUJCYHOUJP-UHFFFAOYSA-N 0.000 claims description 3
- 235000011054 acetic acid Nutrition 0.000 claims description 3
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 claims description 3
- 229940052223 basic fuchsin Drugs 0.000 claims description 3
- 235000012730 carminic acid Nutrition 0.000 claims description 3
- 239000004106 carminic acid Substances 0.000 claims description 3
- 229940080423 cochineal Drugs 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 3
- OBRMNDMBJQTZHV-UHFFFAOYSA-N cresol red Chemical compound C1=C(O)C(C)=CC(C2(C3=CC=CC=C3S(=O)(=O)O2)C=2C=C(C)C(O)=CC=2)=C1 OBRMNDMBJQTZHV-UHFFFAOYSA-N 0.000 claims description 3
- ZBQZBWKNGDEDOA-UHFFFAOYSA-N eosin B Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC([N+]([O-])=O)=C(O)C(Br)=C1OC1=C2C=C([N+]([O-])=O)C(O)=C1Br ZBQZBWKNGDEDOA-UHFFFAOYSA-N 0.000 claims description 3
- ZUVCYFMOHFTGDM-UHFFFAOYSA-N hexadecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCCCCCOP(O)(O)=O ZUVCYFMOHFTGDM-UHFFFAOYSA-N 0.000 claims description 3
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 3
- 239000011976 maleic acid Substances 0.000 claims description 3
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical compound [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 claims description 3
- HWPKGOGLCKPRLZ-UHFFFAOYSA-M monosodium citrate Chemical compound [Na+].OC(=O)CC(O)(C([O-])=O)CC(O)=O HWPKGOGLCKPRLZ-UHFFFAOYSA-M 0.000 claims description 3
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 3
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 3
- 239000001488 sodium phosphate Substances 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 3
- KLCDQSGLLRINHY-UHFFFAOYSA-N 1-phenyldiazenylnaphthalen-2-amine Chemical compound NC1=CC=C2C=CC=CC2=C1N=NC1=CC=CC=C1 KLCDQSGLLRINHY-UHFFFAOYSA-N 0.000 claims description 2
- RUDINRUXCKIXAJ-UHFFFAOYSA-N 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,14-heptacosafluorotetradecanoic acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F RUDINRUXCKIXAJ-UHFFFAOYSA-N 0.000 claims description 2
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 claims description 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 2
- MFGOFGRYDNHJTA-UHFFFAOYSA-N 2-amino-1-(2-fluorophenyl)ethanol Chemical compound NCC(O)C1=CC=CC=C1F MFGOFGRYDNHJTA-UHFFFAOYSA-N 0.000 claims description 2
- MRDOFVRMTNWMDA-UHFFFAOYSA-N 2-bromo-4-[3-(3-bromo-4-hydroxy-2,5-dimethylphenyl)-1,1-dioxo-2,1$l^{6}-benzoxathiol-3-yl]-3,6-dimethylphenol Chemical compound BrC1=C(O)C(C)=CC(C2(C3=CC=CC=C3S(=O)(=O)O2)C=2C(=C(Br)C(O)=C(C)C=2)C)=C1C MRDOFVRMTNWMDA-UHFFFAOYSA-N 0.000 claims description 2
- MDGFKZKMIQQRPU-UHFFFAOYSA-N 2-bromo-4-[3-(3-bromo-5-chloro-4-hydroxyphenyl)-1,1-dioxo-2,1$l^{6}-benzoxathiol-3-yl]-6-chlorophenol Chemical compound C1=C(Br)C(O)=C(Cl)C=C1C1(C=2C=C(Br)C(O)=C(Cl)C=2)C2=CC=CC=C2S(=O)(=O)O1 MDGFKZKMIQQRPU-UHFFFAOYSA-N 0.000 claims description 2
- RTZZCYNQPHTPPL-UHFFFAOYSA-N 3-nitrophenol Chemical compound OC1=CC=CC([N+]([O-])=O)=C1 RTZZCYNQPHTPPL-UHFFFAOYSA-N 0.000 claims description 2
- JCYPECIVGRXBMO-UHFFFAOYSA-N 4-(dimethylamino)azobenzene Chemical compound C1=CC(N(C)C)=CC=C1N=NC1=CC=CC=C1 JCYPECIVGRXBMO-UHFFFAOYSA-N 0.000 claims description 2
- ZPLCXHWYPWVJDL-UHFFFAOYSA-N 4-[(4-hydroxyphenyl)methyl]-1,3-oxazolidin-2-one Chemical compound C1=CC(O)=CC=C1CC1NC(=O)OC1 ZPLCXHWYPWVJDL-UHFFFAOYSA-N 0.000 claims description 2
- MGUKYHHAGPFJMC-UHFFFAOYSA-N 4-[3-(4-hydroxy-2,5-dimethylphenyl)-1,1-dioxo-2,1$l^{6}-benzoxathiol-3-yl]-2,5-dimethylphenol Chemical compound C1=C(O)C(C)=CC(C2(C3=CC=CC=C3S(=O)(=O)O2)C=2C(=CC(O)=C(C)C=2)C)=C1C MGUKYHHAGPFJMC-UHFFFAOYSA-N 0.000 claims description 2
- OLQIKGSZDTXODA-UHFFFAOYSA-N 4-[3-(4-hydroxy-2-methylphenyl)-1,1-dioxo-2,1$l^{6}-benzoxathiol-3-yl]-3-methylphenol Chemical compound CC1=CC(O)=CC=C1C1(C=2C(=CC(O)=CC=2)C)C2=CC=CC=C2S(=O)(=O)O1 OLQIKGSZDTXODA-UHFFFAOYSA-N 0.000 claims description 2
- MCTQNEBFZMBRSQ-GEEYTBSJSA-N Chrysoidine Chemical compound Cl.NC1=CC(N)=CC=C1\N=N\C1=CC=CC=C1 MCTQNEBFZMBRSQ-GEEYTBSJSA-N 0.000 claims description 2
- RZSYLLSAWYUBPE-UHFFFAOYSA-L Fast green FCF Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC(O)=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 RZSYLLSAWYUBPE-UHFFFAOYSA-L 0.000 claims description 2
- 229910021577 Iron(II) chloride Inorganic materials 0.000 claims description 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 2
- 229920003091 Methocel™ Polymers 0.000 claims description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- BELBBZDIHDAJOR-UHFFFAOYSA-N Phenolsulfonephthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2S(=O)(=O)O1 BELBBZDIHDAJOR-UHFFFAOYSA-N 0.000 claims description 2
- 239000004111 Potassium silicate Substances 0.000 claims description 2
- 239000004115 Sodium Silicate Substances 0.000 claims description 2
- LDKDGDIWEUUXSH-UHFFFAOYSA-N Thymophthalein Chemical compound C1=C(O)C(C(C)C)=CC(C2(C3=CC=CC=C3C(=O)O2)C=2C(=CC(O)=C(C(C)C)C=2)C)=C1C LDKDGDIWEUUXSH-UHFFFAOYSA-N 0.000 claims description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 2
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 2
- 229910052916 barium silicate Inorganic materials 0.000 claims description 2
- HMOQPOVBDRFNIU-UHFFFAOYSA-N barium(2+);dioxido(oxo)silane Chemical compound [Ba+2].[O-][Si]([O-])=O HMOQPOVBDRFNIU-UHFFFAOYSA-N 0.000 claims description 2
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 claims description 2
- 229960001506 brilliant green Drugs 0.000 claims description 2
- UDSAIICHUKSCKT-UHFFFAOYSA-N bromophenol blue Chemical compound C1=C(Br)C(O)=C(Br)C=C1C1(C=2C=C(Br)C(O)=C(Br)C=2)C2=CC=CC=C2S(=O)(=O)O1 UDSAIICHUKSCKT-UHFFFAOYSA-N 0.000 claims description 2
- HUCVOHYBFXVBRW-UHFFFAOYSA-M caesium hydroxide Inorganic materials [OH-].[Cs+] HUCVOHYBFXVBRW-UHFFFAOYSA-M 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 235000010216 calcium carbonate Nutrition 0.000 claims description 2
- 239000000378 calcium silicate Substances 0.000 claims description 2
- 229910052918 calcium silicate Inorganic materials 0.000 claims description 2
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 claims description 2
- MEAHOQPOZNHISZ-UHFFFAOYSA-M cesium;hydrogen sulfate Chemical compound [Cs+].OS([O-])(=O)=O MEAHOQPOZNHISZ-UHFFFAOYSA-M 0.000 claims description 2
- OIQPTROHQCGFEF-UHFFFAOYSA-L chembl1371409 Chemical compound [Na+].[Na+].OC1=CC=C2C=C(S([O-])(=O)=O)C=CC2=C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 OIQPTROHQCGFEF-UHFFFAOYSA-L 0.000 claims description 2
- CEZCCHQBSQPRMU-UHFFFAOYSA-L chembl174821 Chemical compound [Na+].[Na+].COC1=CC(S([O-])(=O)=O)=C(C)C=C1N=NC1=C(O)C=CC2=CC(S([O-])(=O)=O)=CC=C12 CEZCCHQBSQPRMU-UHFFFAOYSA-L 0.000 claims description 2
- XBLIFEQTVVSTIM-UHFFFAOYSA-L chembl2105392 Chemical compound [Na+].[Na+].[O-]S(=O)(=O)C1=CC2=CC(S([O-])(=O)=O)=CC=C2C(O)=C1N=NC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O XBLIFEQTVVSTIM-UHFFFAOYSA-L 0.000 claims description 2
- ONTQJDKFANPPKK-UHFFFAOYSA-L chembl3185981 Chemical compound [Na+].[Na+].CC1=CC(C)=C(S([O-])(=O)=O)C=C1N=NC1=CC(S([O-])(=O)=O)=C(C=CC=C2)C2=C1O ONTQJDKFANPPKK-UHFFFAOYSA-L 0.000 claims description 2
- WWAABJGNHFGXSJ-UHFFFAOYSA-N chlorophenol red Chemical compound C1=C(Cl)C(O)=CC=C1C1(C=2C=C(Cl)C(O)=CC=2)C2=CC=CC=C2S(=O)(=O)O1 WWAABJGNHFGXSJ-UHFFFAOYSA-N 0.000 claims description 2
- GVPFVAHMJGGAJG-UHFFFAOYSA-L cobalt dichloride Chemical compound [Cl-].[Cl-].[Co+2] GVPFVAHMJGGAJG-UHFFFAOYSA-L 0.000 claims description 2
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- DWCZIOOZPIDHAB-UHFFFAOYSA-L methyl green Chemical compound [Cl-].[Cl-].C1=CC(N(C)C)=CC=C1C(C=1C=CC(=CC=1)[N+](C)(C)C)=C1C=CC(=[N+](C)C)C=C1 DWCZIOOZPIDHAB-UHFFFAOYSA-L 0.000 claims description 2
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- CTIQLGJVGNGFEW-UHFFFAOYSA-L naphthol yellow S Chemical compound [Na+].[Na+].C1=C(S([O-])(=O)=O)C=C2C([O-])=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 CTIQLGJVGNGFEW-UHFFFAOYSA-L 0.000 claims description 2
- PGSADBUBUOPOJS-UHFFFAOYSA-N neutral red Chemical compound Cl.C1=C(C)C(N)=CC2=NC3=CC(N(C)C)=CC=C3N=C21 PGSADBUBUOPOJS-UHFFFAOYSA-N 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 2
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- OXNIZHLAWKMVMX-UHFFFAOYSA-N picric acid Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-N 0.000 claims description 2
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- CHKVPAROMQMJNQ-UHFFFAOYSA-M potassium bisulfate Chemical compound [K+].OS([O-])(=O)=O CHKVPAROMQMJNQ-UHFFFAOYSA-M 0.000 claims description 2
- 229910000343 potassium bisulfate Inorganic materials 0.000 claims description 2
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 claims description 2
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- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims description 2
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- KXXXUIKPSVVSAW-UHFFFAOYSA-K pyranine Chemical compound [Na+].[Na+].[Na+].C1=C2C(O)=CC(S([O-])(=O)=O)=C(C=C3)C2=C2C3=C(S([O-])(=O)=O)C=C(S([O-])(=O)=O)C2=C1 KXXXUIKPSVVSAW-UHFFFAOYSA-K 0.000 claims description 2
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- FZUOVNMHEAPVBW-UHFFFAOYSA-L quinoline yellow ws Chemical compound [Na+].[Na+].O=C1C2=CC=CC=C2C(=O)C1C1=NC2=C(S([O-])(=O)=O)C=C(S(=O)(=O)[O-])C=C2C=C1 FZUOVNMHEAPVBW-UHFFFAOYSA-L 0.000 claims description 2
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- ZHFPEICFUVWJIS-UHFFFAOYSA-M sodium 2-hydroxy-5-[(3-nitrophenyl)diazenyl]benzoate Chemical compound [Na+].Oc1ccc(cc1C([O-])=O)N=Nc1cccc(c1)[N+]([O-])=O ZHFPEICFUVWJIS-UHFFFAOYSA-M 0.000 claims description 2
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- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 2
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- PODWXQQNRWNDGD-UHFFFAOYSA-L sodium thiosulfate pentahydrate Chemical compound O.O.O.O.O.[Na+].[Na+].[O-]S([S-])(=O)=O PODWXQQNRWNDGD-UHFFFAOYSA-L 0.000 claims description 2
- GNTPCYMJCJNRQB-UHFFFAOYSA-M sodium;2-[[4-(dimethylamino)phenyl]diazenyl]benzoate Chemical compound [Na+].C1=CC(N(C)C)=CC=C1N=NC1=CC=CC=C1C([O-])=O GNTPCYMJCJNRQB-UHFFFAOYSA-M 0.000 claims description 2
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- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims description 2
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- OORQUAGUOJMPCS-UHFFFAOYSA-N 4-[[4-(diethylamino)phenyl]diazenyl]benzenesulfonic acid Chemical compound C1=CC(N(CC)CC)=CC=C1N=NC1=CC=C(S(O)(=O)=O)C=C1 OORQUAGUOJMPCS-UHFFFAOYSA-N 0.000 claims 1
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims 1
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- COEZWFYORILMOM-UHFFFAOYSA-N sodium 4-[(2,4-dihydroxyphenyl)diazenyl]benzenesulfonic acid Chemical compound [Na+].OC1=CC(O)=CC=C1N=NC1=CC=C(S(O)(=O)=O)C=C1 COEZWFYORILMOM-UHFFFAOYSA-N 0.000 claims 1
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- GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical compound [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 description 1
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- XOSXWYQMOYSSKB-UHFFFAOYSA-L water blue Chemical compound [Na+].[Na+].[O-]S(=O)(=O)C1=C(N)C(C)=CC(C(=C2C=CC(C=C2)=NC=2C=CC(=CC=2)S([O-])(=O)=O)C=2C=CC(NC=3C=CC(=CC=3)S(O)(=O)=O)=CC=2)=C1 XOSXWYQMOYSSKB-UHFFFAOYSA-L 0.000 description 1
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Classifications
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/56—Wetness-indicators or colourants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61F—FILTERS IMPLANTABLE INTO BLOOD VESSELS; PROSTHESES; DEVICES PROVIDING PATENCY TO, OR PREVENTING COLLAPSING OF, TUBULAR STRUCTURES OF THE BODY, e.g. STENTS; ORTHOPAEDIC, NURSING OR CONTRACEPTIVE DEVICES; FOMENTATION; TREATMENT OR PROTECTION OF EYES OR EARS; BANDAGES, DRESSINGS OR ABSORBENT PADS; FIRST-AID KITS
- A61F13/00—Bandages or dressings; Absorbent pads
- A61F13/15—Absorbent pads, e.g. sanitary towels, swabs or tampons for external or internal application to the body; Supporting or fastening means therefor; Tampon applicators
- A61F13/42—Absorbent pads, e.g. sanitary towels, swabs or tampons for external or internal application to the body; Supporting or fastening means therefor; Tampon applicators with wetness indicator or alarm
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/50—Sympathetic, colour changing or similar inks
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/28—Web or sheet containing structurally defined element or component and having an adhesive outermost layer
- Y10T428/2813—Heat or solvent activated or sealable
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
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Landscapes
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- Compositions Of Macromolecular Compounds (AREA)
Description
「吸収性物品」とは、身体の排出物を吸収及び収容するデバイスを指し、より詳細には、着用者の身体に接してあるいは、近接して配置されて、身体から排出される様々な排出物を吸収し、収容するデバイスを指す。吸収性物品としては、おむつ、トレーニングパンツ、成人用失禁下着、女性用衛生製品、胸パッド、ケアマット、よだれ掛け、創傷包帯製品、及び同種のものを挙げることができる。本明細書で使用するところの「体液」又は「身体排出物」なる用語には、これらに限定されるものではないが、尿、血液、膣排泄物、母乳、汗及び糞便が含まれる。
結合剤は、液体活性化着色剤、又は着色剤の組み合わせを、マトリックス内で不動化して着色剤がおむつのコア又は吸収性物品のその他の領域内に浸出するのを妨害するいかなる材料であってもよい。色のコントラスト及び鮮やかさを最適化するためには、尿等の液体と接触する前後に、着色剤をマトリックス内に「閉じ込める」ことが非常に好ましい。結合剤は、着色剤がマトリックスの外部へ浸出するのを妨害するだけでなく、液体活性化処方物全体が吸収性物品の構成要素に結合するのを助けることもできる。例えば、結合剤は、おむつバックシートの表面と液体活性化処方物との間に強力な結合を形成するのを助けることができる。本発明の液体活性化処方物のホットメルト結合マトリックス又は溶媒系結合マトリックスに結合剤として使用するのに好適となり得る様々な材料が存在する。
いくつかの実施形態では、結合剤はホットメルト接着剤であってもよく、いくつかの実施形態では、溶媒系結合マトリックスであってもよい。ホットメルト接着剤結合マトリックスの追加成分としては、ベースポリマー、粘着付与剤、ワックス、ゴム、溶媒、湿潤剤、及び/又は酸化防止剤が挙げられる。ホットメルト接着剤に使用されるベースポリマーの例としては、エチレン−酢酸ビニル(EVA)コポリマー;エチレン−アクリル酸コポリマー;エチレン−酢酸ビニル−無水マレイン酸ターポリマー;エチレン−アクリル酸−無水マレイン酸ターポリマー;低密度及び高密度ポリエチレンのようなポリオレフィン、アタクチックポリプロピレン、酸化ポリエチレン、ポリブテン−1;非晶質ポリオレフィン、例えば非晶質アタクチックプロピレン(APP)、非晶質プロピレン/エチレン(APE)、非晶質プロピレン/ブタン(APB)、非晶質プロピレン/ヘキサン(APH)、及び非晶質プロピレン/エチレン/ブタン;ポリアミド;スチレンブロックコポリマー(SBC);スチレン/アクリル酸ポリマー及び変性スチレン/アクリル酸ポリマー;ポリカーボネート;シリコーンゴム;ポリピロール系ポリマー;熱可塑性エラストマー、例えば天然及び合成ポリイソプレン、ポリブタジエンゴム、ブチルゴム、クロロプレンゴム、エチレン−プロピレンゴム、エピクロロヒドリンゴム、ポリアクリルゴム、ポリエーテルブロックアミド;アクリル酸のポリマー、アルキド樹脂、アミド、アミノ樹脂、エチレン−コ−ターポリマー樹脂、例えばEVA、エポキシ樹脂、フルオロポリマー、炭化水素樹脂、フェノール、ポリエステル、オレフィン、ポリウレタン、シリコーン及び官能化シリコーン、ポリスチレン及びポリビニルが挙げられる。
本発明で使用される液体活性化処方物は、液体活性化着色剤を含む。着色剤は、染料、インク、顔料、又はpHインジケータであってもよい。液体活性化着色剤は、湿り度インジケータ組成物中で可溶性であり得るものであり、特定の場合には、湿り度インジケータ組成物内に着色剤を均質に懸濁又は分散するのに好適であり得る。前述したように、着色剤は水又は尿と接触すると変色する。いくつかの実施形態において、液体活性化処方物は、水又は尿と接触したときに変色しない永久着色剤を更に含んでもよい。
水発色性イオン化合物は一般的に、イオン化塩のような反応性イオン化合物である。本発明の実施に使用できる水発色性イオン化合物のいくつかの代表例としては、硫酸水素リチウム、炭酸水素リチウム、硫酸水素カリウム、炭酸水素カリウム、硫酸水素ルビジウム、炭酸水素ルビジウム、硫酸水素セシウム、炭酸水素セシウム、硫酸水素ナトリウム、炭酸水素ナトリウム、炭酸ナトリウム、水酸化セシウム、水酸化リチウム、水酸化カリウム、水酸化カルシウム、水酸化マグネシウム、チオ硫酸ナトリウム五水和物、水酸化ナトリウム、水酸化ルビジウム、塩化コバルト、硝酸コバルト、硫酸銅、硝酸銅、硫酸鉄(II)、硫酸鉄(III)、塩化鉄(II)、塩化鉄(III)、クエン酸、クエン酸二水素一ナトリウム、クエン酸水素二ナトリウム、クエン酸三ナトリウム、グルコン酸、グルコン酸ナトリウム、グリコール酸、グリコール酸ナトリウム、リンゴ酸、リンゴ酸ナトリウム、マレイン酸、マレイン酸ナトリウム、酢酸、リン酸、リン酸三ナトリウム、リン酸二水素ナトリウム、リン酸一水素二ナトリウム、リン酸モノステアリル、リン酸モノセチル、クエン酸モノステアリル、塩化水素酸、硝酸、硫酸及びこれらの組み合わせが挙げられる。
本発明の液体活性化処方物に使用できる乳白剤は、ポロシゲンであっても抗ポロシゲンであってもよく、一般的には乾燥固体状態にあるとき(インク処方に組み込まれる前)に白色粉末である。乳白剤がポロシゲンとして作用する場合、乳白剤は、基材に塗布されたコーティング(例えば、おむつの外層に印刷されたコーティング)を通して液体を透過させる。換言すれば、ポロシゲンは、液体がその中を通過することができ、コーティングを通した液体の透過を促進する化合物である。抗ポロシゲンの場合、液体透過は、液体遮蔽材料の構造を破壊することによって抗ポロシゲンに近接して形成される液体透過性の隙間によって達成される。換言すれば、抗ポロシゲンは、コーティングを通して液体を流すことができるようにするサイズ及び構造の孔を乾燥コーティング構造内に存在させる。利用可能な乳白剤のいくつかの代表例としては、二酸化チタン、炭酸カルシウム、水酸化カルシウム、ケイ酸ナトリウム、ケイ酸カリウム、シリカ、デンプン、エトセル、メトセル、炭酸バリウム、ケイ酸バリウム、ケイ酸カルシウム、ケイ酸アルミニウム、水酸化アルミニウム、酸化亜鉛、EvonikのSipernat(商標)820aのようなケイ酸アルミニウムナトリウム、ケイ酸ジルコニウム、ケイ酸アルミニウムマグネシウム、及び酸化アルミニウムが挙げられる。好適な高分子乳白剤としては、Rohm and HaasからのOpulyn(商標)301、同じくRohm and HaasからのSunSphere(商標)シリーズのようなスチレン/アクリレートコポリマーが挙げられる。
本発明は、界面活性剤を包含する。本発明に好適な界面活性剤としては、例えば、当該技術分野で既知のように、tergitol、エトキシル化アルコール、脂肪族アルコール、高分子量アルコール、エステル、ポリマー及びその他の天然及び合成ワックス又はオレフィン性材料;アニオン性及びカチオン性界面活性剤、PEG−20ステアレートのようなアルコキシル化アルキレート、末端キャップされたアルコキシル化アルコール、PEG−30グリセリルステアレートのようなアルコキシル化グリセリル及びポリグリセリルアルキレート、グリセリルステアレートのようなグリセリルアルキレート、アルコキシル化硬化ヒマシ油、アルコキシル化ラノリン及び水素添加ラノリン、アルコキシル化ソルビタンアルキレート、アルキルグリコシド及び糖エステルのような糖誘導界面活性剤、ポロキサマー、ポリソルベート、及びスルホコハク酸アルキルエステルが挙げられる。更なる例としては、非イオン性界面活性剤及び両性界面活性剤並びにこれらの組み合わせ、UniqemaからMONOWET MOE75として入手可能な特定のジエチルヘキシルスルホコハク酸ナトリウムが挙げられる。別の例は、4−1−アミノエチルフェノールポリオキシエチレン脂肪エーテル、ポリオキシエチレンソルビタンエステル、及びポリオキシエチレン脂肪酸エステルである。界面活性剤は、液体活性化処方物の約3重量%〜約8重量%含まれてもよい。
追加成分としては、例えば、安定剤、界面活性剤、構造補助剤、及び/又は溶媒が挙げられる。存在する場合、このような追加成分は、典型的には、例えば組成物の約0.001重量%〜約50重量%、約0.1重量%〜約40重量%、又は約1重量%〜約35重量%のような、成分の効果をもたらすのに有効な濃度で組成物中に用いられる。溶媒としては、液体、ゲル又は半固体材料が挙げられる。溶媒は、水、揺変性材料、ペースト、アルコール、エチレングリコールモノブチルエーテル、鉱物油、エステル、シリコーン流体、イソパラフィン、ヘキサン等のアルカン、トルエン、キシレン、PEG−200のような低分子量ポリエチレングリコール、グリセリン、グリコール、不燃性溶媒、接着剤、又はその他の有機種であってもよい。好ましい非水性溶媒は、アルコール、アセテート、及びこれらの組み合わせを含んでもよい。アルコール溶媒は、好ましくは、イソプロピルアルコール、n−プロピルアルコール、エタノール、メタノール、及びこれらの組み合わせからなる群から選択される。同様に、好適なアセテート溶媒としては、限定するものではないが、イソプロピルアセテート、n−プロピルアセテート、及びこれらの組み合わせが挙げられる。
本発明の一実施形態では、本発明の液体活性化処方物は、基材上及び/又は基材中にあってもよい。基材上に存在する場合、液体活性化処方物は、典型的に、水、尿、経血、血液等の液体と接触する基材上及び/又は基材中にある。基材としては、限定するものではないが、構造成分、例えば、織布、不織布、フィルム、スポンジ、及びこれらの組み合わせが挙げられる。基材は、合成材料及び/又は天然材料を含んでよい。本発明の一実施形態では、任意の基材は、連続不織布のようにそれ自体で物品であってよい。本発明の別の実施形態では、液体活性化処方物が適用されてもよい、又は別の方法で付着されてもよい基材は、バックシート、トップシート、締結具、吸収材料等が挙げられるが、これらに限定されない吸収性物品の構造要素の任意の1つ又はこれらの組み合わせを含むか、又は製品に追加若しくは適用される別個の要素であってよい。本発明の任意の一実施形態では、液体活性化処方物は、吸収性物品の全体に適用される。いくつかの実施形態において、液体活性化処方物は単一層である。このような単一層は、基材又は構造成分に適用されてもよい。いくつかの実施形態では、単一層処方は、バックシートと吸収性コアとの間に配置されてもよく、他の実施形態では、トップシートと吸収性コアとの間に配置されてもよい。
室温で固体である成分は、最初に約90℃の温度で溶融される。こうした成分には、結合剤、ホットメルト接着剤、ワックス、界面活性剤、及び酸化防止剤のような任意成分が包含される。一般的に、これらの成分を溶融するためには、約80℃〜100℃の温度が必要である。ホットプレート上で液体状態に溶融した後、IKA RW−20(又は類似のミキサー)のようなプロペラミキサーを用いて、混合物が均質になるまで材料を十分に混合する。この混合物を加熱及び混合し続けながら、ケイ酸アルミニウムナトリウム粉末を組成物に均質に混合する。次に、加熱を続けながら、水発色性イオン化合物、炭酸水素ナトリウムを組成物に混合する。最後に、ブロモクレゾールグリーン(遊離酸)のような着色剤を、混合物が均質になるまで組成物に混合する。ワイヤーコーターを用いてフィルムを作製するために組成物に加熱を続けてもよく、又は組成物を室温まで冷却して更に使用してもよい。
Claims (14)
- (A)液体活性化着色剤と、(B)水発色性イオン化合物と、(C)乳白剤と、(D)結合マトリックスと、(E)界面活性剤と、を含む、単一層液体活性化処方物であって、
前記乳白剤が、二酸化チタン、炭酸カルシウム、水酸化カルシウム、ケイ酸ナトリウム、ケイ酸カリウム、シリカ、デンプン、エトセル、メトセル、炭酸バリウム、ケイ酸バリウム、ケイ酸カルシウム、ケイ酸アルミニウム、水酸化アルミニウム、酸化アルミニウム、ケイ酸アルミニウムナトリウム、ケイ酸ジルコニウム、ケイ酸アルミニウムマグネシウム、及びスチレン/アクリレートコポリマーからなる群から選択され、
前記液体活性化処方物の総重量を基準にして、前記乳白剤が20重量%〜45重量%の範囲内の量で前記液体活性化処方物中に存在する、液体活性化処方物。 - 1重量%〜30重量%の界面活性剤を含む、請求項1に記載の液体活性化処方物。
- 前記界面活性剤がtergitol(登録商標)である、請求項1に記載の液体活性化処方物。
- 前記結合マトリックスがホットメルト結合マトリックスである、請求項1に記載の液体活性化処方物。
- 永久着色剤を更に含む、請求項1に記載の液体活性化処方物。
- 安定剤及び/又は構造補助剤からなる群から選択される1つ以上を更に含む、請求項1に記載の液体活性化処方物。
- 前記安定剤が、リン酸モノステアリル、クエン酸エステル、アルコールエトキシカルボキシレート、グリコール酸エステル、乳酸エステル、脂肪酸、エーテルカルボン酸、脂肪酸メチルエステル、硫酸エステル、クエン酸及びリンゴ酸のような果実酸、硫酸のような無機酸、モノエタノールアミン、ジエタノールアミン、トリエタノールアミン、ジプロピレントリアミン、ジイソプロピルアミン、1,3−ビス(メチルアミン)−シクロヘキサン、1,3ペンタンジアミン、水酸化ナトリウム、水酸化マグネシウム、及びこれらの組み合わせからなる群から選択される、請求項6に記載の液体活性化処方物。
- 請求項1の液体活性化処方物を含む吸収性物品であって、前記液体活性化処方物が吸収性物品の構造要素に固定される、吸収性物品。
- 請求項1の液体活性化処方物を含む吸収性物品であって、該物品が、バックシートと、トップシートと、前記バックシートと前記トップシートとの間に配置された吸収性コアと、を含み、前記液体活性化処方物が、単一層であり、かつ前記バックシートと前記吸収性コアとの間に配置されている、吸収性物品。
- 請求項1の液体活性化処方物を含む吸収性物品であって、該物品が、バックシートと、トップシートと、前記バックシートと前記トップシートとの間に配置された吸収性コアと、を含み、前記液体活性化処方物が、単一層であり、かつ前記トップシートと前記吸収性コアとの間に配置されている、吸収性物品。
- 前記液体活性化着色剤が、マラカイトグリーン、ブリリアントグリーン、クリスタルバイオレット、エリトロシンB、メチルグリーン、メチルバイオレット2D、ピクリン酸、ナフトールイエローS、キナルジンレッド、エオシンY、メタニルイエロー、m−クレゾールパープル、チモールブルー、キシレノールブルー、塩基性フクシン、エオシンB、4−p−アミノフェノール(アゾ)ベンゼンスルホン酸ナトリウム塩、クレゾールレッド、マルチウスイエロー、フロキシンB、メチルイエロー、ブロモフェノールブルー、コンゴレッド、メチルオレンジ、ブロモクロロフェノールブルー(水溶性又は遊離酸型)、エチルオレンジ、フルオレセインWS、ブロモクレゾールグリーン、クリソイジン、メチルレッドナトリウム塩、アリザリンレッドS−H2O、コチニール、クロロフェノールレッド、ブロモクレゾールパープル、4−ナフサ、アリザリン、ニトラジンイエロー、ブロモチモールブルー、ブリリアントイエロー、ニュートラルレッド、ロゾール酸、フェノールレッド、3−ニトロフェノール、オレンジII、フェノールフタレイン、o−クレゾールフタレイン、ナイルブルーA、チモールフタレイン、アニリンブルーWS、アリザリンイエローGG、モルダントオレンジ、トロペオリンO、オレンジG、酸性フクシン、チアゾールイエローG、インジゴカルミン、FD&CブルーNo.1、FD&CブルーNo.2、FD&CグリーンNo.3、FD&CレッドNo.40、FD&CレッドNo.4、FD&CイエローNo.5、FD&CイエローNo.6、C.I.フードブルー5、及びC.I.フードレッド7、D&CイエローNo.10、D&CイエローNo.7、D&CイエローNo.2、D&CイエローNo.8、D&CオレンジNo.4、D&CレッドNo.22、D&CレッドNo.28、D&CレッドNo.33、D&CグリーンNo.8、D&CグリーンNo.5、D&CブラウンNo.1、ブロモピロガロールレッド、ブロモキシレノールブルー、メチレンブルー、モノアゾ及びこれらの任意の組み合わせからなる群から選択される、請求項1に記載の液体活性化処方物。
- 前記水発色性イオン化合物が、硫酸水素リチウム、炭酸水素リチウム、硫酸水素カリウム、炭酸水素カリウム、硫酸水素ルビジウム、炭酸水素ルビジウム、硫酸水素セシウム、炭酸水素セシウム、硫酸水素ナトリウム、炭酸水素ナトリウム、炭酸ナトリウム、水酸化セシウム、水酸化リチウム、水酸化カリウム、水酸化カルシウム、水酸化マグネシウム、チオ硫酸ナトリウム五水和物、水酸化ナトリウム、水酸化ルビジウム、塩化コバルト、硝酸コバルト、硫酸銅、硝酸銅、硫酸鉄(II)、硫酸鉄(III)、塩化鉄(II)、塩化鉄(III)、ケイ酸アンモニウムナトリウム、クエン酸、クエン酸二水素一ナトリウム、クエン酸水素二ナトリウム、クエン酸三ナトリウム、グルコン酸、グルコン酸ナトリウム、グリコール酸、グリコール酸ナトリウム、リンゴ酸、リンゴ酸ナトリウム、マレイン酸、マレイン酸ナトリウム、酢酸、リン酸、リン酸三ナトリウム、リン酸二水素ナトリウム、リン酸一水素二ナトリウム、リン酸モノステアリル、リン酸モノセチル、クエン酸モノステアリル、塩化水素酸、硝酸、硫酸、及びこれらの組み合わせからなる群から選択される、請求項1に記載の液体活性化処方物。
- 前記液体活性化処方物の総重量を基準にして、前記液体活性化着色剤が0.01重量%〜20重量%の範囲内の量で前記液体活性化処方物中に存在し、前記水発色性イオン化合物が0.05重量%〜35重量%の範囲内の量で前記液体活性化処方物中に存在し、前記乳白剤が30重量%〜40重量%の範囲内の量で前記液体活性化処方物中に存在し、前記結合マトリックスが5重量%〜75重量%の範囲内の量で前記液体活性化処方物中に存在し、前記界面活性剤が1重量%〜30重量%の範囲内の量で前記液体活性化処方物中に存在する、請求項1に記載の液体活性化処方物。
- a)着色から無着色、b)無着色から着色、c)着色から別の色、又はd)a)とb)とc)との組み合わせからなる群から選択される色遷移を有する、請求項1に記載の液体活性化処方物。
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US201361837405P | 2013-06-20 | 2013-06-20 | |
US201361837400P | 2013-06-20 | 2013-06-20 | |
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US61/837,390 | 2013-06-20 | ||
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2013
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