JP5875582B2 - 長時間持続する効果をもたらすケラチン基質に塗布するためのパーソナルケア組成物添加剤 - Google Patents
長時間持続する効果をもたらすケラチン基質に塗布するためのパーソナルケア組成物添加剤 Download PDFInfo
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- JP5875582B2 JP5875582B2 JP2013516802A JP2013516802A JP5875582B2 JP 5875582 B2 JP5875582 B2 JP 5875582B2 JP 2013516802 A JP2013516802 A JP 2013516802A JP 2013516802 A JP2013516802 A JP 2013516802A JP 5875582 B2 JP5875582 B2 JP 5875582B2
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- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
- JLGLQAWTXXGVEM-UHFFFAOYSA-N triethylene glycol monomethyl ether Chemical compound COCCOCCOCCO JLGLQAWTXXGVEM-UHFFFAOYSA-N 0.000 description 1
- YFNKIDBQEZZDLK-UHFFFAOYSA-N triglyme Chemical compound COCCOCCOCCOC YFNKIDBQEZZDLK-UHFFFAOYSA-N 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 229920003176 water-insoluble polymer Polymers 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
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Description
本出願は、2010年6月24日出願の仮出願61/358,226の利益を主張し、その全体が参照により援用される。
カチオン置換の量を決定する手順
基準として2種類の市販のリンスオフコンディショナー及び2種類の市販のリーブオンコンディショナーを、塗布したとき(リーブオン)、又は塗布し洗い流したとき(リンスオフ製品)、及び単純化したシャンプー配合物(12質量%ラウリルエーテル(2EO)硫酸ナトリウム、2質量%コカミドプロピルベタイン)によって洗浄した後で試験した。毛髪1グラム当たり0.1グラムのリーブオンコンディショナー、又は毛髪1グラム当たり0.3グラムのリンスオフコンディショナーとして製品を塗布した。使用する毛髪は、未処理の茶色の毛髪を脱色によって1時間処理することによってダメージを与えた。この毛髪をすべてのさらなる試験に使用した。シャンプーを毛髪1グラム当たり0.3グラムとして塗布し、その後すすいだ。
別の基準として、以下の組成を有する単純化した配合物を試験した。
モル置換(HE-MS)は1.5〜4.0の範囲である。
分子量がおよそ112,000ダルトンであるpolydadmac(実施例7a)の40%水溶液は、3%のセテアリルアルコールと組み合わせて1質量%の濃度で塗布した場合、上記で表10に示した比較例のより高分子量(Mw 850,000)のポリクオタニウム6よりも良好な最初のウェットコーム性能(5888gf-mm)並びに多数回のシャンプー洗浄後の良好な性能(3245gf-mm、5洗浄後)をもたらした。
結果は強力な洗浄系SLES/CAPBによる洗浄について実証する。
シャンプー、コンディショナーの用量レベル
使用した用量は毛髪1グラム当たりコンディショナーが0.3グラムであり、シャンプー洗浄についても同レベルであった。下記の表において、使用量を変化させ、コンディショナー量を減少させシャンプーの量を増加させることによって性能は悪影響を受けたが、実施例5oについて全体としての性能上の効果が見られた。
実施例5d及び実施例7aについて、発明者らは、カチオン性界面活性剤(3%の脂肪アルコールを含む系におけるステアラミドプロピルジメチルアミン)によって50%が置き換えられた、セテアリルアルコールを含む系における本発明の持続性ポリマーを比較した。洗浄はSLES/CAPBを用いて行った。
本発明のポリマーを含有するコンディショニング系の洗浄持続性は、ヘアカラーの退色を防ぐのにも有用である。毛束(3セット)を退色の問題で知られる赤色で処理した。使用したヘアカラーはHenkel Schwarzkopf社の持続性カラー: Syoss Professional Performance Permanent Coloration Mahonie Acajouであった。用いたプロセスは以下の通りであった。
・発色クリームの入った塗布用ボトルを開け、チューブから色を加え、ボトルを閉め、均質な混合物になるまで振る
・毛束の長さに沿って1分間揉み込むことにより、直ちに乾燥した毛束への染色プロセスを開始する
・毛髪をアルミニウム箔で覆い、30〜45分待つ
・水が完全に透明になるまで毛髪をマッサージすることによって水(35C)で洗い流す
・シリコーンを含まない低刺激シャンプーで洗浄する
・BYK-Gardner分光光度計を使用して色指数(L*a*b)の変化を測定する
o 全体の毛髪の色ΔL(+はより明るい)
o 赤-緑Δa(+は赤色寄り、-は緑色寄り)
o 黄-青(+は黄色寄り、-は青色寄り)
・全色差ΔE=[(ΔL)2+(Δa)2+(Δb)2]1/2
・毛束を白紙上の均等に引かれた線の間に置き、表面をより平坦にするためにその上にガラス板を置く。
・毛束の異なる場所から5回測定する
試験結果を表14に示す。
上記と同じ手順を用いる別の実施例において、実施例5lのポリマー溶液による1回のコンディショニング処理を、コンディショナー(水-グリセリン中の5lの1%溶液)による定期的処理と比較した。表15において、定期的処理(シャンプー洗浄前に毎回ポリマー溶液による処理を行う)を用いると赤色 (a値)が10〜15回の洗浄を通して一定のままであったことが示された。
下記の組成を有するカチオン性修飾したヒドロキシエチルセルロースを水/プロピレングリコール(50/50)中に1質量%で溶解させた。
実施例7aのポリマーを1質量%の活性成分として、3質量%のセテアリルアルコール及び0.75質量%のカチオン性界面活性剤と併せて使用し、水を加えて100%とした。次いで単純なコンディショナー配合物を0.05g/脱色した白人の毛髪1gで毛髪に塗布し、乾燥後に浄化用シャンプーベース(12質量%のSLE2S、2質量%のCAPB)で5回洗浄し、5回目の後に毛束を疎水性の保持性について評価した。
Claims (16)
- a) 持続性ポリマーと、
b) 水混和性の極性溶媒と
を含み、前記持続性ポリマーの濃度が0.1質量%〜20質量%の範囲であり、サイズ排除クロマトグラフィーによって決定される前記持続性ポリマーの分子量(Mw)が、50キロダルトンを上回り800キロダルトン以下までの範囲であり、前記持続性ポリマーのカチオン置換度(Cat-DS)が0.001単位を上回り、前記持続性ポリマーが、規則性の疎水性修飾ヒドロキシエチルセルロースであり、前記水混和性の極性溶媒が、ポリオールである、ケラチン表面への持続的効果をもたらすためのパーソナルケア組成物添加剤。 - 前記持続性ポリマーのカチオン置換度(Cat-DS)が0.001〜3.0の範囲である、請求項1に記載のパーソナルケア組成物添加剤。
- 前記持続性ポリマーのカチオン置換度(Cat-DS)が0.2〜3.0の範囲である、請求項2に記載のパーソナルケア組成物添加剤。
- 前記持続性ポリマーのカチオン置換度(Cat-DS)が0.4〜3.0の範囲である、請求項3に記載のパーソナルケア組成物添加剤。
- 前記水混和性の極性溶媒が、シクリトール、ジオール、グリセロール、バルサミノールB、ブタントリオール、バルサミナペンタオール、ククルバルサミノール、及びプロピレングリコールからなる群から選択されるポリオールである、請求項1に記載のパーソナルケア組成物添加剤。
- 前記水混和性の極性溶媒が水との混合物中に存在する、請求項1に記載のパーソナルケア組成物添加剤。
- 前記極性溶媒が、水と質量で10:90〜90:10の範囲の混合物中に存在する、請求項6に記載のパーソナルケア組成物添加剤。
- 前記極性溶媒が、水と質量で25:75〜75:25の範囲の混合物中に存在する、請求項7に記載のパーソナルケア組成物添加剤。
- 前記極性溶媒が、水と質量で50:50の混合物中に存在する、請求項8に記載のパーソナルケア組成物添加剤。
- 前記水混和性の極性溶媒中の前記持続性ポリマーの濃度が1.0質量%である、請求項1に記載のパーソナルケア組成物添加剤。
- 前記極性溶媒がグリセリンであり、前記持続性ポリマーの分子量(Mw)が300キロダルトンである、請求項9に記載のパーソナルケア組成物添加剤。
- a) ケラチン表面への持続的効果をもたらすためのパーソナルケア組成物添加剤と、
b) パーソナルケア活性成分と
を含むパーソナルケア組成物であって、パーソナルケア組成物添加剤が
持続性ポリマーと、
水混和性の極性溶媒と
を含み、前記持続性ポリマーの濃度が0.1質量%〜20質量%の範囲であり、サイズ排除クロマトグラフィーによって決定される前記持続性ポリマーの分子量(Mw)が、50キロダルトンを上回り800キロダルトン以下までの範囲であり、前記持続性ポリマーのカチオン置換度(Cat-DS)が0.001単位を上回り、前記持続性ポリマーが、規則性の疎水性修飾ヒドロキシエチルセルロースであり、前記水混和性の極性溶媒が、ポリオールである、パーソナルケア組成物。 - ヘアケア製品を含む、請求項12に記載のパーソナルケア組成物。
- 前記ヘアケア製品がコンディショニング系を含む、請求項13に記載のパーソナルケア組成物。
- スキンケア製品を含む、請求項12に記載のパーソナルケア組成物。
- 前記パーソナルケア組成物添加剤によってもたらされる持続的効果が、保湿、疎水性、UVA及びUVB防護からなる群から選択される、請求項15に記載のパーソナルケア組成物。
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PCT/US2011/041820 WO2011163589A2 (en) | 2010-06-24 | 2011-06-24 | Personal care composition additive for application on keratin substrates to provide long lasting benefits |
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EA030286B9 (ru) | 2012-12-27 | 2018-10-31 | Юнилевер Н.В. | Солнцезащитная композиция |
US9801900B2 (en) | 2013-11-22 | 2017-10-31 | Mary Kay Inc. | Compositions for sensitive skin |
EP3137039B1 (en) | 2014-05-02 | 2020-08-12 | Hercules LLC | Personal care composition for a keratin substrate comprising conditioning and/or styling cationic tetra polymer |
RU2736076C2 (ru) * | 2016-02-15 | 2020-11-11 | Геркулес Ллк | Бытовые химические композиции |
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EP3722329A4 (en) | 2017-12-06 | 2021-09-08 | Kao Corporation | POLYSACCHARIDE DERIVATIVE |
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US11660260B2 (en) | 2020-02-29 | 2023-05-30 | L'oreal | Compositions and methods for treating keratinous substrates |
US20230145339A1 (en) * | 2020-05-29 | 2023-05-11 | Dow Global Technologies Llc | Process for reducing hair damage upon exposure to heat |
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JPH06312915A (ja) * | 1993-04-30 | 1994-11-08 | Tsumura & Co | 毛髪処理剤 |
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FR2718961B1 (fr) * | 1994-04-22 | 1996-06-21 | Oreal | Compositions pour le lavage et le traitement des cheveux et de la peau à base de céramide et de polymères à groupements cationiques. |
US6582711B1 (en) * | 1997-01-09 | 2003-06-24 | 3M Innovative Properties Company | Hydroalcoholic compositions thickened using polymers |
SE520442C2 (sv) * | 2001-03-29 | 2003-07-08 | Akzo Nobel Nv | Användning av en kvartär ammoniumhydroxyethylcellulosaeter som balsam, kvartär ammoniumhydroxyethylcellulosaeter, process för tillverkning av cellulsaetern och komposition innehållande cellulosaetern |
EP1395233A1 (en) | 2001-06-08 | 2004-03-10 | The Procter & Gamble Company | Hair conditioning composition comprising cellulose polymer |
JP2004107319A (ja) * | 2002-07-22 | 2004-04-08 | Kao Corp | 皮膚洗浄剤組成物 |
CA2513438A1 (en) | 2003-01-17 | 2004-08-05 | The Procter & Gamble Company | Personal care composition containing a cationic cellulose polymer and an anionic surfactant system |
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CN100404555C (zh) * | 2003-06-17 | 2008-07-23 | 联合碳化化学及塑料技术公司 | 纤维素醚 |
DE102004008035A1 (de) * | 2004-02-19 | 2005-09-08 | Symrise Gmbh & Co. Kg | Verwendung von (2-Hydroxyphenyl)-alkoholen sowie diese Verbindungen enthaltende kosmetische oder therapeutische Formulierungen |
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EP1813262A1 (en) * | 2006-01-19 | 2007-08-01 | Wella Aktiengesellschaft | Stable oil-in-water and water/oil/water multiple emulsions and hair treating compositions comprising them |
US20080003192A1 (en) * | 2006-06-29 | 2008-01-03 | Modi Jashawant J | Functional compositions containing cationic hydrophobically modified polysaccharides for personal care, household & institutional and pet care products |
JP4886505B2 (ja) | 2006-12-28 | 2012-02-29 | 花王株式会社 | 洗浄剤用組成物 |
IT1391979B1 (it) * | 2008-07-18 | 2012-02-02 | Lamberti Spa | Eteri di galattomannani modificati |
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US20110318285A1 (en) | 2011-12-29 |
CN102958498A (zh) | 2013-03-06 |
ES2689863T3 (es) | 2018-11-16 |
CN102958498B (zh) | 2015-09-09 |
RU2589261C2 (ru) | 2016-07-10 |
WO2011163589A3 (en) | 2012-07-26 |
WO2011163589A2 (en) | 2011-12-29 |
KR20130121081A (ko) | 2013-11-05 |
JP2013529644A (ja) | 2013-07-22 |
EP2585032A2 (en) | 2013-05-01 |
US8790627B2 (en) | 2014-07-29 |
MX2012014616A (es) | 2013-02-21 |
KR101824754B1 (ko) | 2018-02-01 |
BR112012032835A2 (pt) | 2016-08-30 |
RU2013102915A (ru) | 2014-07-27 |
BR112012032835B1 (pt) | 2018-01-09 |
EP2585032B1 (en) | 2018-08-08 |
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