JP5692729B2 - 金属処理 - Google Patents
金属処理 Download PDFInfo
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- JP5692729B2 JP5692729B2 JP2012502803A JP2012502803A JP5692729B2 JP 5692729 B2 JP5692729 B2 JP 5692729B2 JP 2012502803 A JP2012502803 A JP 2012502803A JP 2012502803 A JP2012502803 A JP 2012502803A JP 5692729 B2 JP5692729 B2 JP 5692729B2
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- Prior art keywords
- voltage
- metal
- metal object
- electrolyte
- surface layer
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
- A61L31/02—Inorganic materials
- A61L31/022—Metals or alloys
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
- A61L31/08—Materials for coatings
- A61L31/082—Inorganic materials
- A61L31/088—Other specific inorganic materials not covered by A61L31/084 or A61L31/086
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L31/00—Materials for other surgical articles, e.g. stents, stent-grafts, shunts, surgical drapes, guide wires, materials for adhesion prevention, occluding devices, surgical gloves, tissue fixation devices
- A61L31/14—Materials characterised by their function or physical properties, e.g. injectable or lubricating compositions, shape-memory materials, surface modified materials
- A61L31/16—Biologically active materials, e.g. therapeutic substances
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/18—After-treatment, e.g. pore-sealing
- C25D11/24—Chemical after-treatment
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/26—Anodisation of refractory metals or alloys based thereon
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/10—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing inorganic materials
- A61L2300/102—Metals or metal compounds, e.g. salts such as bicarbonates, carbonates, oxides, zeolites, silicates
- A61L2300/104—Silver, e.g. silver sulfadiazine
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/40—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
- A61L2300/404—Biocides, antimicrobial agents, antiseptic agents
Description
(a)表面層にとっての基体を提供する金属物体を陽極酸化電解液と接触させ、この金属物体に陽極酸化電圧を印加してその上に陽極酸化された一体化表面層を形成することによって金属を不動態化し、
(b)陽極酸化電圧を印加し続けることによって、一体化表面層を貫通して基体まで至るピットを形成し、
(c)電解液又は溶液と接触させての電気化学的又は化学的還元によって表面層に含水金属酸化物を生成し、
(d)工程(c)で得られた陽極酸化済みの金属物体を工程(c)の電解液又は溶液から取り出し又は分離し、
(e)陽極酸化済みの金属物体を、殺生物性物質を含有する溶液と接触させることによって、この殺生物性物質を表面層に取り込ませることを含み、
ピット形成工程(b)における電圧は、不動態化工程(a)中に印加される最大電圧より低い。
Claims (16)
- 金属物体を処理して、その上に金属物体と一体化しており且つ殺生物性物質を含む表面層を形成する方法であって、
(a)表面層にとっての基体を提供する金属物体を陽極酸化電解液と接触させ、前記金属物体に陽極酸化電圧を印加してその上に陽極酸化された一体化表面層を形成することによって金属を不動態化する工程、
(b)陽極酸化電圧を印加し続けることによって、前記一体化表面層を貫通して前記基体まで至るピットを形成する工程、
(c)電解液又は溶液と接触させての電気化学的又は化学的還元によって前記表面層に含水金属酸化物を生成する工程、
(d)工程(c)で得られた陽極酸化済みの前記金属物体を工程(c)の電解液又は溶液から取り出し又は分離する工程、及び
(e)前記陽極酸化済みの金属物体を、殺生物性物質を含有する溶液と接触させることによって、前記殺生物性物質を前記表面層に取り込ませる工程、
を含み、ピット形成工程(b)における電圧が、不動態化工程(a)中に印加される最大電圧より低く、15〜85Vであることを特徴とする方法。 - ピット形成工程(b)における電圧が20〜75Vである、請求項1に記載の方法。
- ピット形成工程(b)における電圧が20〜60Vである、請求項2に記載の方法。
- 陽極酸化工程(a)及び(b)が60分以下の合計時間で行われる、請求項1〜3のいずれかに記載の方法。
- 不動態化工程(a)において印加する電圧を5V/秒以下で上昇させる、請求項1〜4のいずれかに記載の方法。
- 不動態化工程(a)において印加する電圧を段階的に上昇させる、請求項1〜5のいずれかに記載の方法。
- 複数回の不動態化工程(a)を含む、請求項1〜6のいずれかに記載の方法。
- 不動態化工程(a)において、電圧を、50V未満の値で1〜20分間に亘って維持してから前記最大電圧まで上昇させる、請求項1〜7のいずれかに記載の方法。
- 前記最大電圧まで上昇させる前に、電圧を、3〜35Vの値で2〜5分間に亘って維持する、請求項8に記載の方法。
- 前記最大電圧まで上昇させる前に、不動態化工程(a)において、電圧を50V未満の値まで上昇させ、次にゼロに低下させる、請求項1〜9のいずれかに記載の方法。
- 工程(a)及び(b)における陽極酸化で使用する電荷の量が0.5〜10クーロン/cm2の範囲である、請求項1〜10のいずれかに記載の方法。
- 前記最大不動態化電圧が、30〜2000Vの範囲から選択される、請求項1〜11のいずれか1項に記載の方法。
- 負電圧を金属物体に印加し、前記負電圧を300秒未満で印加することにより、電気化学的還元によって工程(c)において含水金属酸化物が生成される、請求項1〜12のいずれかに記載の方法。
- 不動態化工程(a)中、陽極酸化電解液を攪拌し、及び/又はピット形成工程(b)中、金属物体の表面に対しての電解液の動きを阻害する、請求項1〜13のいずれかに記載の方法。
- 請求項1〜14のいずれかに記載の方法によって製造される、医療処置で使用するための金属物体。
- 請求項1〜14のいずれかに記載の方法によって製造される、宝飾品。
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB0905354.7 | 2009-03-30 | ||
GBGB0905354.7A GB0905354D0 (en) | 2009-03-30 | 2009-03-30 | Metal treatment |
GB0920314.2 | 2009-11-20 | ||
GB0920314A GB0920314D0 (en) | 2009-11-20 | 2009-11-20 | Metal treatment |
PCT/GB2010/050531 WO2010112908A1 (en) | 2009-03-30 | 2010-03-29 | Metal treatment |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2012522135A JP2012522135A (ja) | 2012-09-20 |
JP2012522135A5 JP2012522135A5 (ja) | 2013-05-16 |
JP5692729B2 true JP5692729B2 (ja) | 2015-04-01 |
Family
ID=42154645
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2012502803A Active JP5692729B2 (ja) | 2009-03-30 | 2010-03-29 | 金属処理 |
Country Status (9)
Country | Link |
---|---|
US (2) | US9096943B2 (ja) |
EP (1) | EP2414564B1 (ja) |
JP (1) | JP5692729B2 (ja) |
KR (1) | KR101780923B1 (ja) |
CN (1) | CN102449207B (ja) |
AU (1) | AU2010231092B2 (ja) |
CA (1) | CA2756651C (ja) |
HK (1) | HK1170547A1 (ja) |
WO (1) | WO2010112908A1 (ja) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9809894B2 (en) | 2011-01-14 | 2017-11-07 | Accentus Medical Limited | Metal treatment |
GB201508385D0 (en) * | 2015-05-15 | 2015-07-01 | Accentus Medical Ltd | Metal treatment |
KR101701314B1 (ko) * | 2015-07-02 | 2017-02-02 | 고려대학교 산학협력단 | 양극산화된 금속산화물 나노다공성 템플레이트 제작방법 |
WO2017130029A1 (en) * | 2016-01-29 | 2017-08-03 | Nanoti Limited | Scratch resistance and corrosion behavior of nanotubular and nano-pitted anodic films on medical grade bulk titanium substrates |
CN106887379B (zh) * | 2017-03-01 | 2019-12-31 | 重庆京东方光电科技有限公司 | 一种半透掩膜构图方法及阵列基板、显示装置 |
US10893944B2 (en) | 2017-03-30 | 2021-01-19 | Biomet Manufacturing, Llc | Methods of modifying the porous surface of implants |
CN108103553B (zh) * | 2017-12-28 | 2019-11-26 | 大博医疗科技股份有限公司 | 一种钛表面无掺杂低缺陷的彩色阳极氧化膜制备方法 |
EP3640372A1 (de) * | 2018-10-18 | 2020-04-22 | Hirtenberger Engineered Surfaces GmbH | Verfahren zum entfernen von metallischen stützstrukturen an einem additiv gefertigten metallbauteil |
CN112831817B (zh) * | 2020-12-22 | 2022-05-24 | 北京钛古科技有限责任公司 | 一种锐型生物钛材料及其制备方法 |
Family Cites Families (16)
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JPS61198245A (ja) * | 1985-02-28 | 1986-09-02 | Showa Alum Corp | 電子写真用感光体の下地処理方法 |
US4822458A (en) * | 1988-04-25 | 1989-04-18 | The United States Of America As Represented By The Secretary Of The Navy | Anodic coating with enhanced thermal conductivity |
JPH0747838B2 (ja) * | 1989-07-07 | 1995-05-24 | 賢三 小林 | チタンまたはその合金の通電量制御による着色法 |
JPH0372098A (ja) * | 1989-08-10 | 1991-03-27 | Showa Alum Corp | 真空用アルミニウム材の製造方法 |
US5340605A (en) * | 1993-03-05 | 1994-08-23 | The United States Of America As Represented By The United States Department Of Energy | Method for plating with metal oxides |
US5500106A (en) * | 1994-03-04 | 1996-03-19 | Shipley Company, L.L.C. | Electroplating process |
ATE217366T1 (de) * | 1996-08-15 | 2002-05-15 | Alcan Tech & Man Ag | Reflektor mit resistenter oberfläche |
US6267782B1 (en) * | 1997-11-20 | 2001-07-31 | St. Jude Medical, Inc. | Medical article with adhered antimicrobial metal |
GB0208642D0 (en) * | 2002-04-16 | 2002-05-22 | Accentus Plc | Metal implants |
GB0405680D0 (en) * | 2004-03-13 | 2004-04-21 | Accentus Plc | Metal implants |
US7727372B2 (en) * | 2004-12-06 | 2010-06-01 | Greatbatch Ltd. | Anodizing valve metals by self-adjusted current and power |
US8012338B2 (en) * | 2006-02-10 | 2011-09-06 | Syracuse University | Method for preparing biomedical surfaces |
US20090198344A1 (en) * | 2006-06-12 | 2009-08-06 | Accentus Plc | Metal Implants |
CA2702119C (en) * | 2007-10-03 | 2017-03-28 | Accentus Plc | Method of manufacturing metal with biocidal properties |
GB0720982D0 (en) * | 2007-10-25 | 2007-12-05 | Plasma Coatings Ltd | Method of forming a bioactive coating |
US8379993B2 (en) * | 2007-12-13 | 2013-02-19 | Edward Joseph Kendall | Image analysis |
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2010
- 2010-03-29 WO PCT/GB2010/050531 patent/WO2010112908A1/en active Application Filing
- 2010-03-29 AU AU2010231092A patent/AU2010231092B2/en active Active
- 2010-03-29 EP EP10712135.2A patent/EP2414564B1/en active Active
- 2010-03-29 KR KR1020117025813A patent/KR101780923B1/ko active IP Right Grant
- 2010-03-29 CN CN201080024942.3A patent/CN102449207B/zh not_active Expired - Fee Related
- 2010-03-29 JP JP2012502803A patent/JP5692729B2/ja active Active
- 2010-03-29 US US13/262,350 patent/US9096943B2/en active Active
- 2010-03-29 CA CA2756651A patent/CA2756651C/en active Active
-
2012
- 2012-11-09 HK HK12111363.2A patent/HK1170547A1/xx not_active IP Right Cessation
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2015
- 2015-06-29 US US14/754,398 patent/US9738980B2/en active Active
Also Published As
Publication number | Publication date |
---|---|
AU2010231092A2 (en) | 2011-11-03 |
CA2756651A1 (en) | 2010-10-07 |
US9738980B2 (en) | 2017-08-22 |
KR101780923B1 (ko) | 2017-09-22 |
EP2414564B1 (en) | 2018-03-14 |
CN102449207B (zh) | 2015-05-27 |
WO2010112908A1 (en) | 2010-10-07 |
US9096943B2 (en) | 2015-08-04 |
HK1170547A1 (en) | 2013-03-01 |
JP2012522135A (ja) | 2012-09-20 |
CA2756651C (en) | 2017-05-23 |
AU2010231092B2 (en) | 2016-06-30 |
AU2010231092A1 (en) | 2011-10-27 |
US20120018308A1 (en) | 2012-01-26 |
US20150299865A1 (en) | 2015-10-22 |
EP2414564A1 (en) | 2012-02-08 |
KR20110139303A (ko) | 2011-12-28 |
CN102449207A (zh) | 2012-05-09 |
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