JP5629236B2 - 蛍光粒子、蛍光粒子を製造する方法及びトナー組成物 - Google Patents
蛍光粒子、蛍光粒子を製造する方法及びトナー組成物 Download PDFInfo
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- JP5629236B2 JP5629236B2 JP2011099057A JP2011099057A JP5629236B2 JP 5629236 B2 JP5629236 B2 JP 5629236B2 JP 2011099057 A JP2011099057 A JP 2011099057A JP 2011099057 A JP2011099057 A JP 2011099057A JP 5629236 B2 JP5629236 B2 JP 5629236B2
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- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
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- G—PHYSICS
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2211/00—Chemical nature of organic luminescent or tenebrescent compounds
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- C—CHEMISTRY; METALLURGY
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- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
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| US8367294B2 (en) * | 2008-03-27 | 2013-02-05 | Xerox Corporation | Toner process |
| US8123848B2 (en) | 2010-05-03 | 2012-02-28 | Xerox Corporation | Fluorescent ink compositions and fluorescent particles |
| DE102011119821A1 (de) | 2011-12-01 | 2013-06-06 | Bundesdruckerei Gmbh | Elektrooptisches Sicherheitselement |
| US9052624B2 (en) | 2012-05-02 | 2015-06-09 | Eastman Kodak Company | Use of fluorescing toners for imaging |
| JP6332052B2 (ja) * | 2014-12-25 | 2018-05-30 | コニカミノルタ株式会社 | 静電荷像現像用トナーおよびその製造方法 |
| CN113533292B (zh) * | 2021-08-24 | 2024-04-26 | 常州工学院 | 一种双酚s含量的荧光检测方法 |
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| US5916A (en) | 1848-11-14 | Mill for breaking and grinding | ||
| GB1442835A (en) | 1972-10-21 | 1976-07-14 | Konishiroku Photo Ind | Toner for use in developing electrostatic images |
| US5290654A (en) | 1992-07-29 | 1994-03-01 | Xerox Corporation | Microsuspension processes for toner compositions |
| US5278020A (en) | 1992-08-28 | 1994-01-11 | Xerox Corporation | Toner composition and processes thereof |
| US5308734A (en) | 1992-12-14 | 1994-05-03 | Xerox Corporation | Toner processes |
| US5346797A (en) | 1993-02-25 | 1994-09-13 | Xerox Corporation | Toner processes |
| US5348832A (en) | 1993-06-01 | 1994-09-20 | Xerox Corporation | Toner compositions |
| US5370963A (en) | 1993-06-25 | 1994-12-06 | Xerox Corporation | Toner emulsion aggregation processes |
| US5403693A (en) | 1993-06-25 | 1995-04-04 | Xerox Corporation | Toner aggregation and coalescence processes |
| US5405728A (en) | 1993-06-25 | 1995-04-11 | Xerox Corporation | Toner aggregation processes |
| US5364729A (en) | 1993-06-25 | 1994-11-15 | Xerox Corporation | Toner aggregation processes |
| US5418108A (en) | 1993-06-25 | 1995-05-23 | Xerox Corporation | Toner emulsion aggregation process |
| US5344738A (en) | 1993-06-25 | 1994-09-06 | Xerox Corporation | Process of making toner compositions |
| US5366841A (en) | 1993-09-30 | 1994-11-22 | Xerox Corporation | Toner aggregation processes |
| EP0716344A1 (en) | 1994-12-05 | 1996-06-12 | Konica Corporation | Light-sensitive composition and light-sensitive lithographic printing plate using the same |
| US5501935A (en) | 1995-01-17 | 1996-03-26 | Xerox Corporation | Toner aggregation processes |
| US5977210A (en) | 1995-01-30 | 1999-11-02 | Xerox Corporation | Modified emulsion aggregation processes |
| US5527658A (en) | 1995-03-13 | 1996-06-18 | Xerox Corporation | Toner aggregation processes using water insoluble transition metal containing powder |
| US5496676A (en) | 1995-03-27 | 1996-03-05 | Xerox Corporation | Toner aggregation processes |
| US5565296A (en) | 1995-07-03 | 1996-10-15 | Xerox Corporation | Coated carriers by aggregation processes |
| US5585215A (en) | 1996-06-13 | 1996-12-17 | Xerox Corporation | Toner compositions |
| US5650255A (en) | 1996-09-03 | 1997-07-22 | Xerox Corporation | Low shear toner aggregation processes |
| US5723252A (en) | 1996-09-03 | 1998-03-03 | Xerox Corporation | Toner processes |
| US5650256A (en) | 1996-10-02 | 1997-07-22 | Xerox Corporation | Toner processes |
| US5683848A (en) | 1996-10-02 | 1997-11-04 | Xerox Corporation | Acrylonitrile-modified toner composition and processes |
| US6770687B1 (en) * | 1996-11-21 | 2004-08-03 | Ncr Corporation | Water-based dual security ink |
| US5763133A (en) | 1997-03-28 | 1998-06-09 | Xerox Corporation | Toner compositions and processes |
| US5827633A (en) | 1997-07-31 | 1998-10-27 | Xerox Corporation | Toner processes |
| US5766818A (en) | 1997-10-29 | 1998-06-16 | Xerox Corporation | Toner processes with hydrolyzable surfactant |
| US5916725A (en) | 1998-01-13 | 1999-06-29 | Xerox Corporation | Surfactant free toner processes |
| US5853944A (en) | 1998-01-13 | 1998-12-29 | Xerox Corporation | Toner processes |
| US5910387A (en) | 1998-01-13 | 1999-06-08 | Xerox Corporation | Toner compositions with acrylonitrile and processes |
| US5869215A (en) | 1998-01-13 | 1999-02-09 | Xerox Corporation | Toner compositions and processes thereof |
| US5840462A (en) | 1998-01-13 | 1998-11-24 | Xerox Corporation | Toner processes |
| US5919595A (en) | 1998-01-13 | 1999-07-06 | Xerox Corporation | Toner process with cationic salts |
| US5863698A (en) | 1998-04-13 | 1999-01-26 | Xerox Corporation | Toner processes |
| US6063827A (en) | 1998-07-22 | 2000-05-16 | Xerox Corporation | Polyester process |
| US6576155B1 (en) * | 1998-11-10 | 2003-06-10 | Biocrystal, Ltd. | Fluorescent ink compositions comprising functionalized fluorescent nanocrystals |
| DE10054344A1 (de) * | 2000-11-02 | 2002-05-29 | Clariant Gmbh | Verwendung von gecoateten Pigmentgranulaten in elektrophotographischen Tonern und Entwicklern, Pulverlacken und Ink-Jet-Tinten |
| US6593049B1 (en) | 2001-03-26 | 2003-07-15 | Xerox Corporation | Toner and developer compositions |
| US6576389B2 (en) | 2001-10-15 | 2003-06-10 | Xerox Corporation | Toner coagulant processes |
| US6638677B2 (en) | 2002-03-01 | 2003-10-28 | Xerox Corporation | Toner processes |
| US6627373B1 (en) | 2002-03-25 | 2003-09-30 | Xerox Corporation | Toner processes |
| US6617092B1 (en) | 2002-03-25 | 2003-09-09 | Xerox Corporation | Toner processes |
| US6673505B2 (en) | 2002-03-25 | 2004-01-06 | Xerox Corporation | Toner coagulant processes |
| US6656657B2 (en) | 2002-03-25 | 2003-12-02 | Xerox Corporation | Toner processes |
| US6656658B2 (en) | 2002-03-25 | 2003-12-02 | Xerox Corporation | Magnetite toner processes |
| US6664017B1 (en) | 2002-08-20 | 2003-12-16 | Xerox Corporation | Document security processes |
| US6756176B2 (en) | 2002-09-27 | 2004-06-29 | Xerox Corporation | Toner processes |
| US6830860B2 (en) | 2003-01-22 | 2004-12-14 | Xerox Corporation | Toner compositions and processes thereof |
| US6858070B1 (en) * | 2003-11-25 | 2005-02-22 | Xerox Corporation | Phase change inks |
| US20050272851A1 (en) | 2004-06-04 | 2005-12-08 | Xerox Corporation | Wax emulsion for emulsion aggregation toner |
| US7329476B2 (en) | 2005-03-31 | 2008-02-12 | Xerox Corporation | Toner compositions and process thereof |
| US20080098929A1 (en) * | 2006-10-26 | 2008-05-01 | Xerox Corporation | Phase change inks |
| US8039187B2 (en) | 2007-02-16 | 2011-10-18 | Xerox Corporation | Curable toner compositions and processes |
| US7465348B1 (en) * | 2007-06-07 | 2008-12-16 | Xerox Corporation | Nanosized particles of monoazo laked pigment |
| US20090214972A1 (en) * | 2008-02-26 | 2009-08-27 | Xerox Corporation | Toner compositions |
| US8420286B2 (en) | 2008-03-27 | 2013-04-16 | Xerox Corporation | Toner process |
| US7857900B2 (en) * | 2008-09-19 | 2010-12-28 | Xerox Corporation | Solid phase change fluorescent ink and ink sets |
| US8236198B2 (en) | 2008-10-06 | 2012-08-07 | Xerox Corporation | Fluorescent nanoscale particles |
| US8147714B2 (en) * | 2008-10-06 | 2012-04-03 | Xerox Corporation | Fluorescent organic nanoparticles and a process for producing fluorescent organic nanoparticles |
| US8586141B2 (en) * | 2008-10-06 | 2013-11-19 | Xerox Corporation | Fluorescent solid ink made with fluorescent nanoparticles |
| US8541154B2 (en) * | 2008-10-06 | 2013-09-24 | Xerox Corporation | Toner containing fluorescent nanoparticles |
| US8101801B2 (en) | 2009-05-18 | 2012-01-24 | Xerox Corporation | Low molecular weight quaternary ammonium salt dispersants |
-
2010
- 2010-05-03 US US12/772,689 patent/US8252494B2/en active Active
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2011
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- 2011-04-27 CA CA2738440A patent/CA2738440C/en not_active Expired - Fee Related
- 2011-05-02 KR KR1020110041681A patent/KR101668496B1/ko not_active Expired - Fee Related
- 2011-05-02 DE DE102011075090.8A patent/DE102011075090B4/de active Active
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Also Published As
| Publication number | Publication date |
|---|---|
| CN102295920B (zh) | 2015-05-27 |
| CN102295920A (zh) | 2011-12-28 |
| CA2738440C (en) | 2014-09-30 |
| DE102011075090A1 (de) | 2012-02-23 |
| US8252494B2 (en) | 2012-08-28 |
| JP2011236418A (ja) | 2011-11-24 |
| CA2738440A1 (en) | 2011-11-03 |
| KR20110122063A (ko) | 2011-11-09 |
| US20110269065A1 (en) | 2011-11-03 |
| DE102011075090B4 (de) | 2022-10-13 |
| KR101668496B1 (ko) | 2016-10-21 |
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