JP5628685B2 - ジルコニア含有ナノ粒子の製造方法 - Google Patents

ジルコニア含有ナノ粒子の製造方法 Download PDF

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Publication number
JP5628685B2
JP5628685B2 JP2010540795A JP2010540795A JP5628685B2 JP 5628685 B2 JP5628685 B2 JP 5628685B2 JP 2010540795 A JP2010540795 A JP 2010540795A JP 2010540795 A JP2010540795 A JP 2010540795A JP 5628685 B2 JP5628685 B2 JP 5628685B2
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zirconia
zirconium
raw material
weight
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JP2011508721A5 (enExample
JP2011508721A (ja
Inventor
ユー． コルブ，ブラント
ユー． コルブ，ブラント
ビー． アンダーソン，ダニー
ビー． アンダーソン，ダニー
エス． ダビッドソン，ロバート
エス． ダビッドソン，ロバート
ジェイ． ヘンドリクソン，マーク
ジェイ． ヘンドリクソン，マーク
ジェイ． リーチ，ジェイムズ
ジェイ． リーチ，ジェイムズ
エル． マッケンジー，タウン
エル． マッケンジー，タウン
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3M Innovative Properties Co
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3M Innovative Properties Co
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
    • C04B35/486—Fine ceramics
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605—Treating the starting powders individually or as mixtures
    • C04B35/62625—Wet mixtures
    • C04B35/6263—Wet mixtures characterised by their solids loadings, i.e. the percentage of solids
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/449—Organic acids, e.g. EDTA, citrate, acetate, oxalate
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54—Particle size related information
    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5454—Particle size related information expressed by the size of the particles or aggregates thereof nanometer sized, i.e. below 100 nm
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/72—Products characterised by the absence or the low content of specific components, e.g. alkali metal free alumina ceramics

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Composite Materials (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2010540795A 2007-12-28 2008-12-18 ジルコニア含有ナノ粒子の製造方法 Active JP5628685B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US1732607P 2007-12-28 2007-12-28
US61/017,326 2007-12-28
PCT/US2008/087385 WO2009085926A2 (en) 2007-12-28 2008-12-18 Method of making zirconia-containing nanoparticles

Publications (3)

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JP2011508721A JP2011508721A (ja) 2011-03-17
JP2011508721A5 JP2011508721A5 (enExample) 2012-02-02
JP5628685B2 true JP5628685B2 (ja) 2014-11-19

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US (2) US8647510B2 (enExample)
EP (2) EP2620413B1 (enExample)
JP (1) JP5628685B2 (enExample)
CN (1) CN101945824B (enExample)
WO (1) WO2009085926A2 (enExample)

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US8598058B2 (en) 2009-12-29 2013-12-03 3M Innovative Properties Company Zirconia-based material doped with yttrium and lanthanum
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US9616163B2 (en) * 2012-01-04 2017-04-11 Fresenius Medical Care Holdings, Inc. Method and system of enhancing removal of toxic anions and organic solutes in sorbent dialysis
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Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3058594A (en) 1960-06-06 1962-10-16 Purolator Products Inc Pleated paper filter
US3209034A (en) * 1961-12-08 1965-09-28 Kancgafuchi Spinning Co Ltd Oxidation of olefines
US3432546A (en) * 1964-11-03 1969-03-11 Fmc Corp Manufacture of peracetic acid
US3484573A (en) * 1968-08-08 1969-12-16 Roper Corp Geo D Closure for microwave oven
US4358653A (en) * 1977-11-25 1982-11-09 Raytheon Company Combination microwave oven
CA1254238A (en) * 1985-04-30 1989-05-16 Alvin P. Gerk Process for durable sol-gel produced alumina-based ceramics, abrasive grain and abrasive products
US4639356A (en) 1985-11-05 1987-01-27 American Cyanamid Company High technology ceramics with partially stabilized zirconia
JPH0729771B2 (ja) * 1986-01-14 1995-04-05 悦朗 加藤 単斜ジルコニア超微結晶の高分散ゾルまたはゲルおよび製造方法
US4842739A (en) 1987-08-20 1989-06-27 Minnesota Mining And Manufacturing Company High surface area filter cartridge
US5453262A (en) 1988-12-09 1995-09-26 Battelle Memorial Institute Continuous process for production of ceramic powders with controlled morphology
US5037579A (en) * 1990-02-12 1991-08-06 Nalco Chemical Company Hydrothermal process for producing zirconia sol
US5252224A (en) * 1991-06-28 1993-10-12 Modell Development Corporation Supercritical water oxidation process of organics with inorganics
US5652192A (en) 1992-07-10 1997-07-29 Battelle Memorial Institute Catalyst material and method of making
US5468847A (en) 1994-03-10 1995-11-21 Minnesota Mining And Manufacturing Company Method of isolating and purifying a biomacromolecule
DE19746265A1 (de) 1997-10-20 1999-04-22 Bayer Ag Verbunde aus Polyurethan und einem thermoplastischen Material
JP4524463B2 (ja) 1999-07-27 2010-08-18 三井化学株式会社 ガスバリア性ポリウレタン樹脂及びこれを含むガスバリア性フィルム
US6376590B2 (en) * 1999-10-28 2002-04-23 3M Innovative Properties Company Zirconia sol, process of making and composite material
AUPR152100A0 (en) * 2000-11-16 2000-12-14 University Of Technology, Sydney Method for treating coral
US20040221507A1 (en) * 2003-05-07 2004-11-11 Wu Benjamin C. Method and apparatus for providing hydrogen
JP2005179111A (ja) * 2003-12-18 2005-07-07 Catalysts & Chem Ind Co Ltd ジルコニアゾルの製造方法
JP4399592B2 (ja) 2004-03-10 2010-01-20 独立行政法人産業技術総合研究所 酸化ジルコニウム結晶粒子とその製造方法
JP4230954B2 (ja) 2004-04-08 2009-02-25 株式会社日立製作所 有機ハロゲン化合物処理システム
US7241437B2 (en) * 2004-12-30 2007-07-10 3M Innovative Properties Company Zirconia particles
WO2006098899A2 (en) 2005-03-11 2006-09-21 3M Innovative Properties Company Light management films with zirconia particles
KR100693126B1 (ko) * 2005-07-14 2007-03-13 한국화학연구원 다공성 물질 및 혼합 금속산화물의 연속적 제조방법 및연속적 제조 장치
US20070128707A1 (en) * 2005-11-10 2007-06-07 Oregon State University Method for making metal oxides
EP1884559A1 (en) * 2006-07-26 2008-02-06 Vlaamse Instelling Voor Technologisch Onderzoek (Vito) Novel method for producing biodiesel using an immobilised catalyst
EP2620413B1 (en) 2007-12-28 2020-07-01 3M Innovative Properties Company Continuous hydrothermal reactor system comprising a fluorinated polymer tubular reactor
JP5247854B2 (ja) 2011-07-06 2013-07-24 株式会社インスピーディア 集荷システムおよび集荷方法

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CN101945824B (zh) 2014-07-23
US8647510B2 (en) 2014-02-11
US8808549B2 (en) 2014-08-19
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EP2620413A1 (en) 2013-07-31
EP2244982A2 (en) 2010-11-03
EP2244982B1 (en) 2018-01-24
JP2011508721A (ja) 2011-03-17
US20140056778A1 (en) 2014-02-27
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