JP4551451B2 - 精油所供給原料又は精油所プロセスの生成物の分析のための携帯装置 - Google Patents
精油所供給原料又は精油所プロセスの生成物の分析のための携帯装置 Download PDFInfo
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; viscous liquids; paints; inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2835—Oils, i.e. hydrocarbon liquids specific substances contained in the oil or fuel
- G01N33/2876—Total acid number
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/02—Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering
- G01N25/08—Investigating or analyzing materials by the use of thermal means by investigating changes of state or changes of phase; by investigating sintering of boiling point
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N35/00—Automatic analysis not limited to methods or materials provided for in any single one of groups G01N1/00 - G01N33/00; Handling materials therefor
- G01N35/00584—Control arrangements for automatic analysers
- G01N35/00722—Communications; Identification
- G01N35/00871—Communications between instruments or with remote terminals
Description
本発明は、精油所供給原料又は精油所プロセスの生成物の分析のための携帯装置に関する。
更に、精油所プロセスの生成物の迅速な分析もまた望ましい。かかる生成物としては、全精油所プロセスにおける中間体、ビチューメン、その後に化学供給原料として用いられる全精油所プロセスからの生成物、及びその後に燃料又は潤滑剤、或いは燃料又は潤滑剤のための配合成分、並びに燃料(例えば航空燃料、ガソリン燃料、ディーゼル燃料及び船舶燃料)及び潤滑剤それ自体として用いられる全精油所プロセスからの生成物が挙げられる。
(a)精油所供給原料又は精油所プロセスの生成物の沸点プロフィールを測定するための第1の分析機器;及び
(b)それぞれがデータベース及びアルゴリズムを含むか又はそれに結合されており、その少なくとも一つが精油所供給原料又は精油所プロセスの生成物の密度を測定するように構成されており、その少なくとも一つが精油所供給原料又は精油所プロセスの生成物の全酸価(TAN)を測定するように構成されている、少なくとも二つの更なる分析機器;
を含む、精油所供給原料又は精油所プロセスの生成物を分析するための携帯装置を提供する。
(a)精油所供給原料又は精油所プロセスの生成物の沸点プロフィールを測定することができ、精油所供給原料又は精油所プロセスの生成物を2以上のフラクションに分離するためのマイクロ分離機器;及び
(b)1以上のフラクションの密度及びTANを測定するための2以上の更なる分析機器;
を含む、精油所供給原料又は精油所プロセスの生成物を分析するための携帯装置を提供する。
本発明の装置は、少量の、典型的には100ml未満、例えば10ml以下、好ましくは1ml以下の精油所供給原料又は精油所プロセスの生成物(本明細書において、精油所供給原料又は精油所プロセスの生成物は「試料」と称することができる)しか必要としない。必要とされる試料が少量であるので、分析を、従来の分析、例えば従来の原油アッセイよりも著しく短い時間で行うことができる。
精油所供給原料は、原油、合成原油(合成石油)、生物成分、中間体成分、例えば残留成分又は分解石油成分、或いは1以上のかかる供給原料のブレンドのような、精製所に供給することのできる任意の好適な供給原料であってよい。
Claims (16)
- (a)精油所供給原料又は精油所プロセスの生成物の沸点プロフィールを測定するための第1のマイクロ加工された携帯型分析機器;及び
(b)それぞれが、多数の同様の生成物の分析から誘導されたデータベースモデルを含むか又はそれに結合されており、その少なくとも一つが精油所供給原料又は精油所プロセスの生成物の密度を測定するように構成されており、その少なくとも一つが精油所供給原料又は精油所プロセスの生成物の全酸価を測定するように構成されている、少なくとも二つの更なるマイクロ加工された携帯型分析機器であって、前記測定された沸点プロフィール、密度、及び全酸価を前記データベースモデルに入力して、精油所供給原料又は精油所プロセスの生成物の測定アッセイを行う分析機器;
を含む、
精油所供給原料又は精油所プロセスの生成物の沸点プロフィール、密度、及び全酸価を測定し、これらの値を用いて精油所供給原料又は精油所プロセスの生成物の測定アッセイを行うための携帯装置。 - 前記第1のマイクロ加工された携帯型分析機器が、(i)マイクロ蒸留又はマイクロ分留機器;(ii)マイクロNIR分光光度計;(iii)マイクロオシレータ機器;及び(iv)マイクロGC;から選択される請求項1に記載の携帯装置。
- 前記少なくとも二つの更なるマイクロ加工された携帯型分析機器のうち、少なくとも一つが、1以上の更なる特性に加えて沸点プロフィールを測定することができる分析機器を含む請求項1又は2に記載の携帯装置。
- 前記第1のマイクロ加工された携帯型分析機器と少なくとも二つの更なるマイクロ加工された携帯型分析機器との組み合わせにおいて、マイクロ蒸留又はマイクロ分留機器、マイクロNIR分光光度計、マイクロオシレータ機器及びマイクロGCから選択される3以上の分析機器を含む請求項1又は2に記載の携帯装置。
- 前記第1のマイクロ加工された携帯型分析機器および少なくとも二つの更なるマイクロ加工された携帯型分析機器のうち、少なくとも一つがセンサーの形態で存在する請求項1又は2に記載の携帯装置。
- 前記第1のマイクロ加工された携帯型分析機器と少なくとも二つの更なるマイクロ加工された携帯型分析機器の組み合わせにおいて、マイクロ蒸留又はマイクロ分留機器、マイクロNIR分光光度計、マイクロオシレータ機器及びマイクロGCから選択される3以上の分析機器を、振動センサー及び電気化学センサーと共に含む請求項5に記載の携帯装置。
- 前記第1のマイクロ加工された携帯型分析機器および少なくとも二つの更なるマイクロ加工された携帯型分析機器のうち少なくとも一つが更に硫黄含量を測定するための機器、又は前記第1のマイクロ加工された携帯型分析機器および少なくとも二つの更なるマイクロ加工された携帯型分析機器のうち少なくとも一つが更に金属含量若しくは硫黄含量と金属含量との両方を測定するための機器を含む請求項1又は2に記載の携帯装置。
- 更に以下の特性:全塩基価、任意の低温フロー特性、粘度、リサーチオクタン価、モーター法オクタン価、セタン価、煙点、鉱山局相関指標、屈折率、導電度、窒素含量、及びこれらの組み合わせ;の少なくとも一つを測定することができる請求項1又は2に記載の携帯装置。
- 前記2以上の更なるマイクロ加工された携帯型分析機器が、精油所供給原料又は精油所プロセスの生成物の全体の密度及びTAN、又は精油所供給原料又は精油所プロセスの生成物の1以上のフラクションの密度及びTAN、或いはこれらの両方を測定するように構成されている請求項1又は2に記載の携帯装置。
- 前記第1のマイクロ加工された携帯型分析機器が、精油所供給原料又は精油所プロセスの生成物の沸点プロフィールを測定することができ、精油所供給原料又は精油所プロセスの生成物を2以上のフラクションに分離するためのマイクロ分離機器
を含む請求項1又は2に記載の携帯装置。 - 前記マイクロ分離機器が、マイクロ蒸留又はマイクロ分留機器及びマイクロオシレータ機器から選択される請求項10に記載の携帯装置。
- 前記マイクロ分離機器としてマイクロ蒸留又はマイクロ分留機器を含み、前記少なくとも二つの更なるマイクロ加工された携帯型分析機器のうち少なくとも一つとしてマイクロNIR分光光度計を含む請求項11に記載の携帯装置。
- 手持ち型で、5kg未満の全重量を有する請求項1に記載の携帯装置。
- 少なくとも5個の異なる分析機器を含む請求項1に記載の携帯装置。
- 請求項1に記載の携帯装置を用いて精油所供給原料又は精油所プロセスの生成物を分析することを含み、
前記携帯装置から得られた分析データを、多数の同様の生成物の分析から誘導された好適なデータベースモデルに入力することによって、精油所供給原料又は精油所プロセスの生成物の詳細なアッセイを実施する、
精油所供給原料又は精油所プロセスの生成物の沸点プロフィール、密度、及び全酸価を測定し、これらの値を用いて精油所供給原料又は精油所プロセスの生成物の測定アッセイを行う方法。 - 原油又は原油のブレンドを分析することを含む請求項15に記載の方法。
Applications Claiming Priority (3)
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US61100204P | 2004-09-17 | 2004-09-17 | |
US61105004P | 2004-09-17 | 2004-09-17 | |
PCT/US2005/033240 WO2006034069A1 (en) | 2004-09-17 | 2005-09-15 | Portable apparatus for analysis of a refinery feedstock or a product of a refinery process |
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JP2008513784A JP2008513784A (ja) | 2008-05-01 |
JP4551451B2 true JP4551451B2 (ja) | 2010-09-29 |
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JP2007532518A Expired - Fee Related JP4551451B2 (ja) | 2004-09-17 | 2005-09-15 | 精油所供給原料又は精油所プロセスの生成物の分析のための携帯装置 |
JP2007532521A Pending JP2008513785A (ja) | 2004-09-17 | 2005-09-15 | 炭化水素含有供給原料を分析する方法 |
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US (2) | US20080253426A1 (ja) |
EP (2) | EP1797423B1 (ja) |
JP (2) | JP4551451B2 (ja) |
KR (2) | KR100902806B1 (ja) |
AU (2) | AU2005287020B2 (ja) |
BR (2) | BRPI0515407A (ja) |
CA (2) | CA2581954C (ja) |
EA (2) | EA011591B1 (ja) |
ES (2) | ES2623396T3 (ja) |
MX (2) | MX2007003005A (ja) |
NO (2) | NO20071867L (ja) |
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