JP4310270B2 - 放射フィルター要素およびその製造方法 - Google Patents
放射フィルター要素およびその製造方法 Download PDFInfo
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- JP4310270B2 JP4310270B2 JP2004505808A JP2004505808A JP4310270B2 JP 4310270 B2 JP4310270 B2 JP 4310270B2 JP 2004505808 A JP2004505808 A JP 2004505808A JP 2004505808 A JP2004505808 A JP 2004505808A JP 4310270 B2 JP4310270 B2 JP 4310270B2
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- infrared absorbing
- absorbing dye
- donor
- infrared
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- 239000000434 metal complex dye Substances 0.000 description 1
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- BPHQIXJDBIHMLT-UHFFFAOYSA-N perfluorodecane Chemical compound FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F BPHQIXJDBIHMLT-UHFFFAOYSA-N 0.000 description 1
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- JRKICGRDRMAZLK-UHFFFAOYSA-L peroxydisulfate Chemical compound [O-]S(=O)(=O)OOS([O-])(=O)=O JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
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- 229920000647 polyepoxide Polymers 0.000 description 1
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- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
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- 238000002360 preparation method Methods 0.000 description 1
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- 238000000197 pyrolysis Methods 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
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- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000010187 selection method Methods 0.000 description 1
- 239000012176 shellac wax Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 125000003808 silyl group Chemical group [H][Si]([H])([H])[*] 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 239000012748 slip agent Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 125000006850 spacer group Chemical group 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 229940071182 stannate Drugs 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
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- 239000000758 substrate Substances 0.000 description 1
- QAZLUNIWYYOJPC-UHFFFAOYSA-M sulfenamide Chemical compound [Cl-].COC1=C(C)C=[N+]2C3=NC4=CC=C(OC)C=C4N3SCC2=C1C QAZLUNIWYYOJPC-UHFFFAOYSA-M 0.000 description 1
- 229910052717 sulfur Chemical group 0.000 description 1
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- 150000003557 thiazoles Chemical group 0.000 description 1
- 150000007944 thiolates Chemical class 0.000 description 1
- 150000003585 thioureas Chemical group 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 1
- 239000005052 trichlorosilane Substances 0.000 description 1
- ITMCEJHCFYSIIV-UHFFFAOYSA-M triflate Chemical compound [O-]S(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-M 0.000 description 1
- GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical compound [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000007740 vapor deposition Methods 0.000 description 1
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Classifications
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- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
- G02F1/1333—Constructional arrangements; Manufacturing methods
- G02F1/1335—Structural association of cells with optical devices, e.g. polarisers or reflectors
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- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
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- B41M5/40—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used characterised by the base backcoat, intermediate, or covering layers, e.g. for thermal transfer dye-donor or dye-receiver sheets; Heat, radiation filtering or absorbing means or layers; combined with other image registration layers or compositions; Special originals for reproduction by thermography
- B41M5/42—Intermediate, backcoat, or covering layers
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
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- B41M5/265—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used for the production of optical filters or electrical components
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/26—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used
- B41M5/382—Contact thermal transfer or sublimation processes
- B41M5/38207—Contact thermal transfer or sublimation processes characterised by aspects not provided for in groups B41M5/385 - B41M5/395
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B41M5/38257—Contact thermal transfer or sublimation processes characterised by the use of an intermediate receptor
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B41M5/385—Contact thermal transfer or sublimation processes characterised by the transferable dyes or pigments
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
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- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/26—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used
- B41M5/382—Contact thermal transfer or sublimation processes
- B41M5/392—Additives, other than colour forming substances, dyes or pigments, e.g. sensitisers, transfer promoting agents
- B41M5/395—Macromolecular additives, e.g. binders
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/26—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used
- B41M5/40—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used characterised by the base backcoat, intermediate, or covering layers, e.g. for thermal transfer dye-donor or dye-receiver sheets; Heat, radiation filtering or absorbing means or layers; combined with other image registration layers or compositions; Special originals for reproduction by thermography
- B41M5/42—Intermediate, backcoat, or covering layers
- B41M5/44—Intermediate, backcoat, or covering layers characterised by the macromolecular compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/26—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used
- B41M5/40—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used characterised by the base backcoat, intermediate, or covering layers, e.g. for thermal transfer dye-donor or dye-receiver sheets; Heat, radiation filtering or absorbing means or layers; combined with other image registration layers or compositions; Special originals for reproduction by thermography
- B41M5/46—Thermography ; Marking by high energetic means, e.g. laser otherwise than by burning, and characterised by the material used characterised by the base backcoat, intermediate, or covering layers, e.g. for thermal transfer dye-donor or dye-receiver sheets; Heat, radiation filtering or absorbing means or layers; combined with other image registration layers or compositions; Special originals for reproduction by thermography characterised by the light-to-heat converting means; characterised by the heat or radiation filtering or absorbing means or layers
- B41M5/465—Infrared radiation-absorbing materials, e.g. dyes, metals, silicates, C black
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M7/00—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock
- B41M7/0027—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock using protective coatings or layers by lamination or by fusion of the coatings or layers
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/20—Filters
- G02B5/201—Filters in the form of arrays
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
- G02F1/1333—Constructional arrangements; Manufacturing methods
- G02F1/1335—Structural association of cells with optical devices, e.g. polarisers or reflectors
- G02F1/133509—Filters, e.g. light shielding masks
- G02F1/133514—Colour filters
- G02F1/133516—Methods for their manufacture, e.g. printing, electro-deposition or photolithography
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- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/26—Processing photosensitive materials; Apparatus therefor
- G03F7/34—Imagewise removal by selective transfer, e.g. peeling away
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S430/00—Radiation imagery chemistry: process, composition, or product thereof
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Landscapes
- Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- General Physics & Mathematics (AREA)
- Nonlinear Science (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Mathematical Physics (AREA)
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Thermal Transfer Or Thermal Recording In General (AREA)
Description
関連出願の相互参照
本願は、米国特許法第119条第(e)項に基づいて2003年1月16日出願の米国仮出願第60/440,525号および2002年5月17日出願の米国仮出願第60/381,289号による特典を請求する。これらの仮出願は、その全体が参照により本明細書に組み入れられるものとする。
以下に本明細書に記載される発明を列記する。
1.集成体の一部分を赤外線で露光する工程であって、該集成体は、(1)赤外光を透過することのできる支持体と、(2)転写性物質と赤外線吸収染料とを含む転写性層とを備えた供与体を含み、該供与体の転写性層は、該転写性層の露光部分と該転写性層の非露光部とを備えた露光集成体を提供するように受容体に接触した状態である工程と、
該露光集成体の該受容体と該支持体とを分離させて、画像化受容体と使用済み供与体とを取得する工程であって、該画像化受容体は、該受容体と、該転写性物質の転写部分と、該赤外線吸収染料の転写部分とを含み、該IR染料の該転写部分は着色を有し、そして該使用済み供与体は、該支持体と該転写性層の保持部分とを含む工程と、
該赤外線吸収染料の転写部分の50%〜100%を熱的に脱色するのに十分な時間をかけて摂氏約100度〜摂氏約350度の範囲の温度で該転写性物質の転写部分および該赤外線吸収染料の転写部分を加熱する工程であって、該加熱を熱漂白剤の不在下で行って、液晶ディスプレイに使用するのに好適な放射フィルター要素を提供する工程とを含むことを特徴とする放射フィルター要素の製造方法。
2.前記赤外線吸収染料が、
(a)2−(2−(2−クロロ−3−(2−(1,3−ジヒドロ−1,1−ジメチル−3−(4−スルホブチル)−2H−ベンゾ[e]インドール−2−イリデン)エチリデン)−1−シクロヘキセン−1−イル)エテニル)−1,1−ジメチル−3−(4−スルホブチル)−1H−ベンゾ[e]インドリウム,分子内塩,遊離酸、
(b)2−[2−[2−(2−ピリミジノチオ)−3−[2−(1,3−ジヒドロ−1,1−ジメチル−3−(4−スルホブチル)−2H−ベンゾ[e]インドール−2−イリデン)]エチリデン−1−シクロペンテン−1−イル]エテニル]−1,1ジメチル−3−(4−スルホブチル)−1H−ベンゾ[e]インドリウム,分子内塩,ナトリウム塩、
(c)インドシアニングリーン、および
(d)3H−インドリウム,2−[2−[2−クロロ−3−[(1,3−ジヒドロ−1,3,3−トリメチル−2H−インドール−2−イリデン)エチリデン]−1−シクロペンテン−1−イル]エテニル]−1,3,3−トリメチル−,トリフルオロメタンスルホン酸との(1:1)塩よりなる群から選択されることを特徴とする前記1.に記載の方法。
3.(1)支持体と、(2)転写性物質と赤外線吸収染料とを含む転写性層とを備えた供与体を含む集成体を加熱する工程であって、該転写性層は受容体に接触した状態である工程と、
該転写性層に向けられた赤外線で該集成体の一部分を露光して、該転写性層の露光部分と該転写性層の非露光部とを備える露光集成体を提供する工程と、
該露光集成体の該受容体と該支持体とを分離させて、画像化受容体と使用済み供与体とを取得する工程であって、該画像化受容体は、該受容体と、該転写性物質の一部分と、該赤外線吸収染料の一部分とを含み、そして該使用済み供与体は、該支持体と、該転写性物質を含む保持された転写性層とを備える工程と、
添加漂白剤の不在下で該赤外線吸収染料の該一部分の50%〜100%を熱的に脱色するのに十分な時間をかけて摂氏約100度〜摂氏約350度で該赤外線吸収染料の該一部分を加熱して、熱的に脱色された物質を含むカラーフィルター要素を提供する工程であって、該カラーフィルター要素は、液晶ディスプレイに好適である工程とを含むことを特徴とする、液晶ディスプレイデバイスに使用するのに好適なモノクロームまたはカラーのフィルター要素を製造する方法。
4.前記赤外線吸収染料が、
(a)2−(2−(2−クロロ−3−(2−(1,3−ジヒドロ−1,1−ジメチル−3−(4−スルホブチル)−2H−ベンゾ[e]インドール−2−イリデン)エチリデン)−1−シクロヘキセン−1−イル)エテニル)−1,1−ジメチル−3−(4−スルホブチル)−1H−ベンゾ[e]インドリウム,分子内塩,遊離酸、
(b)2−[2−[2−(2−ピリミジノチオ)−3−[2−(1,3−ジヒドロ−1,1−ジメチル−3−(4−スルホブチル)−2H−ベンゾ[e]インドール−2−イリデン)]エチリデン−1−シクロペンテン−1−イル]エテニル]−1,1ジメチル−3−(4−スルホブチル)−1H−ベンゾ[e]インドリウム,分子内塩,ナトリウム塩、
(c)インドシアニングリーン、および
(d)3H−インドリウム,2−[2−[2−クロロ−3−[(1,3−ジヒドロ−1,3,3−トリメチル−2H−インドール−2−イリデン)エチリデン]−1−シクロペンテン−1−イル]エテニル]−1,3,3−トリメチル−,トリフルオロメタンスルホン酸との(1:1)塩よりなる群から選択されることを特徴とする前記3.に記載の方法。
5.前記1.または3.に記載の方法により製造されることを特徴とする放射フィルター要素。
6.前記1.または3.に記載の方法により製造された放射フィルター要素を、導電性コーティング、液晶材料、および配向層に関連づけて備えることを特徴とする液晶ディスプレイデバイス。
連鎖移動剤溶液CTA−1は、ベルゲ(Berge)らの米国特許公報(特許文献42)およびアントネリ(Antonelli)らの米国特許公報(特許文献43)に記載されているように調製した。
摂氏82度〜摂氏88度で開始剤として過硫酸アンモニウムを使用し、61部のメチルメタクリレートと、30部のn−ブチルアクリレートと、4.0部のCTA−1と、3部のメタクリル酸と、2部のグリシジルメタクリレートと、よりなるモノマーと連鎖移動剤との組成物を用いて、好適なラテックスPR−1を製造した。86ナノメートルの粒子直径平均、摂氏55度のガラス転移温度、1モルあたり20,000グラムのMn、および1モルあたり85,000グラムのMwを有する、重量基準で固形分33.1%のポリマーとして、PR−1を特性づけした。他の成分と混合する直前に、3%アンモニア水(10部の溶液あたり約0.25部のアンモニア)でラテックスを8.5のpHにした。
摂氏82度〜摂氏88度で開始剤として過硫酸アンモニウムを使用して、好適なラテックスPR−2を製造した。PR−2の合成では、内容物を窒素雰囲気下に保持した状態で、凝縮器、添加漏斗、開始溶液入口ポート、機械的攪拌機、ヒーター、および温度調節器プローブを備えた3リットル丸底フラスコを使用した。フラスコに700グラムの脱イオン水および6.90グラムのポリステップ(Polystep)(登録商標)B−7を仕込んだ。100mLの脱イオン水中に溶解された0.40グラムの過硫酸アンモニウムの第1の開始溶液を調製した。96グラムのメチルメタクリレートと、4.0グラムのグリシジルメタクリレートと、80.0グラムのn−ブチルアクリレートと、の第1のモノマーブレンドを調製し、添加漏斗中に配置した。96.0グラムのメチルメタクリレートと、4.0グラムのグリシジルメタクリレートと、80グラムのn−ブチルアクリレートと、40.0グラムのメタクリル酸と、の第2のモノマーブレンドを調製した。攪拌しながら、反応フラスコの内容物を摂氏85度に加熱し、後続の工程を通してその温度を±摂氏3度の範囲内に保持した。
摂氏82度〜摂氏88度で開始剤として過硫酸アンモニウムを使用し、204部のメチルメタクリレートと、160部のn−ブチルアクリレートと、16部のCTA−1と、12部のメタクリル酸と、8部のグリシジルメタクリレートと、よりなるモノマーと連鎖移動剤との組成物を用いて、好適なラテックスPR−10を製造した。3%アンモニア水(10部の溶液あたり約0.25部のアンモニア)でラテックスを8.5のpHにした。73ナノメートルの粒子直径平均、摂氏37度のガラス転移温度、1モルあたり34,000グラムのMn、および1モルあたり125,000グラムのMwを有する、固形分32.4%のポリマーとして、PR−10を特性づけした。
摂氏82度〜摂氏88度で開始剤として過硫酸アンモニウムを使用し、252部のメチルメタクリレートと、120部のn−ブチルアクリレートと、16部のCTA−1と、12部のメタクリル酸と、よりなるモノマーと連鎖移動剤との組成物を用いて、好適なラテックスPR−11を製造した。79ナノメートルの粒子直径平均、摂氏58度のガラス転移温度、1モルあたり30,000グラムのMn、および1モルあたり95,000グラムのMwを有する、固形分32.9%のポリマーとして、PR−11を特性づけした。
(赤色)
ピグメントレッド254の好適な水性顔料分散PD−R3を、24重量パーセントの顔料および1.5の顔料対バインダー比で、使用した(ペン・カラー32R238D(Penn Color 32R238D),ペンシルバニア州のペン・カラー(Penn Color,PA))。
ピグメントイエロー83の好適な水性顔料分散PD−Y1を、28重量パーセントの顔料および2.3の顔料対バインダー比で使用した(ペン・カラー32Y145D(Penn Color 32Y145D),ペンシルバニア州のペン・カラー(Penn Color,PA))。
内容物を窒素雰囲気下に保持した状態で、凝縮器、添加漏斗、開始溶液入口ポート、機械的攪拌機、ヒーター、および温度調節器プローブを備えた3リットル丸底フラスコ中で、好適に接着剤AP−1を生成させた。700グラムの脱イオン水と、アンモニウムラウリルスルフェート(ポリステップ(Polystep)(登録商標)B−7)の30%溶液6.90グラムと、をフラスコに仕込んだ。100mLの脱イオン水中に溶解された0.40グラムの過硫酸アンモニウムの第1の開始溶液を調製した。66.0グラムのメチルメタクリレートと、4.0グラムのグリシジルメタクリレートと、110.0グラムのn−ブチルアクリレートと、の第1のモノマーブレンドを調製し、添加漏斗中に配置した。66.0グラムのメチルメタクリレートと、4.0グラムのグリシジルメタクリレートと、110グラムのn−ブチルアクリレートと、40.0グラムのメタクリル酸と、の第2のモノマーブレンドを調製した。攪拌しながら、反応フラスコの内容物を摂氏85度に加熱し、後続の工程を通してその温度を±摂氏3度の範囲内に保持した。
実施例1では、カラーフィルターの製造に好適な一連の工程で、赤外線吸収染料を有する熱画像形成赤色配合物の本発明に係る実施形態について具体的に説明する。
比較例2では、赤色配合物を加熱した場合と加熱しない場合の両方において、赤外線吸収染料の添加前の熱画像形成赤色配合物の吸光度について具体的に説明する。次の例では、実施例1に記載されているように供与体支持体に適用してレーザーを用いて熱的に画像化こととは対照的に、迅速に吸光度スペクトルを決定するために、不完全に配合された熱画像形成赤色配合物をガラススライドに直接適用する。
実施例3では、赤色配合物を加熱することによる熱画像形成赤色配合物中の赤外線吸収染料の熱的脱色について具体的に説明する。
実施例4では、赤色配合物を加熱することによる熱画像形成赤色配合物中の赤外線吸収染料の熱的脱色について具体的に説明する。
実施例5では、赤色配合物を加熱することによる熱画像形成赤色配合物中の赤外線吸収染料の熱的脱色について具体的に説明する。
実施例6では、赤外線吸収染料の熱分解により白色に一段と近い色を生成させることができることを具体的に説明する。この実施例は、顔料非含有配合物を含む。そのため、顔料により覆い隠された吸光度について調べることができるようになる。
実施例7では、赤外線吸収染料の熱分解により白色に一段と近い色を生成させることができることを具体的に説明する。この実施例は、顔料非含有配合物を含む。そのため、顔料により覆い隠された吸光度について調べることができるようになる。
実施例8では、赤外線吸収染料の熱分解により白色に一段と近い色を生成させることができることを具体的に説明する。この実施例は、顔料非含有配合物を含む。そのため、顔料により覆い隠された吸光度について調べることができるようになる。水以外の液体(たとえば、アセトン)を、配合物用の主要なキャリヤーとして使用することができる。
実施例9では、赤外線吸収染料の熱分解により白色に一段と近い色を生成させることができることを具体的に説明する。この実施例は、顔料非含有配合物を含む。そのため、顔料により覆い隠された吸光度について調べることができるようになる。
実施例10では、赤外線吸収染料の熱的脱色が1気圧の圧力の空気の存在に依存しないことを具体的に説明する。この実施例は、顔料非含有配合物を含む。そのため、顔料により覆い隠された吸光度について調べることができるようになる。
Claims (4)
- 集成体の一部分を赤外線で露光する工程であって、該集成体は、(1)赤外光を透過することのできる支持体と、(2)転写性物質と赤外線吸収染料とを含む転写性層とを備えた供与体を含み、該供与体の転写性層は、該転写性層の露光部分と該転写性層の非露光部とを備えた露光集成体を提供するように受容体に接触した状態である工程と、
該露光集成体の該受容体と該支持体とを分離させて、画像化受容体と使用済み供与体とを取得する工程であって、該画像化受容体は、該受容体と、該転写性物質の転写部分と、該赤外線吸収染料の転写部分とを含み、該IR染料の該転写部分は着色を有し、そして該使用済み供与体は、該支持体と該転写性層の保持部分とを含む工程と、
該赤外線吸収染料の転写部分の50%〜100%を熱的に脱色するのに十分な時間をかけて摂氏約100度〜摂氏約350度の範囲の温度で該転写性物質の転写部分および該赤外線吸収染料の転写部分を加熱する工程であって、該加熱を熱漂白剤の不在下で行って、液晶ディスプレイに使用するのに好適な放射フィルター要素を提供する工程とを含むことを特徴とする放射フィルター要素の製造方法。 - 前記赤外線吸収染料が、
(a)2−(2−(2−クロロ−3−(2−(1,3−ジヒドロ−1,1−ジメチル−3−(4−スルホブチル)−2H−ベンゾ[e]インドール−2−イリデン)エチリデン)−1−シクロヘキセン−1−イル)エテニル)−1,1−ジメチル−3−(4−スルホブチル)−1H−ベンゾ[e]インドリウム,分子内塩,遊離酸、
(b)2−[2−[2−(2−ピリミジノチオ)−3−[2−(1,3−ジヒドロ−1,1−ジメチル−3−(4−スルホブチル)−2H−ベンゾ[e]インドール−2−イリデン)]エチリデン−1−シクロペンテン−1−イル]エテニル]−1,1ジメチル−3−(4−スルホブチル)−1H−ベンゾ[e]インドリウム,分子内塩,ナトリウム塩、
(c)インドシアニングリーン、および
(d)3H−インドリウム,2−[2−[2−クロロ−3−[(1,3−ジヒドロ−1,3,3−トリメチル−2H−インドール−2−イリデン)エチリデン]−1−シクロペンテン−1−イル]エテニル]−1,3,3−トリメチル−,トリフルオロメタンスルホン酸との(1:1)塩よりなる群から選択されることを特徴とする請求項1に記載の方法。 - 請求項1に記載の方法により製造されることを特徴とする放射フィルター要素。
- 請求項1に記載の方法により製造された放射フィルター要素を、導電性コーティング、液晶材料、および配向層に関連づけて備えることを特徴とする液晶ディスプレイデバイス。
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-
2003
- 2003-05-15 AU AU2003237251A patent/AU2003237251A1/en not_active Abandoned
- 2003-05-15 KR KR1020047018037A patent/KR100978185B1/ko not_active IP Right Cessation
- 2003-05-15 WO PCT/US2003/016536 patent/WO2003098351A1/en active Application Filing
- 2003-05-15 JP JP2004505808A patent/JP4310270B2/ja not_active Expired - Fee Related
- 2003-05-15 US US10/510,805 patent/US7018751B2/en not_active Expired - Fee Related
- 2003-05-15 EP EP03736717A patent/EP1506456B1/en not_active Expired - Fee Related
- 2003-05-15 DE DE60328482T patent/DE60328482D1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
US20050214659A1 (en) | 2005-09-29 |
EP1506456A1 (en) | 2005-02-16 |
EP1506456A4 (en) | 2006-06-14 |
KR100978185B1 (ko) | 2010-08-25 |
KR20050012240A (ko) | 2005-01-31 |
EP1506456B1 (en) | 2009-07-22 |
JP2005526284A (ja) | 2005-09-02 |
AU2003237251A1 (en) | 2003-12-02 |
US7018751B2 (en) | 2006-03-28 |
DE60328482D1 (de) | 2009-09-03 |
WO2003098351A1 (en) | 2003-11-27 |
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